DETERMINATION OF INTERFACIAL MECHANICAL PARAMETERS FOR AN Al/EPOXY/Al_2O_3 SYSTEM BY USING PEEL TEST SIMULATIONS

Peel test measurements and simulations of the interfacial mechanical parameters for the Al/Epoxy/Al2O3 system are performed in the present investigation. A series of Al film thicknesses between 20 and 250 microns and three peel angles of 90, 135 and 180 degrees are considered. Two types of epoxy adhesives are adopted to obtain both strong and weak interface adhesions. A finite element model with cohesive zone elements is used to identify the interfacial parameters and simulate the peel test process. By simulating and recording normal stress near the crack tip, the separation strength is obtained, Furthermore, the cohesive energy is identified by comparing the simulated steady-state peel force and the experimental result. It is found from the research that both the cohesive energy and the separation strength can be taken as the intrinsic interfacial parameters which are dependent on the thickness of the adhesive layer and independent of the film thickness and peel angle.

Evolution of bonding interface in solid-liquid cast-rolling bonding of Cu/Al clad strip

Cu/Al clad strips are prepared using solid?liquid cast-rolling bonding(SLCRB)technique with a d160mm×150mm twin-roll experimental caster.The extent of interfacial reactions,composition of the reaction products,and their micro-morphology evolution in the SLCRB process are investigated with scanning electron microscope(SEM),energy dispersive spectrometer(EDS),and X-ray diffraction(XRD).In the casting pool,initial aluminized coating is first generated on the copper strip surface,with the diffusion layer mainly consisting ofα(Al)+CuAl2and growing at high temperatures,with the maximum thickness of10μm.After sequent rolling below the kiss point,the diffusion layer is broken by severe elongation,which leads to an additional crack bond process with a fresh interface of virgin base metal.The average thickness is reduced from10to5μm.The reaction products,CuAl2,CuAl,and Cu9Al4,are dispersed along the rolling direction.Peeling and bending test results indicate that the fracture occurs in the aluminum substrate,and the morphology is a dimple pattern.No crack or separation is found at the bonding interface after90°-180°bending.The presented method provides an economical way to fabricate Cu/Al clad strip directly.

Inverse analysis determining interfacial properties between metal film and ceramic substrate with an adhesive layer

In the present study, peel tests and inverse analysis were performed to determine the interracial mechanical parameters for the metal film/ceramic system with an epoxy interface layer between film and ceramic. Al films with a series of thicknesses between 20 and 250 μm and three peel angles of 90°, 135° and 180° were considered. A finite element model with the cohesive zone elements was used to simulate the peeling process. The finite element results were taken as the training data of a neural network in the inverse analysis. The interracial cohesive energy and the separation strength can be determined based on the inverse analysis and peel experimental result

A Dugdale model based geometrical amplifier enables the measurement of separation-to-failure for a cohesive interface

Regardless of all kinds of different formulae used for the traction-separation relationship in cohesive zone modeling,the peak tractionσ_m and the separation-to-failureδ_0(or equivalently the work-to-separationΓ) are the primary parameters which control the interfacial fracture behaviors. Experimentally,it is hard to determine those quantities,especially forδ_0,which occurs in a very localized region with possibly complicated geometries by material failure.Based on the Dugdale model,we show that the separation-to-failure of an interface could be amplified by a factor of L/r_p in a typical peeling test,where L is the beam length and r_p is the cohesive zone size.Such an amplifier makesδ_0 feasible to be probed quantitatively from a simple peeling test. The method proposed here may be of importance to understanding interfacial fractures of layered structures,or in some nanoscale mechanical phenomena such as delamination of thin films and coatings.

Influence and optimization of parameters of prepreg viscosity during placement

This paper tested the viscosity of prepreg in the automatic placement process, and conducted the probe and placement-90° peel tests through the test systems. The law of variation of prepreg viscosity during the laying process was studied through these tests under different conditions by taking the peel force to intuitively and quantitatively characterise the viscosity of the prepreg.The results show that this viscosity is inversely proportional to the laying rate, proportional to the laying pressure, and quadratic to the laying temperature. Then, peel tests were simulated to validate both the correctness of the peel test and that of the probe test data fitting the two-line cohesion model. On this basis, a response surface test for laying and peeling was designed. Taking viscous peel force as the response target, the laying process parameters were optimised and the significance of their influence was further studied. The error between the test value and the predicted value of the maximum viscous peel force is 3.03%.