In this article,a single-layer symmetrical full-port quasi-absorptive filtering phase shifter is presented.The proposed phase shifter is composed of a main quasi-absorptive filtering branch,a reference quasi-absorptiv...In this article,a single-layer symmetrical full-port quasi-absorptive filtering phase shifter is presented.The proposed phase shifter is composed of a main quasi-absorptive filtering branch,a reference quasi-absorptive filtering branch,and two delay lines.The proposed phase shifter achieves both phase controlling function and quasi-absorptive filtering function for the first time.Each quasi-absorptive filtering branch can realize the quasi-absorptive filtering function.Meanwhile,the constant phase shift can be obtained by combining the two quasi-absorptive filtering branches and the two delay lines.The design formulas can be derived from the even-and odd-mode network analysis,and then two quasi-absorptive filtering phase shifters can be devised easily and quickly.For verification,a 90°quasi-absorptive filtering phase shifter,which is critical for circularly polarized antenna systems,is simulated,manufactured,and measured.展开更多
A poly(L-lactide)-b-poly(ethylene glycol)-b-poly(L-lactide)(PLLA-PEG-PLLA)block copolymer has great potential for use as a flexible bioplastic.Highly flexible bioplastics are required for flexible packaging applicatio...A poly(L-lactide)-b-poly(ethylene glycol)-b-poly(L-lactide)(PLLA-PEG-PLLA)block copolymer has great potential for use as a flexible bioplastic.Highly flexible bioplastics are required for flexible packaging applications.In this work,a PEG was incorporated into block copolymer as a plasticizer by solvent casting.PLLA-PEG-PLLA/PEG blends with different blend ratios were prepared,and the plasticizing effect and miscibility of PEG in block copolymer were intensively investigated compared to PLLA/PEG blends.The results indicated that the PEG was an effective plasticizer for the block copolymer.The blending of PEG decreased glass-transition temperature and accelerated the crystallization of both the PLLA and PLLA-PEG-PLLA matrices.The PEG was completely miscible when blended with block copolymer and it improved thermal stability of the block copolymer matrix but not of the PLLA matrix.Film extensibility of PLLA-PEG-PLLA/PEG blends steadily increased as the PEG ratio increased.These non-toxic and highly flexible PLLA-PEG-PLLA/PEG bioplastics are promising candidates for several applications such as biomedical devices,tissue scaffolds and packaging materials.展开更多
When used for separating multi-component non-stationary signals, the adaptive time-varying filter(ATF) based on multi-scale chirplet sparse signal decomposition(MCSSD) generates phase shift and signal distortion. To o...When used for separating multi-component non-stationary signals, the adaptive time-varying filter(ATF) based on multi-scale chirplet sparse signal decomposition(MCSSD) generates phase shift and signal distortion. To overcome this drawback, the zero phase filter is introduced to the mentioned filter, and a fault diagnosis method for speed-changing gearbox is proposed. Firstly, the gear meshing frequency of each gearbox is estimated by chirplet path pursuit. Then, according to the estimated gear meshing frequencies, an adaptive zero phase time-varying filter(AZPTF) is designed to filter the original signal. Finally, the basis for fault diagnosis is acquired by the envelope order analysis to the filtered signal. The signal consisting of two time-varying amplitude modulation and frequency modulation(AM-FM) signals is respectively analyzed by ATF and AZPTF based on MCSSD. The simulation results show the variances between the original signals and the filtered signals yielded by AZPTF based on MCSSD are 13.67 and 41.14, which are far less than variances (323.45 and 482.86) between the original signals and the filtered signals obtained by ATF based on MCSSD. The experiment results on the vibration signals of gearboxes indicate that the vibration signals of the two speed-changing gearboxes installed on one foundation bed can be separated by AZPTF effectively. Based on the demodulation information of the vibration signal of each gearbox, the fault diagnosis can be implemented. Both simulation and experiment examples prove that the proposed filter can extract a mono-component time-varying AM-FM signal from the multi-component time-varying AM-FM signal without distortion.展开更多
This paper presents a new phase unwrapping algorithm based on the unscented Kalman filter(UKF) for synthetic aperture radar(SAR) interferometry.This method is the result of combining an UKF with path-following str...This paper presents a new phase unwrapping algorithm based on the unscented Kalman filter(UKF) for synthetic aperture radar(SAR) interferometry.This method is the result of combining an UKF with path-following strategy and an omni-directional local phase slope estimator.This technique performs simultaneously noise filtering and phase unwrapping along the high-quality region to the low-quality region,which is also able to avoid going directly through the noisy regions.In addition,phase slope is estimated directly from the sample frequency spectrum of the complex interferogram,by which the underestimation of phase slope is overcome.Simulation and real data processing results validate the effectiveness of the proposed method,and show a significant improvement with respect to the extended Kalman filtering(EKF) algorithm and some conventional phase unwrapping algorithms in some situations.展开更多
Ionic liquid(IL),1-butyl-3-methylimidazolium hexafluorophosphate([BMIM]PF6)as a new and environmentally friendly diluent was introduced to prepare poly(vinylidene fluoride)(PVDF)membranes via thermally induced phase s...Ionic liquid(IL),1-butyl-3-methylimidazolium hexafluorophosphate([BMIM]PF6)as a new and environmentally friendly diluent was introduced to prepare poly(vinylidene fluoride)(PVDF)membranes via thermally induced phase separation(TIPS).Phase diagram of PVDF/[BMIM]PF6 was measured.The effects of polymer concentration and quenching temperature on the morphologies,properties,and performances of the PVDF membranes were investigated.When the polymer concentration was 15 wt%,the pure water flux of the fabricated membrane was up to nearly 2000 L·m-2·h-1,along with adequate mechanical strength.With the increasing of PVDF concentration and quenching temperature,mean pore size and water permeability of the membrane decreased.SEM results showed that PVDF membranes manufactured by ionic liquid(BMIm PF6)presented spherulite structure.And the PVDF membranes were represented asβphase by XRD and FTIR characterization.It provides a new way to prepare PVDF membranes with piezoelectric properties.展开更多
This paper presents an enhanced multi-baseline phase unwrapping algorithm by combining an unscented Kalman filter with an enhanced joint phase gradient estimator based on the amended matrix pencil model, and an optima...This paper presents an enhanced multi-baseline phase unwrapping algorithm by combining an unscented Kalman filter with an enhanced joint phase gradient estimator based on the amended matrix pencil model, and an optimal path-following strategy based on phase quality estimate function. The enhanced joint phase gradient estimator can accurately and effectively extract the phase gradient information of wrapped pixels from noisy interferograms, which greatly increases the performances of the proposed method. The optimal path-following strategy ensures that the proposed algorithm simultaneously performs noise suppression and phase unwrapping along the pixels with high-reliance to the pixels with low-reliance. Accordingly, the proposed algorithm can be predicted to obtain better results, with respect to some other algorithms, as will be demonstrated by the results obtained from synthetic data.展开更多
The phase separation behavior of blend of Surlyn and poly(ethylene terephthalate) (PET) has been studied by scanning electron microscopy and IR. It is shown that particles of Surlyn are dispersed in PET matrix, and th...The phase separation behavior of blend of Surlyn and poly(ethylene terephthalate) (PET) has been studied by scanning electron microscopy and IR. It is shown that particles of Surlyn are dispersed in PET matrix, and this phase separation is controlled by heat-treated conditions of the blend.展开更多
Hydrophilic hyperbranched poly(ester-amine) (HPEA) synthesized from diethanolamine and methyl acrylate was used as phase transfer agent for the first time to transfer methyl orange (MO) from water into chloroform. Thi...Hydrophilic hyperbranched poly(ester-amine) (HPEA) synthesized from diethanolamine and methyl acrylate was used as phase transfer agent for the first time to transfer methyl orange (MO) from water into chloroform. This process was quantified by UV-Vis spectra. A possible mechanism was put forward based on the formation of amphiphilic aggregates.展开更多
In this paper,a new design method for digital infinite impulse response(IIR)filters with nearly linear-phase response is presented using fractional derivative constraints(FDCs).In the proposed method,design problem of...In this paper,a new design method for digital infinite impulse response(IIR)filters with nearly linear-phase response is presented using fractional derivative constraints(FDCs).In the proposed method,design problem of an IIR frlter is constructed as the minimization of phase error between the desired and designed phase response of an allpass filter(APF)such that the designed lowpass filter(LPF)or highpass frlter(HPF)yields less passband(ep),and stopband errors(es)with optimal stopband attenuation(As).In order to have accurate passband(pb)response,FDCs are imposed on appropriate reference frequency,where the optimality of these FDCs are ensured by using a new greedy based sorting mechanism.The simulated results reflect the efficiency of the proposed method in term of improved passband response along with better transition width.However,small reduction in^is observed within the allowable limit,when compared to noin-fractional design approach,but the designed filter remains immune to wordlength(WL)effect.展开更多
Poly(vinylidene fluoride) /polysulfone(PVDF/PSF) flat blend membrane was prepared via thermally induced phase separation(TIPS) technique.The membrane formation mechanism and membrane structure were investigated and th...Poly(vinylidene fluoride) /polysulfone(PVDF/PSF) flat blend membrane was prepared via thermally induced phase separation(TIPS) technique.The membrane formation mechanism and membrane structure were investigated and the effects of PSF/PVDF weight ratio on morphology,crystallinity,porosity,and mechanical properties of the membrane were discussed.The relationship between membrane structure and performances,such as pure water flux and the rejection of carbonic black,was also discussed.It was found that solid-liquid(S-L) phase separation occurred for the PVDF/PSF/diluent system.The addition of PSF influences structure and crystallinity of the membrane,which in turn influences mechanical properties and performances of the membrane.The results reveal that it is possible to obtain network structure via S-L phase separation by blending the polymer,which has a partial compatibility with PVDF.展开更多
Micro-encapsulated phase-change materials(micro PCMs) with Na_2 HPO_4·12 H_2 O encapsulated in poly(lactic acid)(PLA) shell were prepared by a solvent evaporation–precipitation method that involves the use of a ...Micro-encapsulated phase-change materials(micro PCMs) with Na_2 HPO_4·12 H_2 O encapsulated in poly(lactic acid)(PLA) shell were prepared by a solvent evaporation–precipitation method that involves the use of a coaxial needle. The effects of PLA concentration, stirring speed, injection rate of core and shell solutions, and polyvinyl alcohol(PVA) concentration on phase change properties were investigated. The thermal properties of microP CMs were characterized by differential scanning calorimetry(DSC). The capsules prepared under the optimal conditions are about 2 mm in diameter and show a latent heat of up to 122.2 J·g^(-1).展开更多
In the forthcoming 5G systems, new technologies, such as amorphous networks and non-orthogonal filter bank multicarriers(FBMC), provide an effective way to accommodate high-rate transmissions. Meanwhile, the prototype...In the forthcoming 5G systems, new technologies, such as amorphous networks and non-orthogonal filter bank multicarriers(FBMC), provide an effective way to accommodate high-rate transmissions. Meanwhile, the prototype filter affects the adjacent channel interference, and therefore is important for FBMC systems. Besides, once the amorphous network is taken into account, the requirement for interference controlmust be much stricter. Accordingly, this paper focuses on the design of prototype filter with better ability of interference controlling, where we exploit the nonlinear phase FIR filter(NLPFF) instead of traditional linear phase FIR filter(LPFF) to achieve more optimization spaces under a small sacrifice of linear phase. In ourdesigns, both the amplitude and phase responsesare handled independently to approach the stopband performance enhancements, in while the nearly perfect reconstruction(NPR) conditionsare relaxed by pre-specified thresholds. Computer simulations confirm the effectiveness of the NLPFF designs, and demonstrate the advantages of the proposed NLPFF in FBMC applications.展开更多
Poly(vinyl butyral)(PVB) hollow fiber membranes were fabricated via thermally induced phase separation(TIPS).The effects of coagulation bath temperature(CBT) on the structure and performance of membranes were investig...Poly(vinyl butyral)(PVB) hollow fiber membranes were fabricated via thermally induced phase separation(TIPS).The effects of coagulation bath temperature(CBT) on the structure and performance of membranes were investigated in detail.The morphologies of the membranes were studied by scanning electron microscopy(SEM),the performances of water permeability,rejection,breaking strength and elongation were measured,respectively.The results indicate that all the membranes have the asymmetric morphology and the thickness of the skin layer decreases and the pore size of the outer layer increases with the increase of CBT.The permeability of membranes prepared at air gap 1.0 cm and take-up speed 0.253 m/s increases from 1.047×10-7 to 5.909×10-7 m3/(m2·s·kPa) with the CBT increasing from 20 °C to 40 °C,and sharply increases to 35.226×10-7 m3/(m2·s·kPa) once the CBT arrives at 50 °C.While the carbonic ink rejections have no significant decrease,totally exceed 98%,but that of acid-maleic acid copolymer greatly decreases with the increase of CBT.Both the breaking strength and elongation decrease with the increase of CBT.展开更多
Poly(ethylene- co -chlorotrifluoroethylene) with a 1∶1 molar ratio of ethylene and chlorotrifluoroethylene in composition, PECTFE, is a statistically alternating copolymer widely used in cable coating industry. PECTF...Poly(ethylene- co -chlorotrifluoroethylene) with a 1∶1 molar ratio of ethylene and chlorotrifluoroethylene in composition, PECTFE, is a statistically alternating copolymer widely used in cable coating industry. PECTFE has been commonly characterized as a semicrystalline polymer with crystals melting at 238 ℃. Differential scanning calorimetry, thermal mechanical analysis and dynamic mechanical analysis indicated that PECTFE undergoes a reversible solid-solid transition during cooling and heating in the temperature range between 100 ℃ and 200 ℃. Based on detailed structural analysis via wide angle X-ray diffraction and electron diffraction techniques, we proposed that PECTFE possesses a hexagonal phase above 200 ℃( a =0 60 nm, c =0 49 nm) and an orthorhombic phase( a =0 99 nm, b =0 57 nm, c =0 49 nm) at room temperature.展开更多
A novel current-source active power filter (APF) based on multi-modular converter with carrier phase-shifted SPWM (CPS-SPWM) technique is proposed. With this technique, the effect of equivalent high switching frequenc...A novel current-source active power filter (APF) based on multi-modular converter with carrier phase-shifted SPWM (CPS-SPWM) technique is proposed. With this technique, the effect of equivalent high switching frequency con-verter is obtained with low switching frequency converter. It is very promising in current-source APF that adopt super-conducting magnetic energy storage component.展开更多
A method of single-shot phase-shifting digital holography with a photon-sieve-filtering telescope is proposed.Three copy images with different phases are first generated by use of a monofocal photon-sieve filter in Ke...A method of single-shot phase-shifting digital holography with a photon-sieve-filtering telescope is proposed.Three copy images with different phases are first generated by use of a monofocal photon-sieve filter in Kepler telescope,and then interfere with the reference plane wave by a beam combiner.The hologram is captured by a charge-coupled device(CCD)in one single exposure.The complex-valued amplitude of the test object can be reconstructed by three-step phase-shifting interferometry through three frames of extracted sub-interferograms from the single-exposure hologram.The principle and simulation experiments are carried out and verified the validity of our proposed method.This method can be applied for snapshot imaging and three-dimensional object construction.展开更多
This paper reports the use of the fast Fourier transform (FFT) in the direct Fourier transform method (DFM) in Computerized Tomography (CT) reconstruction. Phase corrections are needed in the CT reconstruction. In ord...This paper reports the use of the fast Fourier transform (FFT) in the direct Fourier transform method (DFM) in Computerized Tomography (CT) reconstruction. Phase corrections are needed in the CT reconstruction. In order to eliminate the image distortion from the basic DFM, Padding and band-pass filters are used in the improved DFM. Finally, some reconstructions from simulated projections and several experimental results are given.展开更多
High density polyethylene (HDPE)/polyethylene-block-poly(ethylene glycol) (PE-b-PEG) blend porous membranes were prepared via thermally induced phase separation (TIPS) process using diphenyl ether (DPE) as d...High density polyethylene (HDPE)/polyethylene-block-poly(ethylene glycol) (PE-b-PEG) blend porous membranes were prepared via thermally induced phase separation (TIPS) process using diphenyl ether (DPE) as diluent. The phase diagrams of HDPE/PE-b-PEG/DPE systems were determined by optical microscopy and differential scanning calorimetry (DSC). By varying the content of PE-b-PEG, the effects of PE-b-PEG copolymer on morphology and crystalline structure of membranes were studied by scanning electron microscopy (SEM) and wide angle X-ray diffraction (WAXD). The chemical compositions of whole membranes and surface layers were characterized by elementary analysis, Fourier transform infrared spectroscopy-attenuated total reflection (FTIR-ATR) and X-ray photoelectron spectroscopy (XPS). Water contact angle, static protein adsorption and water flux experiments were used to evaluate the hydrophilicity, antifouling and water permeation properties of the membranes. It was found that the addition of PE-b-PEG increased the pore size of the obtained blend membranes. In the investigated range of PE-b-PEG content, the PEG blocks could not aggregate into obviously separated domains in membrane matrix. More importantly, PE-b-PEG could not only be retained stably in the membrane matrix during membrane formation, but also enrich at the membrane surface layer. Such stability and surface enrichment of PE-b-PEG endowed the blend membranes with improved hydrophilicity, protein absorption resistance and water permeation properties, which would be substantially beneficial to HDPE membranes for water treatment application.展开更多
This paper proposes a new multi-baseline extended particle filtering phase unwrapping algorithm which combines an extended particle filter with an amended matrix pencil model and a quantized path-following strategy. T...This paper proposes a new multi-baseline extended particle filtering phase unwrapping algorithm which combines an extended particle filter with an amended matrix pencil model and a quantized path-following strategy. The contributions to multibaseline synthetic aperture radar(SAR) interferometry are as follows: a new recursive multi-baseline phase unwrapping model based on an extended particle filter is built, and the amended matrix pencil model is used to acquire phase gradient information with a higher precision and lower computational cost, and the quantized path-following strategy is introduced to guide the proposed phase unwrapping procedure to efficiently unwrap wrapped phase image along the paths routed by a phase derivative variance map.展开更多
Swelling capacity of vinyl chloride (VC) in chlorinated polyethylene (CPE) with 25—40 wt% Cl at temperature 30—57℃ was studied and their relationships were correlated with Langmuir and Freundlich adsorption equatio...Swelling capacity of vinyl chloride (VC) in chlorinated polyethylene (CPE) with 25—40 wt% Cl at temperature 30—57℃ was studied and their relationships were correlated with Langmuir and Freundlich adsorption equations. A ternary phase diagram for VC-CPE-PVC was also established. In-situ polymerization conditions of CPE-g-VC were proposed and CPE content control was analyzed for the manufacturing process of CPE-g-VC graft product based on results of phase equilibrium study.展开更多
基金supported by National Natural Science Foundations of China(No.U20A20203,No.61971052,U21A20510)the Fundamental Research Funds for the Central Universities(2021XDA07-1)Key Research and Development Project of Guangdong Province(2020B0101080001)。
文摘In this article,a single-layer symmetrical full-port quasi-absorptive filtering phase shifter is presented.The proposed phase shifter is composed of a main quasi-absorptive filtering branch,a reference quasi-absorptive filtering branch,and two delay lines.The proposed phase shifter achieves both phase controlling function and quasi-absorptive filtering function for the first time.Each quasi-absorptive filtering branch can realize the quasi-absorptive filtering function.Meanwhile,the constant phase shift can be obtained by combining the two quasi-absorptive filtering branches and the two delay lines.The design formulas can be derived from the even-and odd-mode network analysis,and then two quasi-absorptive filtering phase shifters can be devised easily and quickly.For verification,a 90°quasi-absorptive filtering phase shifter,which is critical for circularly polarized antenna systems,is simulated,manufactured,and measured.
基金financially supported by Mahasarakham University。
文摘A poly(L-lactide)-b-poly(ethylene glycol)-b-poly(L-lactide)(PLLA-PEG-PLLA)block copolymer has great potential for use as a flexible bioplastic.Highly flexible bioplastics are required for flexible packaging applications.In this work,a PEG was incorporated into block copolymer as a plasticizer by solvent casting.PLLA-PEG-PLLA/PEG blends with different blend ratios were prepared,and the plasticizing effect and miscibility of PEG in block copolymer were intensively investigated compared to PLLA/PEG blends.The results indicated that the PEG was an effective plasticizer for the block copolymer.The blending of PEG decreased glass-transition temperature and accelerated the crystallization of both the PLLA and PLLA-PEG-PLLA matrices.The PEG was completely miscible when blended with block copolymer and it improved thermal stability of the block copolymer matrix but not of the PLLA matrix.Film extensibility of PLLA-PEG-PLLA/PEG blends steadily increased as the PEG ratio increased.These non-toxic and highly flexible PLLA-PEG-PLLA/PEG bioplastics are promising candidates for several applications such as biomedical devices,tissue scaffolds and packaging materials.
基金supported by National Natural Science Foundation of China (Grant No. 71271078)National Hi-tech Research and Development Program of China (863 Program, Grant No. 2009AA04Z414)Integration of Industry, Education and Research of Guangdong Province, and Ministry of Education of China (Grant No. 2009B090300312)
文摘When used for separating multi-component non-stationary signals, the adaptive time-varying filter(ATF) based on multi-scale chirplet sparse signal decomposition(MCSSD) generates phase shift and signal distortion. To overcome this drawback, the zero phase filter is introduced to the mentioned filter, and a fault diagnosis method for speed-changing gearbox is proposed. Firstly, the gear meshing frequency of each gearbox is estimated by chirplet path pursuit. Then, according to the estimated gear meshing frequencies, an adaptive zero phase time-varying filter(AZPTF) is designed to filter the original signal. Finally, the basis for fault diagnosis is acquired by the envelope order analysis to the filtered signal. The signal consisting of two time-varying amplitude modulation and frequency modulation(AM-FM) signals is respectively analyzed by ATF and AZPTF based on MCSSD. The simulation results show the variances between the original signals and the filtered signals yielded by AZPTF based on MCSSD are 13.67 and 41.14, which are far less than variances (323.45 and 482.86) between the original signals and the filtered signals obtained by ATF based on MCSSD. The experiment results on the vibration signals of gearboxes indicate that the vibration signals of the two speed-changing gearboxes installed on one foundation bed can be separated by AZPTF effectively. Based on the demodulation information of the vibration signal of each gearbox, the fault diagnosis can be implemented. Both simulation and experiment examples prove that the proposed filter can extract a mono-component time-varying AM-FM signal from the multi-component time-varying AM-FM signal without distortion.
基金supported by the National Natural Science Foundation of China (60772143)
文摘This paper presents a new phase unwrapping algorithm based on the unscented Kalman filter(UKF) for synthetic aperture radar(SAR) interferometry.This method is the result of combining an UKF with path-following strategy and an omni-directional local phase slope estimator.This technique performs simultaneously noise filtering and phase unwrapping along the high-quality region to the low-quality region,which is also able to avoid going directly through the noisy regions.In addition,phase slope is estimated directly from the sample frequency spectrum of the complex interferogram,by which the underestimation of phase slope is overcome.Simulation and real data processing results validate the effectiveness of the proposed method,and show a significant improvement with respect to the extended Kalman filtering(EKF) algorithm and some conventional phase unwrapping algorithms in some situations.
基金the financial support of the National Natural Science Foundation of China(Grant No.21606125)the Natural Science Foundation of Jiangsu Province(Grant No.BK20160984)+3 种基金the National Key R&D Program of China(Grant No.2017YFC0403702)the Materials-Oriented Chemical Engineering State Key Laboratory Program(KL16-09)the open project program of Jiangsu Key Lab for Chemistry of Low-Dimensional Materials(JSKC17005)the Priority Academic Program Development of Jiangsu Higher Education Institution(PAPD)。
文摘Ionic liquid(IL),1-butyl-3-methylimidazolium hexafluorophosphate([BMIM]PF6)as a new and environmentally friendly diluent was introduced to prepare poly(vinylidene fluoride)(PVDF)membranes via thermally induced phase separation(TIPS).Phase diagram of PVDF/[BMIM]PF6 was measured.The effects of polymer concentration and quenching temperature on the morphologies,properties,and performances of the PVDF membranes were investigated.When the polymer concentration was 15 wt%,the pure water flux of the fabricated membrane was up to nearly 2000 L·m-2·h-1,along with adequate mechanical strength.With the increasing of PVDF concentration and quenching temperature,mean pore size and water permeability of the membrane decreased.SEM results showed that PVDF membranes manufactured by ionic liquid(BMIm PF6)presented spherulite structure.And the PVDF membranes were represented asβphase by XRD and FTIR characterization.It provides a new way to prepare PVDF membranes with piezoelectric properties.
基金supported by the National Natural Science Foundation of China(4120147961261033+2 种基金61461011)the Guangxi Natural Science Foundation(2014GXNSFBA118273)the Dean Project of Guangxi Key Laboratory of Wireless Broadband Communication and Signal Processing(GXKL061503)
文摘This paper presents an enhanced multi-baseline phase unwrapping algorithm by combining an unscented Kalman filter with an enhanced joint phase gradient estimator based on the amended matrix pencil model, and an optimal path-following strategy based on phase quality estimate function. The enhanced joint phase gradient estimator can accurately and effectively extract the phase gradient information of wrapped pixels from noisy interferograms, which greatly increases the performances of the proposed method. The optimal path-following strategy ensures that the proposed algorithm simultaneously performs noise suppression and phase unwrapping along the pixels with high-reliance to the pixels with low-reliance. Accordingly, the proposed algorithm can be predicted to obtain better results, with respect to some other algorithms, as will be demonstrated by the results obtained from synthetic data.
文摘The phase separation behavior of blend of Surlyn and poly(ethylene terephthalate) (PET) has been studied by scanning electron microscopy and IR. It is shown that particles of Surlyn are dispersed in PET matrix, and this phase separation is controlled by heat-treated conditions of the blend.
文摘Hydrophilic hyperbranched poly(ester-amine) (HPEA) synthesized from diethanolamine and methyl acrylate was used as phase transfer agent for the first time to transfer methyl orange (MO) from water into chloroform. This process was quantified by UV-Vis spectra. A possible mechanism was put forward based on the formation of amphiphilic aggregates.
文摘In this paper,a new design method for digital infinite impulse response(IIR)filters with nearly linear-phase response is presented using fractional derivative constraints(FDCs).In the proposed method,design problem of an IIR frlter is constructed as the minimization of phase error between the desired and designed phase response of an allpass filter(APF)such that the designed lowpass filter(LPF)or highpass frlter(HPF)yields less passband(ep),and stopband errors(es)with optimal stopband attenuation(As).In order to have accurate passband(pb)response,FDCs are imposed on appropriate reference frequency,where the optimality of these FDCs are ensured by using a new greedy based sorting mechanism.The simulated results reflect the efficiency of the proposed method in term of improved passband response along with better transition width.However,small reduction in^is observed within the allowable limit,when compared to noin-fractional design approach,but the designed filter remains immune to wordlength(WL)effect.
基金National Natural Foundation of China(No.51003074)
文摘Poly(vinylidene fluoride) /polysulfone(PVDF/PSF) flat blend membrane was prepared via thermally induced phase separation(TIPS) technique.The membrane formation mechanism and membrane structure were investigated and the effects of PSF/PVDF weight ratio on morphology,crystallinity,porosity,and mechanical properties of the membrane were discussed.The relationship between membrane structure and performances,such as pure water flux and the rejection of carbonic black,was also discussed.It was found that solid-liquid(S-L) phase separation occurred for the PVDF/PSF/diluent system.The addition of PSF influences structure and crystallinity of the membrane,which in turn influences mechanical properties and performances of the membrane.The results reveal that it is possible to obtain network structure via S-L phase separation by blending the polymer,which has a partial compatibility with PVDF.
基金Supported by the National Natural Science Foundation of China(21476065)the China National Tobacco Corporation
文摘Micro-encapsulated phase-change materials(micro PCMs) with Na_2 HPO_4·12 H_2 O encapsulated in poly(lactic acid)(PLA) shell were prepared by a solvent evaporation–precipitation method that involves the use of a coaxial needle. The effects of PLA concentration, stirring speed, injection rate of core and shell solutions, and polyvinyl alcohol(PVA) concentration on phase change properties were investigated. The thermal properties of microP CMs were characterized by differential scanning calorimetry(DSC). The capsules prepared under the optimal conditions are about 2 mm in diameter and show a latent heat of up to 122.2 J·g^(-1).
基金supported by National Natural Science Foundation of China under Grants No.61471322
文摘In the forthcoming 5G systems, new technologies, such as amorphous networks and non-orthogonal filter bank multicarriers(FBMC), provide an effective way to accommodate high-rate transmissions. Meanwhile, the prototype filter affects the adjacent channel interference, and therefore is important for FBMC systems. Besides, once the amorphous network is taken into account, the requirement for interference controlmust be much stricter. Accordingly, this paper focuses on the design of prototype filter with better ability of interference controlling, where we exploit the nonlinear phase FIR filter(NLPFF) instead of traditional linear phase FIR filter(LPFF) to achieve more optimization spaces under a small sacrifice of linear phase. In ourdesigns, both the amplitude and phase responsesare handled independently to approach the stopband performance enhancements, in while the nearly perfect reconstruction(NPR) conditionsare relaxed by pre-specified thresholds. Computer simulations confirm the effectiveness of the NLPFF designs, and demonstrate the advantages of the proposed NLPFF in FBMC applications.
基金Project(21176264)supported by the National Natural Science Foundation of ChinaProject(11JJ2010)supported by the Hunan Provincial Natural Science Foundation of China
文摘Poly(vinyl butyral)(PVB) hollow fiber membranes were fabricated via thermally induced phase separation(TIPS).The effects of coagulation bath temperature(CBT) on the structure and performance of membranes were investigated in detail.The morphologies of the membranes were studied by scanning electron microscopy(SEM),the performances of water permeability,rejection,breaking strength and elongation were measured,respectively.The results indicate that all the membranes have the asymmetric morphology and the thickness of the skin layer decreases and the pore size of the outer layer increases with the increase of CBT.The permeability of membranes prepared at air gap 1.0 cm and take-up speed 0.253 m/s increases from 1.047×10-7 to 5.909×10-7 m3/(m2·s·kPa) with the CBT increasing from 20 °C to 40 °C,and sharply increases to 35.226×10-7 m3/(m2·s·kPa) once the CBT arrives at 50 °C.While the carbonic ink rejections have no significant decrease,totally exceed 98%,but that of acid-maleic acid copolymer greatly decreases with the increase of CBT.Both the breaking strength and elongation decrease with the increase of CBT.
文摘Poly(ethylene- co -chlorotrifluoroethylene) with a 1∶1 molar ratio of ethylene and chlorotrifluoroethylene in composition, PECTFE, is a statistically alternating copolymer widely used in cable coating industry. PECTFE has been commonly characterized as a semicrystalline polymer with crystals melting at 238 ℃. Differential scanning calorimetry, thermal mechanical analysis and dynamic mechanical analysis indicated that PECTFE undergoes a reversible solid-solid transition during cooling and heating in the temperature range between 100 ℃ and 200 ℃. Based on detailed structural analysis via wide angle X-ray diffraction and electron diffraction techniques, we proposed that PECTFE possesses a hexagonal phase above 200 ℃( a =0 60 nm, c =0 49 nm) and an orthorhombic phase( a =0 99 nm, b =0 57 nm, c =0 49 nm) at room temperature.
文摘A novel current-source active power filter (APF) based on multi-modular converter with carrier phase-shifted SPWM (CPS-SPWM) technique is proposed. With this technique, the effect of equivalent high switching frequency con-verter is obtained with low switching frequency converter. It is very promising in current-source APF that adopt super-conducting magnetic energy storage component.
基金Project supported by the Youth Innovation Promotion Association of the Chinese Academy of Sciences(Grant No.2017292)the National Natural Science Foundation of China(Grant No.61775222)the Zhejiang Provincial Natural Science Foundation of China(Grant No.LQ16A050001)
文摘A method of single-shot phase-shifting digital holography with a photon-sieve-filtering telescope is proposed.Three copy images with different phases are first generated by use of a monofocal photon-sieve filter in Kepler telescope,and then interfere with the reference plane wave by a beam combiner.The hologram is captured by a charge-coupled device(CCD)in one single exposure.The complex-valued amplitude of the test object can be reconstructed by three-step phase-shifting interferometry through three frames of extracted sub-interferograms from the single-exposure hologram.The principle and simulation experiments are carried out and verified the validity of our proposed method.This method can be applied for snapshot imaging and three-dimensional object construction.
文摘This paper reports the use of the fast Fourier transform (FFT) in the direct Fourier transform method (DFM) in Computerized Tomography (CT) reconstruction. Phase corrections are needed in the CT reconstruction. In order to eliminate the image distortion from the basic DFM, Padding and band-pass filters are used in the improved DFM. Finally, some reconstructions from simulated projections and several experimental results are given.
基金supported by the 863 program(No.2006AA03Z233)973 program(No.2009CB623402) of China
文摘High density polyethylene (HDPE)/polyethylene-block-poly(ethylene glycol) (PE-b-PEG) blend porous membranes were prepared via thermally induced phase separation (TIPS) process using diphenyl ether (DPE) as diluent. The phase diagrams of HDPE/PE-b-PEG/DPE systems were determined by optical microscopy and differential scanning calorimetry (DSC). By varying the content of PE-b-PEG, the effects of PE-b-PEG copolymer on morphology and crystalline structure of membranes were studied by scanning electron microscopy (SEM) and wide angle X-ray diffraction (WAXD). The chemical compositions of whole membranes and surface layers were characterized by elementary analysis, Fourier transform infrared spectroscopy-attenuated total reflection (FTIR-ATR) and X-ray photoelectron spectroscopy (XPS). Water contact angle, static protein adsorption and water flux experiments were used to evaluate the hydrophilicity, antifouling and water permeation properties of the membranes. It was found that the addition of PE-b-PEG increased the pore size of the obtained blend membranes. In the investigated range of PE-b-PEG content, the PEG blocks could not aggregate into obviously separated domains in membrane matrix. More importantly, PE-b-PEG could not only be retained stably in the membrane matrix during membrane formation, but also enrich at the membrane surface layer. Such stability and surface enrichment of PE-b-PEG endowed the blend membranes with improved hydrophilicity, protein absorption resistance and water permeation properties, which would be substantially beneficial to HDPE membranes for water treatment application.
基金supported by the National Natural Science Foundation of China(4166109261461011)the Natural Science Foundation of Guangxi Province(2014GXNSFBA118273)
文摘This paper proposes a new multi-baseline extended particle filtering phase unwrapping algorithm which combines an extended particle filter with an amended matrix pencil model and a quantized path-following strategy. The contributions to multibaseline synthetic aperture radar(SAR) interferometry are as follows: a new recursive multi-baseline phase unwrapping model based on an extended particle filter is built, and the amended matrix pencil model is used to acquire phase gradient information with a higher precision and lower computational cost, and the quantized path-following strategy is introduced to guide the proposed phase unwrapping procedure to efficiently unwrap wrapped phase image along the paths routed by a phase derivative variance map.
基金This project is supported by National Natural Science Foundation of China
文摘Swelling capacity of vinyl chloride (VC) in chlorinated polyethylene (CPE) with 25—40 wt% Cl at temperature 30—57℃ was studied and their relationships were correlated with Langmuir and Freundlich adsorption equations. A ternary phase diagram for VC-CPE-PVC was also established. In-situ polymerization conditions of CPE-g-VC were proposed and CPE content control was analyzed for the manufacturing process of CPE-g-VC graft product based on results of phase equilibrium study.