The X-ray powder diffraction data of the compound GdAlSi was studied by means of X-ray diffraction technique and refined by Rietveld method. The compound GdAlSi has tetragonal α-ThSi_2-type structure, space group I4_...The X-ray powder diffraction data of the compound GdAlSi was studied by means of X-ray diffraction technique and refined by Rietveld method. The compound GdAlSi has tetragonal α-ThSi_2-type structure, space group I4_1/amd (No.141), Z=4, the lattice parameters a=041234 (1) nm, c=1.44202(1) nm. The Smith and Snyder figure of merit [5] F_N is F_ 30=2521(36). The R-factors of Rietveld refinement are R_p=0.098 and R_ wp=0.128. The X-ray powder diffraction data are given. The field dependence of the magnetization measured at room temperature and the temperature variation of the inverse magnetic susceptibility of the compound GdAlSi were also presented.展开更多
A new compound K6FeNb15O42 was prepared for the first time by solid state reaction in K2O-Fe2O3-Nb2O5 ternary system. The X-ray powder diffraction data of the title compound was measured. K6FeNb15 O42 crystallizes in ...A new compound K6FeNb15O42 was prepared for the first time by solid state reaction in K2O-Fe2O3-Nb2O5 ternary system. The X-ray powder diffraction data of the title compound was measured. K6FeNb15 O42 crystallizes in the hexagonal system with unit cell parameters, a = 9. 1320(4) A ,c = 12. 0670(9) A , and space group P63/mcm (193) , z = 1. The calculated and measured densities are 4. 489 g/cm3 and 4. 485 g. cm3, respectively.展开更多
A new compound K6FeNb15O42 u(?) prepared for the first time by solid state reaction in K2O-Fe2O3-Nb2O5 ternary system. The XRD data of the title compound was determined. K6FeNb15O42 crystallizes the hexagonal system w...A new compound K6FeNb15O42 u(?) prepared for the first time by solid state reaction in K2O-Fe2O3-Nb2O5 ternary system. The XRD data of the title compound was determined. K6FeNb15O42 crystallizes the hexagonal system with unit cell parameters a=9. 1320(4) A,c=12. 0670(9) A, and space group P63/mcm(193) , 2=1. The calculated and measured densities are 4. 489 g/ cm3 and 4. 485 g. cm3, respectively.展开更多
The compound NdAlSi was studied using X-ray powder diffraction technique and refined by the Rietveld method. The compound NdAlSi has tetragonal α-ThSiE-type structure, space group I41/amd （No. 141）, Z = 4, and the ...The compound NdAlSi was studied using X-ray powder diffraction technique and refined by the Rietveld method. The compound NdAlSi has tetragonal α-ThSiE-type structure, space group I41/amd （No. 141）, Z = 4, and the lattice parameters a = 0.41991（1） nm, c = 1.44916（3） nm. The Smith and Snyder figure of merit FN is F30= 103.1（36）. The R-factors of Rietveld refinement are Rp= 0.113 and Rwp= 0.148, respectively. The X-ray powder diffraction data is presented in this article.展开更多
A new compound K6Ti0.67Nb15.33O42 was prepared for the first time by solid state reaction in K2O-Ni2O3-Nb2O5 ternary system. The new compound was characterized by electron probe, X-ray powder diffraction and DTA. The ...A new compound K6Ti0.67Nb15.33O42 was prepared for the first time by solid state reaction in K2O-Ni2O3-Nb2O5 ternary system. The new compound was characterized by electron probe, X-ray powder diffraction and DTA. The result of X-ray powder diffraction shows that K6Ti0.67Nb15.33O42 crystallizes the hexagonal system with unit cell parameters a = 9. 1341(5) A ,c=12. 090(1)A . and space group P62/mcm(193 ).展开更多
文摘The X-ray powder diffraction data of the compound GdAlSi was studied by means of X-ray diffraction technique and refined by Rietveld method. The compound GdAlSi has tetragonal α-ThSi_2-type structure, space group I4_1/amd (No.141), Z=4, the lattice parameters a=041234 (1) nm, c=1.44202(1) nm. The Smith and Snyder figure of merit [5] F_N is F_ 30=2521(36). The R-factors of Rietveld refinement are R_p=0.098 and R_ wp=0.128. The X-ray powder diffraction data are given. The field dependence of the magnetization measured at room temperature and the temperature variation of the inverse magnetic susceptibility of the compound GdAlSi were also presented.
基金Fund by International Centre for Dlffractlon Data.
文摘A new compound K6FeNb15O42 was prepared for the first time by solid state reaction in K2O-Fe2O3-Nb2O5 ternary system. The X-ray powder diffraction data of the title compound was measured. K6FeNb15 O42 crystallizes in the hexagonal system with unit cell parameters, a = 9. 1320(4) A ,c = 12. 0670(9) A , and space group P63/mcm (193) , z = 1. The calculated and measured densities are 4. 489 g/cm3 and 4. 485 g. cm3, respectively.
文摘A new compound K6FeNb15O42 u(?) prepared for the first time by solid state reaction in K2O-Fe2O3-Nb2O5 ternary system. The XRD data of the title compound was determined. K6FeNb15O42 crystallizes the hexagonal system with unit cell parameters a=9. 1320(4) A,c=12. 0670(9) A, and space group P63/mcm(193) , 2=1. The calculated and measured densities are 4. 489 g/ cm3 and 4. 485 g. cm3, respectively.
基金This project was financially supported by the Doctoral Start-up Foundation of Guangxi University.
文摘The compound NdAlSi was studied using X-ray powder diffraction technique and refined by the Rietveld method. The compound NdAlSi has tetragonal α-ThSiE-type structure, space group I41/amd （No. 141）, Z = 4, and the lattice parameters a = 0.41991（1） nm, c = 1.44916（3） nm. The Smith and Snyder figure of merit FN is F30= 103.1（36）. The R-factors of Rietveld refinement are Rp= 0.113 and Rwp= 0.148, respectively. The X-ray powder diffraction data is presented in this article.
基金Funded by International Centre for Diffraction Data.
文摘A new compound K6Ti0.67Nb15.33O42 was prepared for the first time by solid state reaction in K2O-Ni2O3-Nb2O5 ternary system. The new compound was characterized by electron probe, X-ray powder diffraction and DTA. The result of X-ray powder diffraction shows that K6Ti0.67Nb15.33O42 crystallizes the hexagonal system with unit cell parameters a = 9. 1341(5) A ,c=12. 090(1)A . and space group P62/mcm(193 ).
