An extra-low interstitial near alpha alloy Ti-3Al-2Zr-2Mo(wt%) was fabricated by hydrogenation and thermomechanical consolidation(TMC) of the coarse and spherical pre-alloyed powder with particle sizes of 60 to 270 μ...An extra-low interstitial near alpha alloy Ti-3Al-2Zr-2Mo(wt%) was fabricated by hydrogenation and thermomechanical consolidation(TMC) of the coarse and spherical pre-alloyed powder with particle sizes of 60 to 270 μm. The coarse powder is a byproduct of pre-alloyed powder produced for selective laser and electron beam additive manufacturing. The TMC process involves powder compaction, fast sintering,in-situ dehydrogenation and an immediate hot extrusion to form a fully dense and fine-grained martensitic microstructure. Further dehydrogenation in vaccum at 700 °C converted the martensitic microstructure into an interwoven α/β microstructure which exhibited an improved yield strength, apparent necking and premature cracking at grain boundary α(α_(GB)) ribbons. A further annealing of 880 ℃/1 h/AC led to the formation of a fine-grained α/β_(t)composite structure, which achieved an enhance ultimate tensile strength of 835 MPa and excellent tensile ductility of 16.0%. Analysis of the deformation behavior of the alloy in different states revealed that the α/β_(t)composite structures brought about an enhanced strain hardening capability by heterogeneous deformation effect of hard β_(t)and soft α-laths, which inhibited the formation of microcracks and consequently improved the coordinated deformation.展开更多
Pre-alloyed powder of Ti-22Al-24Nb-0.5Mo（atomic fraction,%） was prepared by gas atomization.Powder metallurgy（PM） Ti 2AlNb alloys were prepared by a hot isostatic pressing（HIPing） route.The influence of experime...Pre-alloyed powder of Ti-22Al-24Nb-0.5Mo（atomic fraction,%） was prepared by gas atomization.Powder metallurgy（PM） Ti 2AlNb alloys were prepared by a hot isostatic pressing（HIPing） route.The influence of experimental variables including HIPing temperatures,solution and aging temperatures on microstructure and properties of PM Ti 2AlNb alloys was studied.The results showed that HIPing temperature affected the porosity distribution and mechanical properties of PM Ti 2AlNb alloys.The microstructure and mechanical properties of the PM Ti 2AlNb alloys changed obviously after various post heat treatments,and a good combination of tensile strength,ductility and rupture lifetime was obtained through an optimized heat treatment in the present work.展开更多
基金financially supported by the“Xing Liao Talent Plan”of Liaoning Province,China(No.XLYC1802080)the Fundamental Research Fund for the Central Universities(No.02080022117003)。
文摘An extra-low interstitial near alpha alloy Ti-3Al-2Zr-2Mo(wt%) was fabricated by hydrogenation and thermomechanical consolidation(TMC) of the coarse and spherical pre-alloyed powder with particle sizes of 60 to 270 μm. The coarse powder is a byproduct of pre-alloyed powder produced for selective laser and electron beam additive manufacturing. The TMC process involves powder compaction, fast sintering,in-situ dehydrogenation and an immediate hot extrusion to form a fully dense and fine-grained martensitic microstructure. Further dehydrogenation in vaccum at 700 °C converted the martensitic microstructure into an interwoven α/β microstructure which exhibited an improved yield strength, apparent necking and premature cracking at grain boundary α(α_(GB)) ribbons. A further annealing of 880 ℃/1 h/AC led to the formation of a fine-grained α/β_(t)composite structure, which achieved an enhance ultimate tensile strength of 835 MPa and excellent tensile ductility of 16.0%. Analysis of the deformation behavior of the alloy in different states revealed that the α/β_(t)composite structures brought about an enhanced strain hardening capability by heterogeneous deformation effect of hard β_(t)and soft α-laths, which inhibited the formation of microcracks and consequently improved the coordinated deformation.
文摘Pre-alloyed powder of Ti-22Al-24Nb-0.5Mo（atomic fraction,%） was prepared by gas atomization.Powder metallurgy（PM） Ti 2AlNb alloys were prepared by a hot isostatic pressing（HIPing） route.The influence of experimental variables including HIPing temperatures,solution and aging temperatures on microstructure and properties of PM Ti 2AlNb alloys was studied.The results showed that HIPing temperature affected the porosity distribution and mechanical properties of PM Ti 2AlNb alloys.The microstructure and mechanical properties of the PM Ti 2AlNb alloys changed obviously after various post heat treatments,and a good combination of tensile strength,ductility and rupture lifetime was obtained through an optimized heat treatment in the present work.
