The aim of this paper is to establish LIMS （laboratory information management system） for the tea pesticides analysis accredited laboratories in Taiwan. The LIMS could help Tungting station and Nantou pesticide insp...The aim of this paper is to establish LIMS （laboratory information management system） for the tea pesticides analysis accredited laboratories in Taiwan. The LIMS could help Tungting station and Nantou pesticide inspection station to computerize the pesticide analysis data. It has completed eight management subsystems so far, including the basic information management subsystem, thesample processing management subsystem, the analysis data management subsystem, the analysis report management subsystem, the inspection standard management subsystem, the instrument connection management subsystem, the laboratory personnel training management subsystem and the laboratory quality document management subsystem. Using the automatic tea pesticide analysis information management system could help laboratory operations to reduce the amount of excess paperwork and human resource, which could ensure the analysis data quality is traceable and reliable.展开更多
The present study was aimed to validate an analytical method for the quantification of 19 organochlorine and 2 synthetic pyrethroid pesticide residues in water samples using modified quick, easy, cheap, effective, rug...The present study was aimed to validate an analytical method for the quantification of 19 organochlorine and 2 synthetic pyrethroid pesticide residues in water samples using modified quick, easy, cheap, effective, rugged and safe (QuEChERS) extraction and Gas Chromatography coupled with Electron Capture Detector (ECD). The selected pesticide residues were determined by in-house validated method. The analytical method was validated by evaluating the accuracy, precision, linearity, limit of detection (LOD) and limit of quantification (LOQ). The average recoveries of the selected pesticides ranged from 78% to 117% with RSDr ≤ 12% in two fortification levels of 0.02 and 0.1 mg/L. The linearity was ≥0.995 for all of the selected pesticides. The LOD ranged from 0.003 to 0.006 mg/L and the LOQ was 0.02 mg/L for all the selected analytes. This method was applied satisfactorily for the residue analysis of 108 water samples collected from nine districts of Bangladesh. Among the analyzed samples, only 4 had cypermethrin residues (0.026 mg/L, 0.034 mg/L, 0.045 mg/L and 0.05 mg/L). The level of detected cypermethrin residues were above the WHO recommended guide line values of water quality.展开更多
文摘The aim of this paper is to establish LIMS （laboratory information management system） for the tea pesticides analysis accredited laboratories in Taiwan. The LIMS could help Tungting station and Nantou pesticide inspection station to computerize the pesticide analysis data. It has completed eight management subsystems so far, including the basic information management subsystem, thesample processing management subsystem, the analysis data management subsystem, the analysis report management subsystem, the inspection standard management subsystem, the instrument connection management subsystem, the laboratory personnel training management subsystem and the laboratory quality document management subsystem. Using the automatic tea pesticide analysis information management system could help laboratory operations to reduce the amount of excess paperwork and human resource, which could ensure the analysis data quality is traceable and reliable.
文摘The present study was aimed to validate an analytical method for the quantification of 19 organochlorine and 2 synthetic pyrethroid pesticide residues in water samples using modified quick, easy, cheap, effective, rugged and safe (QuEChERS) extraction and Gas Chromatography coupled with Electron Capture Detector (ECD). The selected pesticide residues were determined by in-house validated method. The analytical method was validated by evaluating the accuracy, precision, linearity, limit of detection (LOD) and limit of quantification (LOQ). The average recoveries of the selected pesticides ranged from 78% to 117% with RSDr ≤ 12% in two fortification levels of 0.02 and 0.1 mg/L. The linearity was ≥0.995 for all of the selected pesticides. The LOD ranged from 0.003 to 0.006 mg/L and the LOQ was 0.02 mg/L for all the selected analytes. This method was applied satisfactorily for the residue analysis of 108 water samples collected from nine districts of Bangladesh. Among the analyzed samples, only 4 had cypermethrin residues (0.026 mg/L, 0.034 mg/L, 0.045 mg/L and 0.05 mg/L). The level of detected cypermethrin residues were above the WHO recommended guide line values of water quality.
