A quantitative analysis of the porosity,pore size distribution,and fractal dimensions of pores is significant for studying the pore structure characteristics of coal.This study utilized 12 anthracite coal samples from...A quantitative analysis of the porosity,pore size distribution,and fractal dimensions of pores is significant for studying the pore structure characteristics of coal.This study utilized 12 anthracite coal samples from the Sihe mining area to explore the pore structure characteristics of the coal therein.Hundred randomly selected points on each sliced coal sample were imaged via scanning electron microscopy,and a total of 1200 images were used for the analysis.The porosity and fractal dimensions of the coal samples were analyzed via digital image processing and box-counting dimension methods.This method is characterized by extensive graphical analysis,and the results are based on statistical methods.These were also used to analyze the structural and development characteristics of the microscopic pores in the coal.The results reveal that the surface porosity obtained via digital image processing was 16.11%lower than that measured experimentally.The fractal dimension and porosity of the pore surface were fitted to a natural logarithmic curve.The rate of change in the pore fractal dimension depends on the porosity such that,to some degree,a greater porosity is associated with more complex pore structures,a higher degree of micropore development,and improved pore connectivity.展开更多
After exposure to freeze-thaw cycles, scanning electron microscopy(SEM) and nuclear magnetic resonance(NMR) were used to test the four mixtures. The microstructure is qualitatively analyzed from the 2D SEM image and t...After exposure to freeze-thaw cycles, scanning electron microscopy(SEM) and nuclear magnetic resonance(NMR) were used to test the four mixtures. The microstructure is qualitatively analyzed from the 2D SEM image and the 3D pore distribution curve before and after freezing and thawing. The fractal dimension is utilized to characterize the two-dimensional topography image and the three-dimensional pore distribution, quantitatively. The results reveal that the surface porosity and volume porosity increase as the freeze-thaw action increases. Self-similarity characteristics exist in micro-damage inside the concrete. In the fractal dimension, it is possible to characterize pore evolution quantitatively. The fractal dimension correlates with pore damage evolution. The fractal dimension effectively quantitatively characterizes micro-damage features at various scales from the local to the global level.展开更多
Morphology of hydraulic fracture surface has significant effects on oil and gas flow,proppant migration and fracture closure,which plays an important role in oil and gas fracturing stimulation.In this paper,we analyze...Morphology of hydraulic fracture surface has significant effects on oil and gas flow,proppant migration and fracture closure,which plays an important role in oil and gas fracturing stimulation.In this paper,we analyzed the fracture surface characteristics induced by supercritical carbon dioxide(SC-CO_(2))and water in open-hole and perforation completion conditions under triaxial stresses.A simple calculation method was proposed to quantitatively analyze the fracture surface area and roughness in macro-level based on three-dimensional(3D)scanning data.In micro-level,scanning electron micrograph(SEM)was used to analyze the features of fracture surface.The results showed that the surface area of the induced fracture increases with perforation angle for both SC-CO_(2)and water fracturing,and the surface area of SC-CO_(2)-induced fracture is 6.49%e58.57%larger than that of water-induced fracture.The fractal dimension and surface roughness of water-induced fractures increase with the increase in perforation angle,while those of SC-CO_(2)-induced fractures decrease with the increasing perforation angle.A considerable number of microcracks and particle peeling pits can be observed on SC-CO_(2)-induced fracture surface while there are more flat particle surfaces in water-induced fracture surface through SEM images,indicating that fractures tend to propagate along the boundary of the particle for SC-CO_(2)fracturing while water-induced fractures prefer to cut through particles.These findings are of great significance for analyzing fracture mechanism and evaluating fracturing stimulation performance.展开更多
基金This research was in part supported by The National Key R&D Program of China(2018YFC0807803)The National Natural Science Foundation of China(41402143,50490271,and 40672104)+1 种基金Joint Fund of Coal(U1261203)Science and Technology Major Project from Shanxi Province(MQ2015-02).
文摘A quantitative analysis of the porosity,pore size distribution,and fractal dimensions of pores is significant for studying the pore structure characteristics of coal.This study utilized 12 anthracite coal samples from the Sihe mining area to explore the pore structure characteristics of the coal therein.Hundred randomly selected points on each sliced coal sample were imaged via scanning electron microscopy,and a total of 1200 images were used for the analysis.The porosity and fractal dimensions of the coal samples were analyzed via digital image processing and box-counting dimension methods.This method is characterized by extensive graphical analysis,and the results are based on statistical methods.These were also used to analyze the structural and development characteristics of the microscopic pores in the coal.The results reveal that the surface porosity obtained via digital image processing was 16.11%lower than that measured experimentally.The fractal dimension and porosity of the pore surface were fitted to a natural logarithmic curve.The rate of change in the pore fractal dimension depends on the porosity such that,to some degree,a greater porosity is associated with more complex pore structures,a higher degree of micropore development,and improved pore connectivity.
基金Funded by the Key Project of Science and Technology Research in Higher Educational Institutions of Inner Mongolia Autonomous Region (No.NJZZ22518)Inner Mongolia Natural Science Foundation Project (No.2022MS05043)Inner Mongolia Autonomous Region Water Conservancy Research Special Project(No.NSK2016-S11)。
文摘After exposure to freeze-thaw cycles, scanning electron microscopy(SEM) and nuclear magnetic resonance(NMR) were used to test the four mixtures. The microstructure is qualitatively analyzed from the 2D SEM image and the 3D pore distribution curve before and after freezing and thawing. The fractal dimension is utilized to characterize the two-dimensional topography image and the three-dimensional pore distribution, quantitatively. The results reveal that the surface porosity and volume porosity increase as the freeze-thaw action increases. Self-similarity characteristics exist in micro-damage inside the concrete. In the fractal dimension, it is possible to characterize pore evolution quantitatively. The fractal dimension correlates with pore damage evolution. The fractal dimension effectively quantitatively characterizes micro-damage features at various scales from the local to the global level.
基金National Natural Science Foundation of China(Grant No.51804318)the China Postdoctoral Science Foundation Founded Project(Grant No.2019M650963)National Key Basic Research and Development Program of China(Grant No.2014CB239203).
文摘Morphology of hydraulic fracture surface has significant effects on oil and gas flow,proppant migration and fracture closure,which plays an important role in oil and gas fracturing stimulation.In this paper,we analyzed the fracture surface characteristics induced by supercritical carbon dioxide(SC-CO_(2))and water in open-hole and perforation completion conditions under triaxial stresses.A simple calculation method was proposed to quantitatively analyze the fracture surface area and roughness in macro-level based on three-dimensional(3D)scanning data.In micro-level,scanning electron micrograph(SEM)was used to analyze the features of fracture surface.The results showed that the surface area of the induced fracture increases with perforation angle for both SC-CO_(2)and water fracturing,and the surface area of SC-CO_(2)-induced fracture is 6.49%e58.57%larger than that of water-induced fracture.The fractal dimension and surface roughness of water-induced fractures increase with the increase in perforation angle,while those of SC-CO_(2)-induced fractures decrease with the increasing perforation angle.A considerable number of microcracks and particle peeling pits can be observed on SC-CO_(2)-induced fracture surface while there are more flat particle surfaces in water-induced fracture surface through SEM images,indicating that fractures tend to propagate along the boundary of the particle for SC-CO_(2)fracturing while water-induced fractures prefer to cut through particles.These findings are of great significance for analyzing fracture mechanism and evaluating fracturing stimulation performance.
