The crystal structure of the title compound（C24H24N2O5, Mr = 420.45） has been determined by single-crystal X-ray diffraction. The crystal is of triclinic, space group P1 with a = 8.991（1）, b = 11.166（1）, c = 11....The crystal structure of the title compound（C24H24N2O5, Mr = 420.45） has been determined by single-crystal X-ray diffraction. The crystal is of triclinic, space group P1 with a = 8.991（1）, b = 11.166（1）, c = 11.169（1） , α = 91.413（2）, β = 105.887（2）, γ = 90.992（2）°, V = 1077.8（2） 3, Z = 2, Dc = 1.296 g/cm^3, F（000） = 444, μ（MoKα） = 0.091 mm^-1, the final R = 0.0466 and wR = 0.1507 for 4185 observed reflections（I 〉 2σ（I））. The single-crystal X-ray diffraction data indicated intermolecular C（17）–H（17）O（4）, C（5）–H（5）… O（4） hydrogen bonds and C–H…π interaction in the structure.展开更多
基金Supported by the National Natural Science Foundation of China(No.21342004)the Syngenta PhD(postgraduate student)Programme
文摘The crystal structure of the title compound（C24H24N2O5, Mr = 420.45） has been determined by single-crystal X-ray diffraction. The crystal is of triclinic, space group P1 with a = 8.991（1）, b = 11.166（1）, c = 11.169（1） , α = 91.413（2）, β = 105.887（2）, γ = 90.992（2）°, V = 1077.8（2） 3, Z = 2, Dc = 1.296 g/cm^3, F（000） = 444, μ（MoKα） = 0.091 mm^-1, the final R = 0.0466 and wR = 0.1507 for 4185 observed reflections（I 〉 2σ（I））. The single-crystal X-ray diffraction data indicated intermolecular C（17）–H（17）O（4）, C（5）–H（5）… O（4） hydrogen bonds and C–H…π interaction in the structure.
