This study aimed to show that the physicochemical proprieties obtained by Fourier transform infrared spectroscopy （FTIR）, thermogravimetry （TG）, and scanning electronic microscopy （SEM） can be useful tools for e...This study aimed to show that the physicochemical proprieties obtained by Fourier transform infrared spectroscopy （FTIR）, thermogravimetry （TG）, and scanning electronic microscopy （SEM） can be useful tools for evaluating the quality of active pharmaceutical ingredients （APIs） and pharmaceutical products. In addition, a simple, sensitive, and efficient method employing HPLC-DAD was developed for simulta- neous determination of lidocaine （LID）, ciprofloxacin （CFX） and enrofloxacin （EFX） in raw materials and in veterinary pharmaceutical formulations. Compounds were separated using a Gemini Cm （250 mm×4.6 mm, 5μm） Phenomenex column, at a temperature of 25℃, with a mobile phase containing 10 mM of phosphoric acid （pH 3.29）： acetonitrile （85.7：14.3, v/v） and a flow rate of 1.5 mL/min. Physicochemical characterization by TG, FTIR, and SEM of raw materials of LID, CFX, and EFX provided information useful for the evaluation, differentiation, and qualification of raw materials. Finally, the HPLC method was proved to be useful for evaluation of raw material and finished products, besides satisfying the need for an analytical method that allows simultaneous determination of EFX, CFX, and LID, which can also be extended to other matrices and applications.展开更多
The main material of concrete is a construction building material composed of water and mineral mixture and cement and chemical additives in the corresponding proportion and below the standard.In the process of making...The main material of concrete is a construction building material composed of water and mineral mixture and cement and chemical additives in the corresponding proportion and below the standard.In the process of making concrete material,slurry and cement are needed to mix,then cement slurry and sand are mixed into mortar according to the corresponding proportion,and aggregate is added to mortar to form concrete building material.In the process of concrete preparation,the most important construction link is mixing,which needs to be fully stirred to make the performance of concrete meet the construction needs.In the process of concrete construction technology development,both mix ratio and production technology have become more and more mature,but there are still some problems,which have an impact on the quality of concrete[1].Therefore,this paper discusses the quality control of concrete raw materials according to the construction process of road and bridge.展开更多
The present situation of cosmetic raw materials has been introduced,mainly including the measures of risk analysis and quality control for cosmetic raw materials.Through the inspection of cosmetic raw materials,the fo...The present situation of cosmetic raw materials has been introduced,mainly including the measures of risk analysis and quality control for cosmetic raw materials.Through the inspection of cosmetic raw materials,the formulation design and development,and the incoming management,the departments in the enterprise have worked together to achieve the risk analysis and quality control of cosmetic raw materials,to ensure the quality and safety of cosmetics.展开更多
基金the Brazilian agencies CNPq(Conselho Nacional de Desenvolvimento Científico e Tecnológico)CAPES(Coordenacao de Aperfeicoamento de Pessoal de Nível Superior)+3 种基金FAPES(Fundacao de AmparoàPesquisa e Inovacao do Espírito Santo)FAPEMIG(Fundacao de AmparoàPesquisa do Estado de Minas Gerais)for financial supporta collaborative research project with members of Rede Mineira de Química(RQ-MG)supported by FAPEMIG(Project:REDE-113/10Project:CEX-RED-0010–14)
文摘This study aimed to show that the physicochemical proprieties obtained by Fourier transform infrared spectroscopy （FTIR）, thermogravimetry （TG）, and scanning electronic microscopy （SEM） can be useful tools for evaluating the quality of active pharmaceutical ingredients （APIs） and pharmaceutical products. In addition, a simple, sensitive, and efficient method employing HPLC-DAD was developed for simulta- neous determination of lidocaine （LID）, ciprofloxacin （CFX） and enrofloxacin （EFX） in raw materials and in veterinary pharmaceutical formulations. Compounds were separated using a Gemini Cm （250 mm×4.6 mm, 5μm） Phenomenex column, at a temperature of 25℃, with a mobile phase containing 10 mM of phosphoric acid （pH 3.29）： acetonitrile （85.7：14.3, v/v） and a flow rate of 1.5 mL/min. Physicochemical characterization by TG, FTIR, and SEM of raw materials of LID, CFX, and EFX provided information useful for the evaluation, differentiation, and qualification of raw materials. Finally, the HPLC method was proved to be useful for evaluation of raw material and finished products, besides satisfying the need for an analytical method that allows simultaneous determination of EFX, CFX, and LID, which can also be extended to other matrices and applications.
文摘The main material of concrete is a construction building material composed of water and mineral mixture and cement and chemical additives in the corresponding proportion and below the standard.In the process of making concrete material,slurry and cement are needed to mix,then cement slurry and sand are mixed into mortar according to the corresponding proportion,and aggregate is added to mortar to form concrete building material.In the process of concrete preparation,the most important construction link is mixing,which needs to be fully stirred to make the performance of concrete meet the construction needs.In the process of concrete construction technology development,both mix ratio and production technology have become more and more mature,but there are still some problems,which have an impact on the quality of concrete[1].Therefore,this paper discusses the quality control of concrete raw materials according to the construction process of road and bridge.
文摘The present situation of cosmetic raw materials has been introduced,mainly including the measures of risk analysis and quality control for cosmetic raw materials.Through the inspection of cosmetic raw materials,the formulation design and development,and the incoming management,the departments in the enterprise have worked together to achieve the risk analysis and quality control of cosmetic raw materials,to ensure the quality and safety of cosmetics.
