Comparing with ordinary ploycrystalline materials sized to μm grade,the slip morphology of the coarse grained polycrystalline pure Al is characterized by:(1)several slip domains occur in a grain,and in same domain,se...Comparing with ordinary ploycrystalline materials sized to μm grade,the slip morphology of the coarse grained polycrystalline pure Al is characterized by:(1)several slip domains occur in a grain,and in same domain,several slip systems operate at same time or one after another intensely,a beautiful and neat slip pattern is forming on the specimen surface;(2)for high Σ-value coincident and random grain boundaries,the grain boundary affecting zone (GBAZ),bout 50—120μm wide,is favourable site to form intergranular crack at early fa- tigue life easily,and migration or slide of the boundaries were often observed.While low Σ-value near-coincident grain boundaries show a higher degree of slip continuity and strain compatibility than high Σ-value ones.Intergranular crack is not easily nucleated at low Σ-value near-coincident boundaries;and(3)due to suppression of grain boundary slip at triple grain boundary node,the high Σ-value and random grain boundary among the three boundaries of tricrystal crack easily during cyclic deformation.展开更多
It is important to inhibit the precipitation of η phases in precipitation strengthened Fe-Ni based alloys,as they will deteriorate not only the mechanical property but also the hydrogen resistance.The present investi...It is important to inhibit the precipitation of η phases in precipitation strengthened Fe-Ni based alloys,as they will deteriorate not only the mechanical property but also the hydrogen resistance.The present investigation shows that grain boundary engineering(GBE) can retard the formation and growth of ηphase in J75 alloy.After GBE treatment with 5% cold rolling followed by annealing at 1000℃ for 1 h,the fraction of special boundaries(SBs) increases from 38.4% in conventional alloy to 77.2% and the fraction of special triple junctions increases from 10% to 74%.During 800℃ aging treatment,quite amount of cellular η phases adjacent to random grain boundary(RGB) will be found in conventional alloy,and only a few small η phases have been observed in GBE treatment alloy subjected to the same aging treatment for long time.The reason for GBE in inhibiting precipitation of η phase can be attributed to not only introducing high fraction of SBs but also breaking the connectivity of RGB networks.As nucleation and growth of η phases on SBs are difficult due to their lower Ti concentration and diffusion rate,and the disruption of RGB networks reduces supply of Ti atoms to the η phases significantly,which impedes their growth at RGB.展开更多
文摘Comparing with ordinary ploycrystalline materials sized to μm grade,the slip morphology of the coarse grained polycrystalline pure Al is characterized by:(1)several slip domains occur in a grain,and in same domain,several slip systems operate at same time or one after another intensely,a beautiful and neat slip pattern is forming on the specimen surface;(2)for high Σ-value coincident and random grain boundaries,the grain boundary affecting zone (GBAZ),bout 50—120μm wide,is favourable site to form intergranular crack at early fa- tigue life easily,and migration or slide of the boundaries were often observed.While low Σ-value near-coincident grain boundaries show a higher degree of slip continuity and strain compatibility than high Σ-value ones.Intergranular crack is not easily nucleated at low Σ-value near-coincident boundaries;and(3)due to suppression of grain boundary slip at triple grain boundary node,the high Σ-value and random grain boundary among the three boundaries of tricrystal crack easily during cyclic deformation.
基金supported by the National Natural Science Foundation of China and China Academy of Engineering Physics[No.U1730140]National Key Research and Development Program of China[Grant No.2019YFB1505201]。
文摘It is important to inhibit the precipitation of η phases in precipitation strengthened Fe-Ni based alloys,as they will deteriorate not only the mechanical property but also the hydrogen resistance.The present investigation shows that grain boundary engineering(GBE) can retard the formation and growth of ηphase in J75 alloy.After GBE treatment with 5% cold rolling followed by annealing at 1000℃ for 1 h,the fraction of special boundaries(SBs) increases from 38.4% in conventional alloy to 77.2% and the fraction of special triple junctions increases from 10% to 74%.During 800℃ aging treatment,quite amount of cellular η phases adjacent to random grain boundary(RGB) will be found in conventional alloy,and only a few small η phases have been observed in GBE treatment alloy subjected to the same aging treatment for long time.The reason for GBE in inhibiting precipitation of η phase can be attributed to not only introducing high fraction of SBs but also breaking the connectivity of RGB networks.As nucleation and growth of η phases on SBs are difficult due to their lower Ti concentration and diffusion rate,and the disruption of RGB networks reduces supply of Ti atoms to the η phases significantly,which impedes their growth at RGB.
