Aluminum killed cold rolled steel used for automobiles was welded in this paper by using CO 2 laser with wavelength 10.6μm.The experiment shows that high quality of welding can be realized at welding speed of 4 500m...Aluminum killed cold rolled steel used for automobiles was welded in this paper by using CO 2 laser with wavelength 10.6μm.The experiment shows that high quality of welding can be realized at welding speed of 4 500mm/min by optimizing the parameters.The strength and hardness of laser welded joints for aluminum killed cold rolled steel increased compared to those of the base metal while the formability decreased.Forming limit diagram of joint material indicated that the laser weld seam should avoid the maximum deformation area of automobile parts during the designing period for the position of weld seam.展开更多
The influence of oxide scales on the corrosion behaviors of B510 L hot-rolled steel strips was investigated in this study. Focused ion beams and scanning electron microscopy were used to observe the morphologies of ox...The influence of oxide scales on the corrosion behaviors of B510 L hot-rolled steel strips was investigated in this study. Focused ion beams and scanning electron microscopy were used to observe the morphologies of oxide scales on the surface and cross sections of the hot-rolled steel. Raman spectroscopy and X-ray diffraction were used for the phase analysis of the oxide scales and corrosion products. The corrosion potential and impedance were measured by anodic polarization and electrochemical impedance spectroscopy. According to the results, oxide scales on the hot-rolled strips mainly comprise iron and iron oxides. The correlation between mass gain and test time follows a power exponential rule in the damp-heat test. The corrosion products are found to be mainly composed of γ-Fe OOH, Fe3O4, ?-Fe OOH, and γ-Fe2O3. The contents of the corrosion products are different on the surfaces of the steels with and without oxide scales. The steel with oxide scales is found to show a higher corrosion resistance and lower corrosion rate.展开更多
This study researches cold rolled ultra high strength martensitic steel processed by water quenching. It is found that both the quenching and overageing temperatures greatly influence the mechanical properties of mart...This study researches cold rolled ultra high strength martensitic steel processed by water quenching. It is found that both the quenching and overageing temperatures greatly influence the mechanical properties of martensitic steel. A tensile strength of 1500 MPa can be obtained from 0.2% C-1.8% Mn steel by soaking at 840℃,quenching at 700℃ and overageing at 200℃ for several minutes. The continuous cooling transformation (CCT) diagram reveals that full martensite can be obtained at a cooling rate of 100℃/s or higher; and at a cooling rate of 3 - 10℃/s,austenite barely decomposes at 700℃. For steel with 0.2% carbon and less manganese, austenite decomposition occurs before it is cooled to 700℃ at a cooling rate of 3 - 10℃/s, which leads to lower tensile strength. It is possible to reduce the manganese content of the 1500 MPa martensitic steel by increasing the quenching temperature. To increase the quenching temperature,the control of flatness during water quenching becomes a major concern.展开更多
Influence of hot deformation and subsequent austempering on the mechanical properties of hot rolled multiphase steel was investigated. Thermo-mechanical control processing (TMCP) was conducted by using a laboratory ...Influence of hot deformation and subsequent austempering on the mechanical properties of hot rolled multiphase steel was investigated. Thermo-mechanical control processing (TMCP) was conducted by using a laboratory hot rolling mill, where three different kinds of finishing rolling reduction, and austemperings with various isothermal holding duration were applied. The results have shown that a multiphase microstructure consisting of polygonal ferrite, granular bainite and larger amount of stabilized retained austenite can be obtained by controlled rolling processes. Mechanical properties increase with increasing the amount of deformation because of the stabilization of retained austenite. Ultimate tensile strength (σb), total elongation (σ) and the product of ultimate tensile strength and total elongation (σb-σ) reach the maximum values (791 MPa, 36% and 28476 MPa%, respectively) at optimal processes.展开更多
Effect of austempering on the transformation induced plasticity (TRIP) of hot rolled multiphase steel was investigated. Polygonal ferrite, granular bainite, and a large amount of stabilized retained austenite could ...Effect of austempering on the transformation induced plasticity (TRIP) of hot rolled multiphase steel was investigated. Polygonal ferrite, granular bainite, and a large amount of stabilized retained austenite could be obtained in the hot rolled multiphase steel. Strain induced martensite transformation (SIMT) of retained austenite and TRIP effectively occur under straining owing to austempering after hot rolling, and mechanical properties of the present steel remain at a relatively high constant value for austempering at 400℃. The mechanical properties of the steel exhibited a good combination of tensile strength (791MPa) and total elongation (36%) because the stability of retained austenite is optimal when the steel is held for 20min.展开更多
Effects of finishing rolling temperatures and reduction on the mechanical properties of hot rolled multiphase steel were investigated. Thermo-mechanical control processing (TMCP) was conducted by using a laboratory ho...Effects of finishing rolling temperatures and reduction on the mechanical properties of hot rolled multiphase steel were investigated. Thermo-mechanical control processing (TMCP) was conducted by using a laboratory hot rolling mill, in which three different kinds of finishing rolling temperatures and reduction and various austempering times were applied. The results showed that polygonal ferrite, granular bainite and larger amount of stabilized retained austenite can be obtained by controlled rolling processes, and that the strain-induced transformation to martensite from the retained austenite can occur gradually when the steel is deformed during tensile test. Mechanical properties increase with decreasing finishing rolling temperature and increasing amount of deformation. The most TRIP (transformation induced plasticity) effect, and ultimate tensile strength (UTS), total elongation (TEL) and the product of ultimate tensile strength and total elongation (UTS×TEL) are obtained at 20 min.展开更多
TWIP steels with 70% cold-rolled reduction were heated at 500, 600, 700, 800, 900, 1000, and 1100 ℃. Then, the properties before and after heating were examined through tensile and hardness experiments. The microstru...TWIP steels with 70% cold-rolled reduction were heated at 500, 600, 700, 800, 900, 1000, and 1100 ℃. Then, the properties before and after heating were examined through tensile and hardness experiments. The microstructures were also analyzed by optical microscopy and transmission electron microscopy. The relationship between the properties and microstructure was examined as well. Finally, the evolution process of cold-rolled microstructures during heating was discussed in detail. Moreover, some conclusions can be drawn, and the heating evolution characteristics are described.展开更多
Influence of hot rolling conditions on the mechanical properties of hot rolled TRIP steel was investigated. Thermomechanical control processing (TMCP) was conducted by using a laboratory hot rolling mill, in which t...Influence of hot rolling conditions on the mechanical properties of hot rolled TRIP steel was investigated. Thermomechanical control processing (TMCP) was conducted by using a laboratory hot rolling mill, in which three different kinds of finish rolling temperatures were applied. The results show that polygonal ferrite, granular bainite and larger amount of stabilized retained austenite can be obtained by controlled rolling processes. The finer ferrite grain size is produced through the deformation induced transformation during deformation rather than after deformation, which affects the mechanical properties of hot rolled TRIP steel. Mechanical properties increase with decreasing finish rolling temperature due to the stabilization of retained austenite. Ultimate tensile strength (UTS), total elongation (TEL) and the product of ultimate tensile strength and total elongation (UTS×TEL) reaches optimal values (791 MPa, 36% and 28 476 MPa%, respectively) when the specimen was hot rolled for 50% reduction at finish rolling temperature of 700 ℃.展开更多
The influence of rare earth (RE) elements on the solidification process and eutectic transformation and mechanical properties of the high-V type cast, high-speed steel roll was studied. Test materials with different...The influence of rare earth (RE) elements on the solidification process and eutectic transformation and mechanical properties of the high-V type cast, high-speed steel roll was studied. Test materials with different RE additions were prepared on a horizontal centrifugal casting machine. The solidification process, eutectic structure transformation, carbide morphology, and the elements present, were all investigated by means of differential scanning calorimetry (DSC) and scanning electron microscopy energy dispersive spectrometry (SEM-EDS). The energy produced by crack initiation and crack extension was analyzed using a digital impact test machine. It was found that rare earth elements increased the tensile strength of the steel by inducing crystallization of earlier eutectic γ-Fe during the solidification process, which in turn increased the solidification temperature and thinned the dendritic grains. Rare earth elements with large atomic radius changed the lattice parameters of the MC carbide by forming rare earth carbides. This had the effect of dispersing longpole M C carbides to provide carbide grains, thereby, reducing the formation of the gross carbide and making more V available, to increase the secondary hardening process and improve the hardness level. The presence of rare earth elements in the steel raised the impact toughness by changing the mechanism of MC carbide formation, thereby increasing the crack initiation energy.展开更多
Core filling process of cast high speed steel roll was simulated.Ductile iron was used as core material.The influences of filling parameters,such as core filling time and core filling temperature,on the filling proces...Core filling process of cast high speed steel roll was simulated.Ductile iron was used as core material.The influences of filling parameters,such as core filling time and core filling temperature,on the filling process were investigated.Based on the simulated results,optimal core filling parameters were determined.The predicted temperature fields show that the temperature at the roll shoulder is the lowest during the core filling process and usually causes binding defects there.Method for solving this problem was presented.展开更多
A high speed steel composite roll billet was fabricated, which is regular in shape, smooth in surface, slight in trace, compact in internal structure, free of slag inclusion, shrinkage cavity, cracks and other flaws, ...A high speed steel composite roll billet was fabricated, which is regular in shape, smooth in surface, slight in trace, compact in internal structure, free of slag inclusion, shrinkage cavity, cracks and other flaws, and good in macro quality of junction surface using a vertical continuous casting machine. The interface zone microstructure of bimetallic in billet of high speed steel composite roll was analyzed by metallurgical microscope(OM), X-ray diffractmeter(XRD), scanning electron microscopy(SEM) and energy-dispersive X-ray analysis(EDS). The results indicate that the microstructure of roll billet is composed of chilled solidified layer, dendrite zone, interfacial zone of bimetal and core material zone. The microstructure of outer shell material is composed of martensite + bainite + residual austenite + some small labyrinth-shape, small-short lath-shape, or dollop-shape eutectic carbides. The microstructure of core material is slice-shape pearlite and a little ferrite along boundary of cells. The interface region microstructure of bimetallic composite roll consists of diffusion region, chilled solidified layer and columnar grain region.展开更多
The critical points and time-temperature-transformation(TTT)curves of the isothermal transformation diagrams for a high-speed steel casting on a horizontal centrifugal casting machine had been determined experimentall...The critical points and time-temperature-transformation(TTT)curves of the isothermal transformation diagrams for a high-speed steel casting on a horizontal centrifugal casting machine had been determined experimentally in the study.The effects of quenching temperature on the microstructures and properties of centrifugal casting high speed steel(HSS)roll has been investigated using scanning electron microscopy(SEM), light optical microscopy(LOM)and X-ray diffraction(XRD)as well as using tensile,impact,and hardness tests. The results show that the HSS roll has excellent hardenability and its matrix structure can be transformed into the martensite after being quenched in the sodium silicate solution.The retained austenite in the quenching structure increases and the hardness decreases when the quenching temperature exceeds 1,040℃.The tensile strength and impact toughness of HSS roll increase once the quenching temperature is raised from 980℃to 1,040℃. However,the tensile strength and impact toughness have no significant change when the quenching temperature exceeds 1,040℃.The HSS roll quenched at 1,040℃exhibits excellent comprehensive mechanical properties.展开更多
In ferritic stainless steels, a significant non-uniform recrystallization orientation and a substantial texture gradient usually occur, which can degrade the ridging resistance of the final sheets. To improve the homo...In ferritic stainless steels, a significant non-uniform recrystallization orientation and a substantial texture gradient usually occur, which can degrade the ridging resistance of the final sheets. To improve the homogeneity of the recrystallization orientation and reduce the texture gradient in ultra-purified 17%Cr ferritic stainless steel, in this work, we performed conventional and asymmetric rolling processes and conducted macro and micro-texture analyses to investigate texture evolution under different cold-rolling conditions. In the conventional rolling specimens, we observed that the deformation was not uniform in the thickness direction, whereas there was homogeneous shear deformation in the asymmetric rolling specimens as well as the formation of uniform recrystallized grains and random orientation grains in the final annealing sheets. As such, the ridging resistance of the final sheets was significantly improved by employing the asymmetric rolling process. This result indicates with certainty that the texture gradient and orientation inhomogeneity can be attributed to non-uniform deformation, whereas the uniform orientation gradient in the thickness direction is explained by the increased number of shear bands obtained in the asymmetric rolling process.展开更多
A new kind of corrosion resistant steelfor cargo oiltanks(COT)was developed.The influences of finalrolling temperature,cooling rate,and finalcooling temperature on microstructure were investigated.The proper rolling...A new kind of corrosion resistant steelfor cargo oiltanks(COT)was developed.The influences of finalrolling temperature,cooling rate,and finalcooling temperature on microstructure were investigated.The proper rolling process parameters were obtained through multi-pass thermalsimulation test.The finalrolling temperature is about 820 ℃,the finalcooling temperature is about 600 ℃,and the cooling rate should be controlled between 10 ℃/s and 20 ℃/s.Based on the above analysis of the results,three groups of rolling samples by thermo mechanicalcontrolprocess are prepared.The tensile strength,yield strength,and toughness of the corrosion resistant steelare measured,which meet the requirements of DH36 steel,it can instruct the actualrolling production.The corrosion behaviour is also researched by weight loss and electrochemicalimpedance spectroscopic method,and it is found that the steelhas good corrosion resistance performance,the best one is No.3 steel,the corrosion rate of which is about 1/4 of the accepted criterion.展开更多
Novel water-based nanolubricants using TiO2 nanoparticles(NPs)were synthesised by adding sodium dodecyl benzene sulfonate(SDBS)and glycerol,which exhibited excellent dispersion stability and wettability.The tribologic...Novel water-based nanolubricants using TiO2 nanoparticles(NPs)were synthesised by adding sodium dodecyl benzene sulfonate(SDBS)and glycerol,which exhibited excellent dispersion stability and wettability.The tribological performance of the synthesised nanolubricants was investigated using an Rtec ball-on-disk tribometer,and their application in hot steel rolling was evaluated on a 2-high Hille 100 experimental rolling mill,in comparison to those without SDBS.The water-based nanolubricant containing 4 wt%TiO2 and 0.4 wt%SDBS demonstrated superior tribological performance by decreasing coefficient of friction and ball wear up to 70.5%and 84.3%,respectively,compared to those of pure water.In addition to the lubrication effect,the suspensions also had significant effect on polishing of the work roll surface.The resultant surface improvement thus enabled the decrease in rolling force up to 8.3%under a workpiece reduction of 30%at a rolling temperature of 850◦C.The lubrication mechanisms were primarily ascribed to the formation of lubricating film and ball-bearing effect of the TiO2 NPs.展开更多
The tensile strength and ductility of a high nitrogen nickel-free austenitic stainless steel with solution and cold rolling treatment were investigated by performing tensile tests at different strain rates and at room...The tensile strength and ductility of a high nitrogen nickel-free austenitic stainless steel with solution and cold rolling treatment were investigated by performing tensile tests at different strain rates and at room temperature. The tensile tests demonstrated that this steel exhibits a significant strain rate and cold rolling dependence of the tensile strength and ductility.With the increase of the strain rate from 10^-4s^-1to 1 s^-1, the yield strength and ultimate tensile strength increase and the uniform elongation and total elongation decrease. The analysis of the double logarithmic stress–strain curves showed that this steel exhibits a two-stage strain hardening behavior, which can be well examined and analyzed by using the Ludwigson equation. The strain hardening exponents at low and high strain regions(n2and n1) and the transition strain(εL) decrease with increasing strain rate and the increase of cold rolling RA. Based on the analysis results of the stress–strain curves, the transmission electron microscopy characterization of the microstructure and the scanning electron microscopy observation of the deformation surfaces, the significant strain rate and cold rolling dependence of the strength and ductility of this steel were discussed and connected with the variation in the work hardening and dislocation activity with strain rate and cold rolling.展开更多
Commercial grain oriented silicon steel was cold rolled to thickness from 0.06 to 0.10 mm by cross shear rolling, then annealed in vacuum or a hydrogen atmosphere furnace. Deformation textures of the sheets were resea...Commercial grain oriented silicon steel was cold rolled to thickness from 0.06 to 0.10 mm by cross shear rolling, then annealed in vacuum or a hydrogen atmosphere furnace. Deformation textures of the sheets were researched by ODF method and reverse pole figure quantitative analyses. The results indicate that: in the condition of the cross shear rolling, the deformation texture of rolled sheet is generally similar to that of conventional rolled sheet, however, the texture distribution through the thickness is asymmetrical. With mismatch speed ratio increasing, the amount of Goss texture increases. With reduction ratio increasing, the intensity of γ-fiber becomes strong.展开更多
This paper reviews recent developments in the contin- uous processing of steels in Japan.The following items are discussed:continuous casting-direct rolling(CC-DR) process of hot-rolled strip:thermomechanical control ...This paper reviews recent developments in the contin- uous processing of steels in Japan.The following items are discussed:continuous casting-direct rolling(CC-DR) process of hot-rolled strip:thermomechanical control process(TMCP)of heavy plates:in—line heat treating pro- cess of rails:direct lead patenting(DLP)process of wire rods;and fully integrated processing line(FIPL)of cold-rolled strip.展开更多
1 Scope This standard specifies the classification, technical requirements, test methods, quality appraisal procedures, packing, marking, transportation, storage and quality certificate of castables for steel rolling...1 Scope This standard specifies the classification, technical requirements, test methods, quality appraisal procedures, packing, marking, transportation, storage and quality certificate of castables for steel rolling reheating furnace.展开更多
The program to predict the microstructure evolutions during hot strip rolling of C-M n steels has been developed in this paper, BV using this program, the microstructure changes with the processing parameters were ana...The program to predict the microstructure evolutions during hot strip rolling of C-M n steels has been developed in this paper, BV using this program, the microstructure changes with the processing parameters were analysed in detail. showing not only a good agreement of prediction with the measured values, but also entirely possibility to optimize hot strip rolling precess by computer simulation展开更多
文摘Aluminum killed cold rolled steel used for automobiles was welded in this paper by using CO 2 laser with wavelength 10.6μm.The experiment shows that high quality of welding can be realized at welding speed of 4 500mm/min by optimizing the parameters.The strength and hardness of laser welded joints for aluminum killed cold rolled steel increased compared to those of the base metal while the formability decreased.Forming limit diagram of joint material indicated that the laser weld seam should avoid the maximum deformation area of automobile parts during the designing period for the position of weld seam.
基金supported by the National Natural Science Foundation of China(No.51222106)the Fundamental Research Funds for the Central Universities(No.FRF-TP-14-011C1)+1 种基金the Major State Basic Research Development Program of China(No.2014CB643300)the Beijing Municipal Commission of Education
文摘The influence of oxide scales on the corrosion behaviors of B510 L hot-rolled steel strips was investigated in this study. Focused ion beams and scanning electron microscopy were used to observe the morphologies of oxide scales on the surface and cross sections of the hot-rolled steel. Raman spectroscopy and X-ray diffraction were used for the phase analysis of the oxide scales and corrosion products. The corrosion potential and impedance were measured by anodic polarization and electrochemical impedance spectroscopy. According to the results, oxide scales on the hot-rolled strips mainly comprise iron and iron oxides. The correlation between mass gain and test time follows a power exponential rule in the damp-heat test. The corrosion products are found to be mainly composed of γ-Fe OOH, Fe3O4, ?-Fe OOH, and γ-Fe2O3. The contents of the corrosion products are different on the surfaces of the steels with and without oxide scales. The steel with oxide scales is found to show a higher corrosion resistance and lower corrosion rate.
文摘This study researches cold rolled ultra high strength martensitic steel processed by water quenching. It is found that both the quenching and overageing temperatures greatly influence the mechanical properties of martensitic steel. A tensile strength of 1500 MPa can be obtained from 0.2% C-1.8% Mn steel by soaking at 840℃,quenching at 700℃ and overageing at 200℃ for several minutes. The continuous cooling transformation (CCT) diagram reveals that full martensite can be obtained at a cooling rate of 100℃/s or higher; and at a cooling rate of 3 - 10℃/s,austenite barely decomposes at 700℃. For steel with 0.2% carbon and less manganese, austenite decomposition occurs before it is cooled to 700℃ at a cooling rate of 3 - 10℃/s, which leads to lower tensile strength. It is possible to reduce the manganese content of the 1500 MPa martensitic steel by increasing the quenching temperature. To increase the quenching temperature,the control of flatness during water quenching becomes a major concern.
基金This work was supported by the National Natural Science Foundation of China(No.50334010)The author(Zhuang LI)also acknowledges the support of the Doctor Degree Thesis Subsidization Item of Northeastern University(No.200302).
文摘Influence of hot deformation and subsequent austempering on the mechanical properties of hot rolled multiphase steel was investigated. Thermo-mechanical control processing (TMCP) was conducted by using a laboratory hot rolling mill, where three different kinds of finishing rolling reduction, and austemperings with various isothermal holding duration were applied. The results have shown that a multiphase microstructure consisting of polygonal ferrite, granular bainite and larger amount of stabilized retained austenite can be obtained by controlled rolling processes. Mechanical properties increase with increasing the amount of deformation because of the stabilization of retained austenite. Ultimate tensile strength (σb), total elongation (σ) and the product of ultimate tensile strength and total elongation (σb-σ) reach the maximum values (791 MPa, 36% and 28476 MPa%, respectively) at optimal processes.
基金supported by the National Natural Science Foundation of China(No.50334010)the Doctor Degree Thesis Subsidization Item of Northeastern University(No.200302).
文摘Effect of austempering on the transformation induced plasticity (TRIP) of hot rolled multiphase steel was investigated. Polygonal ferrite, granular bainite, and a large amount of stabilized retained austenite could be obtained in the hot rolled multiphase steel. Strain induced martensite transformation (SIMT) of retained austenite and TRIP effectively occur under straining owing to austempering after hot rolling, and mechanical properties of the present steel remain at a relatively high constant value for austempering at 400℃. The mechanical properties of the steel exhibited a good combination of tensile strength (791MPa) and total elongation (36%) because the stability of retained austenite is optimal when the steel is held for 20min.
基金Project (No. 50334010) supported by the National Natural ScienceFoundation of China
文摘Effects of finishing rolling temperatures and reduction on the mechanical properties of hot rolled multiphase steel were investigated. Thermo-mechanical control processing (TMCP) was conducted by using a laboratory hot rolling mill, in which three different kinds of finishing rolling temperatures and reduction and various austempering times were applied. The results showed that polygonal ferrite, granular bainite and larger amount of stabilized retained austenite can be obtained by controlled rolling processes, and that the strain-induced transformation to martensite from the retained austenite can occur gradually when the steel is deformed during tensile test. Mechanical properties increase with decreasing finishing rolling temperature and increasing amount of deformation. The most TRIP (transformation induced plasticity) effect, and ultimate tensile strength (UTS), total elongation (TEL) and the product of ultimate tensile strength and total elongation (UTS×TEL) are obtained at 20 min.
基金Funded by the National Natural Science Foundation o f China(51201154)the Natural Science Foundation of Shanxi Province(2014011015-1)
文摘TWIP steels with 70% cold-rolled reduction were heated at 500, 600, 700, 800, 900, 1000, and 1100 ℃. Then, the properties before and after heating were examined through tensile and hardness experiments. The microstructures were also analyzed by optical microscopy and transmission electron microscopy. The relationship between the properties and microstructure was examined as well. Finally, the evolution process of cold-rolled microstructures during heating was discussed in detail. Moreover, some conclusions can be drawn, and the heating evolution characteristics are described.
基金the National Natural Science Foundation of China(No.50334010)the Program of Education Branch of Liaoning Province of China(No.2006B075)
文摘Influence of hot rolling conditions on the mechanical properties of hot rolled TRIP steel was investigated. Thermomechanical control processing (TMCP) was conducted by using a laboratory hot rolling mill, in which three different kinds of finish rolling temperatures were applied. The results show that polygonal ferrite, granular bainite and larger amount of stabilized retained austenite can be obtained by controlled rolling processes. The finer ferrite grain size is produced through the deformation induced transformation during deformation rather than after deformation, which affects the mechanical properties of hot rolled TRIP steel. Mechanical properties increase with decreasing finish rolling temperature due to the stabilization of retained austenite. Ultimate tensile strength (UTS), total elongation (TEL) and the product of ultimate tensile strength and total elongation (UTS×TEL) reaches optimal values (791 MPa, 36% and 28 476 MPa%, respectively) when the specimen was hot rolled for 50% reduction at finish rolling temperature of 700 ℃.
基金Project supported by"863"Project (2006AA03Z532)the National Natural Science Foundation of China (NSFC 50341050)
文摘The influence of rare earth (RE) elements on the solidification process and eutectic transformation and mechanical properties of the high-V type cast, high-speed steel roll was studied. Test materials with different RE additions were prepared on a horizontal centrifugal casting machine. The solidification process, eutectic structure transformation, carbide morphology, and the elements present, were all investigated by means of differential scanning calorimetry (DSC) and scanning electron microscopy energy dispersive spectrometry (SEM-EDS). The energy produced by crack initiation and crack extension was analyzed using a digital impact test machine. It was found that rare earth elements increased the tensile strength of the steel by inducing crystallization of earlier eutectic γ-Fe during the solidification process, which in turn increased the solidification temperature and thinned the dendritic grains. Rare earth elements with large atomic radius changed the lattice parameters of the MC carbide by forming rare earth carbides. This had the effect of dispersing longpole M C carbides to provide carbide grains, thereby, reducing the formation of the gross carbide and making more V available, to increase the secondary hardening process and improve the hardness level. The presence of rare earth elements in the steel raised the impact toughness by changing the mechanism of MC carbide formation, thereby increasing the crack initiation energy.
文摘Core filling process of cast high speed steel roll was simulated.Ductile iron was used as core material.The influences of filling parameters,such as core filling time and core filling temperature,on the filling process were investigated.Based on the simulated results,optimal core filling parameters were determined.The predicted temperature fields show that the temperature at the roll shoulder is the lowest during the core filling process and usually causes binding defects there.Method for solving this problem was presented.
基金Project(200809123) supported by the National Natural Science Foundation of China
文摘A high speed steel composite roll billet was fabricated, which is regular in shape, smooth in surface, slight in trace, compact in internal structure, free of slag inclusion, shrinkage cavity, cracks and other flaws, and good in macro quality of junction surface using a vertical continuous casting machine. The interface zone microstructure of bimetallic in billet of high speed steel composite roll was analyzed by metallurgical microscope(OM), X-ray diffractmeter(XRD), scanning electron microscopy(SEM) and energy-dispersive X-ray analysis(EDS). The results indicate that the microstructure of roll billet is composed of chilled solidified layer, dendrite zone, interfacial zone of bimetal and core material zone. The microstructure of outer shell material is composed of martensite + bainite + residual austenite + some small labyrinth-shape, small-short lath-shape, or dollop-shape eutectic carbides. The microstructure of core material is slice-shape pearlite and a little ferrite along boundary of cells. The interface region microstructure of bimetallic composite roll consists of diffusion region, chilled solidified layer and columnar grain region.
基金supported by the innovation fund of small and medium-sized enterprise of Science&Technology Ministry of China under grant(07C26215110842).
文摘The critical points and time-temperature-transformation(TTT)curves of the isothermal transformation diagrams for a high-speed steel casting on a horizontal centrifugal casting machine had been determined experimentally in the study.The effects of quenching temperature on the microstructures and properties of centrifugal casting high speed steel(HSS)roll has been investigated using scanning electron microscopy(SEM), light optical microscopy(LOM)and X-ray diffraction(XRD)as well as using tensile,impact,and hardness tests. The results show that the HSS roll has excellent hardenability and its matrix structure can be transformed into the martensite after being quenched in the sodium silicate solution.The retained austenite in the quenching structure increases and the hardness decreases when the quenching temperature exceeds 1,040℃.The tensile strength and impact toughness of HSS roll increase once the quenching temperature is raised from 980℃to 1,040℃. However,the tensile strength and impact toughness have no significant change when the quenching temperature exceeds 1,040℃.The HSS roll quenched at 1,040℃exhibits excellent comprehensive mechanical properties.
基金financially supported by the National Key R&D Program of China (2016YFB0300200)National Natural Science Foundation of China (Nos. U1660114 and 51174026)
文摘In ferritic stainless steels, a significant non-uniform recrystallization orientation and a substantial texture gradient usually occur, which can degrade the ridging resistance of the final sheets. To improve the homogeneity of the recrystallization orientation and reduce the texture gradient in ultra-purified 17%Cr ferritic stainless steel, in this work, we performed conventional and asymmetric rolling processes and conducted macro and micro-texture analyses to investigate texture evolution under different cold-rolling conditions. In the conventional rolling specimens, we observed that the deformation was not uniform in the thickness direction, whereas there was homogeneous shear deformation in the asymmetric rolling specimens as well as the formation of uniform recrystallized grains and random orientation grains in the final annealing sheets. As such, the ridging resistance of the final sheets was significantly improved by employing the asymmetric rolling process. This result indicates with certainty that the texture gradient and orientation inhomogeneity can be attributed to non-uniform deformation, whereas the uniform orientation gradient in the thickness direction is explained by the increased number of shear bands obtained in the asymmetric rolling process.
基金Funded by the National Key Technology Research and Development Program of the Ministry of Science and Technology of China during the“12th Five-Year Plan”(No.2011BAE25B03)
文摘A new kind of corrosion resistant steelfor cargo oiltanks(COT)was developed.The influences of finalrolling temperature,cooling rate,and finalcooling temperature on microstructure were investigated.The proper rolling process parameters were obtained through multi-pass thermalsimulation test.The finalrolling temperature is about 820 ℃,the finalcooling temperature is about 600 ℃,and the cooling rate should be controlled between 10 ℃/s and 20 ℃/s.Based on the above analysis of the results,three groups of rolling samples by thermo mechanicalcontrolprocess are prepared.The tensile strength,yield strength,and toughness of the corrosion resistant steelare measured,which meet the requirements of DH36 steel,it can instruct the actualrolling production.The corrosion behaviour is also researched by weight loss and electrochemicalimpedance spectroscopic method,and it is found that the steelhas good corrosion resistance performance,the best one is No.3 steel,the corrosion rate of which is about 1/4 of the accepted criterion.
基金The authors acknowledge the financial supports from Baosteel-Australia Joint Research&Development Center(BAJC)under the project of BA17004 and Australian Research Council(ARC)under Linkage Project Program(LP150100591)。
文摘Novel water-based nanolubricants using TiO2 nanoparticles(NPs)were synthesised by adding sodium dodecyl benzene sulfonate(SDBS)and glycerol,which exhibited excellent dispersion stability and wettability.The tribological performance of the synthesised nanolubricants was investigated using an Rtec ball-on-disk tribometer,and their application in hot steel rolling was evaluated on a 2-high Hille 100 experimental rolling mill,in comparison to those without SDBS.The water-based nanolubricant containing 4 wt%TiO2 and 0.4 wt%SDBS demonstrated superior tribological performance by decreasing coefficient of friction and ball wear up to 70.5%and 84.3%,respectively,compared to those of pure water.In addition to the lubrication effect,the suspensions also had significant effect on polishing of the work roll surface.The resultant surface improvement thus enabled the decrease in rolling force up to 8.3%under a workpiece reduction of 30%at a rolling temperature of 850◦C.The lubrication mechanisms were primarily ascribed to the formation of lubricating film and ball-bearing effect of the TiO2 NPs.
基金Project supported by the National Natural Science Foundations of China(Grant Nos.51371089 and 51401083)
文摘The tensile strength and ductility of a high nitrogen nickel-free austenitic stainless steel with solution and cold rolling treatment were investigated by performing tensile tests at different strain rates and at room temperature. The tensile tests demonstrated that this steel exhibits a significant strain rate and cold rolling dependence of the tensile strength and ductility.With the increase of the strain rate from 10^-4s^-1to 1 s^-1, the yield strength and ultimate tensile strength increase and the uniform elongation and total elongation decrease. The analysis of the double logarithmic stress–strain curves showed that this steel exhibits a two-stage strain hardening behavior, which can be well examined and analyzed by using the Ludwigson equation. The strain hardening exponents at low and high strain regions(n2and n1) and the transition strain(εL) decrease with increasing strain rate and the increase of cold rolling RA. Based on the analysis results of the stress–strain curves, the transmission electron microscopy characterization of the microstructure and the scanning electron microscopy observation of the deformation surfaces, the significant strain rate and cold rolling dependence of the strength and ductility of this steel were discussed and connected with the variation in the work hardening and dislocation activity with strain rate and cold rolling.
基金National Natural Science Foundation of China!(No. 59671037).
文摘Commercial grain oriented silicon steel was cold rolled to thickness from 0.06 to 0.10 mm by cross shear rolling, then annealed in vacuum or a hydrogen atmosphere furnace. Deformation textures of the sheets were researched by ODF method and reverse pole figure quantitative analyses. The results indicate that: in the condition of the cross shear rolling, the deformation texture of rolled sheet is generally similar to that of conventional rolled sheet, however, the texture distribution through the thickness is asymmetrical. With mismatch speed ratio increasing, the amount of Goss texture increases. With reduction ratio increasing, the intensity of γ-fiber becomes strong.
文摘This paper reviews recent developments in the contin- uous processing of steels in Japan.The following items are discussed:continuous casting-direct rolling(CC-DR) process of hot-rolled strip:thermomechanical control process(TMCP)of heavy plates:in—line heat treating pro- cess of rails:direct lead patenting(DLP)process of wire rods;and fully integrated processing line(FIPL)of cold-rolled strip.
文摘1 Scope This standard specifies the classification, technical requirements, test methods, quality appraisal procedures, packing, marking, transportation, storage and quality certificate of castables for steel rolling reheating furnace.
文摘The program to predict the microstructure evolutions during hot strip rolling of C-M n steels has been developed in this paper, BV using this program, the microstructure changes with the processing parameters were analysed in detail. showing not only a good agreement of prediction with the measured values, but also entirely possibility to optimize hot strip rolling precess by computer simulation