Effect of deformation mode,dynamic recrystallization and twinning on rolling texture evolution of AZ31 magnesium alloys

In order to obtain quantitative relationship between（0002） texture intensity and hot rolling conditions, conventional rolling experiments on AZ31 magnesium alloys were performed with 20%-40% reductions and temperatures within the range of 300-500 ℃. Shear strain and equivalent strain distributions along the thickness of the rolled sheets were calculated experimentally using embedded pin in a rolling sheet. Rolling microstructures and textures in the sheet surface and center layers of the AZ31 alloys were measured by optical microscopy（OM）, X-ray diffractometry（XRD） and electron back scatter diffraction（EBSD）. Effects of the rolling strain, dynamic recrystallization（DRX） and twinning on the texture evolution of the AZ31 alloys were investigated quantitatively. It is found that the highest（0002） basal texture intensities are obtained at a starting rolling temperature of 400 ℃ under the same strain. Strain–temperature dependency of the（0002） texture intensity of the AZ31 alloy is derived.

Correlation of morphological anisotropy and Lankford value of deep drawing sheets hot-rolled by compact strip production

Cold-rolled steel sheets in automotive applications require an excellent deep draw ability, which is characterized by the Lankford value （r-value）. In this study, a correlation was identified between r-value and pancake-shaped grain flatness which is indicated as the ratio of grain diameter in the rolling direction （RD） and normal direction （ND） of sheets （dr/dn）. A mathematical model （ r = e^0.345（dn^1/2-dr^1/2） ） was developed to calculate r-value by the microstructure of steel sheets hot-rolled by compact strip production （CSP）. It is shown that the r-value is higher, if the microstructure of steel sheet is of pancake-shaped grains elongated in the rolling direction. The calculated r-value is confirmed to fit exactly to the measured one from the large-scale production.

Development and future prospect of hot strip rolling technology at Baosteel

Since the 2050 mm hot strip mill was put into operation in 1989, Baosteel has made great achievements in increasing productivity, developing new process technologies and steel products and improving product quality. In the past 18 years from 1989 to 2007 ,Baosteel has constructed five hot strip mills with a total annual capacity of 19.8 Mt. Indices for technology standards, product categories and steel grades, product quality, both technically and economically, take the lead domestically or reached the world class level. As there are many hot strip mills that expected to be put into operation by the end of 2010 ,the overall annual capacity will exceed 30 Mt ,and the product will cover grain oriented （GO） Si steels and alloyed steels.

Effects of trace Gd concentration on texture and mechanical properties of hot-rolled Mg-2Zn-xGd sheets

The effects of Gd concentration(0.1,0.3,0.7 wt%)on the microstructure,texture and mechanical properties of rolled and annealed Mg-2Zn-xGd sheets have been investigated aiming to develop low cost and high ductile Mg-Zn-Gd sheets.Dynamic recrystallization,static recrystallization and grain growth during hot rolling process and annealing process were delayed with increase of Gd concentration,leading to fine grain microstructure.The rolled 0.1 wt%Gd sheet showed strong basal texture which remained stable after annealing process and exhibited medium elongation of about 25%.In contrast,the rolled 0.3 wt%Gd sheet had weak basal texture which transformed to non-basal texture with double peaks tilted about±48°to the transverse direction due to the static recrystallization during annealing process.Consequently,the annealed sheets exhibited higher elongation of 40%along the rolling direction and 50%along the transverse direction due to the existence of non-basal texture.It is suggested that the minimum effective concentration for texture randomization in the Mg-2Zn-xGd alloy is about 0.3 wt%.

Effect of hot rolling on microstructure and properties of the ZEK100 alloy

Attempts to expand manufacturing capabilities of magnesium-based sheet materials are described.The as-cast ZEK100(Mg-1.2Zn-0.35Zr-0.17Nd,in wt%)magnesium alloy was subjected to hot rolling at temperatures from 350℃to 450℃using the laboratory 50 ton reversible mill with preheated rolls to manufacture the 1.5-1.7 mm thick sheet.The rolling temperature affected the sheet properties and an increase in the rolling temperature from 250 to 450℃caused reduction of tensile strength from 257 to 228 MPa ac-companied by a reduction in tensile yield stress from 237 to 185 MPa.At the same time,the alloy elongation increased from 17 to 21%.For the same rolling temperature range,the compressive strength reduced from 418 to 351 MPa.The post-rolling annealing at 450℃led to reduction of both tensile and compressive properties with the largest changes corresponding to the rolling temperature of 350°C.The correlation between the alloy grain size after rolling and the sheet properties was established where a reduction in grain size was accompanied by an increase of both the tensile/compressive strength and yield stress.Based on Hall-Petch relationship and an average grain size the correlation developed in this study may be used as the prediction model for properties of the hot rolled magnesium sheet.The results are discussed in terms of recent developments in magnesium sheet alloys and the vital role played in this process by rare earth elements.

Effect of casting parameters and deformation on microstructure evolution of twin-roll casting magnesium alloy AZ31

Twin roll casting method is a promising route to directly produce magnesium alloy strip. It is a rapid solidification process with high temperature gradient combined with thermal flow and rolling deformation in the casting region. As-cast strip with proper microstructure is requested to serve as next rolling feedstock. However the microstructure of as-cast strip is sensitive for casting conditions during the casting process and the as-cast microstructure greatly affects the mechanical properties. In this work, the effect of casting speed, pouring temperature, deformation as well as anneal process on microstructure and mechanical properties were investigated. The results revels that twin-roll casting process can effectively refine the grain size, improve the morphology and distribution states of Mg17Al12. The homogenization treatment time can be shorted for the fine microstructure and lower the cost dramatically for the next forming process.

Production of 150 cm wide AZ31 magnesium sheet by twin roll casting

150 cm wide AZ31 magnesium alloy sheet was produced by twin roll casting.The sheets of 6 mm thickness were cast. The sheet material was characterized using various techniques including metallography and XRD.The mechanical properties were investigated by tensile tests and hardness measurements.The procedures were developed for thermomechanical treatment of cast sheet material.The products of these procedures were characterized and the results were discussed for possible potential applications.

Application of Anand's constitutive model on twin roll casting process of AZ31 magnesium alloy

Twin-roll thin strip casting process combines casting and hot rolling into a single process, in which thermal stress and thermal mechanical stress were involved. Considering the high temperature gradient, the existing of liquid and solid regions and rolling deformation, suitable constitutive model is the key to describe the process. Anand's model is a temperature-dependent, rate-dependent and unified of creep and plasticity model and the Jaumann derivative was employed in Anand's model which makes the constitutive model frame-indifferent or objective, therefore the highly nonlinearities behavior in the twin-roll casting process can be simulated. The parameters of the Anand's model were regressed based on the compression tests of AZ31 magnesium alloy. The simulation results reveal that the Anand's model can well describe the deformation characteristics of twin-roll casting process. Based on the simulation results, the form of evolution equations in Anand's model was discussed.

Consideration of Castability and Formability for New Magnesium Alloys

A comprehensive consideration based on castability or plastic formability, as well as mechanical properties for development of either cast magnesium alloys or wrought magnesium alloys is a very important issue. To develop new magnesium alloy sheets with high formability at room temperature, the microstructure, texture, ductility and anisotropy of rolled Mg-Zn-Gd alloy sheets were investigated. The sheets exhibit an excellent ultimate elongation of nearly 50% and an uniform elongation greater than 30% with a very low planar anisotropy. The new sheet has a random basal texture and the basal pole is tilted by maximum 40° from the normal direction towards the transverse direction. The majority of grains in the tilted texture have an orientation favorable for both basal slip and tensile twining because of their high Schmid factor. The low planar anisotropy, the large uniform elongations and the high strain hardening rate observed in the Mg-Zn-Gd sheets result in excellent room temperature formability, the Erichsen values reach ~8, well comparable with the conventional aluminum alloys sheets at room temperature. The solidification pathways and phase equilibria of Mg-Al-Ca alloys have been profoundly investigated by using thermal analysis and thermodynamic calculations. The relationship between hot tearing tendency and alloy compositions were discussed in terms of strength of the mushy zone, solidification pathways and feeding mechanisms, et al. Thixoforming refers to as that metal components are formed in their semi-solid state. Criteria for thixoforming are summarized and then the thixoformability of Mg-Al-Ca based alloys (AC alloys) are evaluated using the thermodynamic calculations based on the consideration of metallurgical parameters.

Microstructures and mechanical properties of hot rolled AZ31 Mg alloy sheets

The microstructures and mechanical properties of hot rolled AZ31 Mg alloy sheets were studied to understand the microstrucrure evolution during AZ31 Mg alloy hot rolling process. The roller was heated to 180℃with burning hydrogen, and the extruded plates were rolled at 400℃from 10 to 1 mm with a reduction of 30% in thickness per pass. The result shows that there is no side-cracking of these rolled sheets every pass. The extruded microstructures are greatly refined and mechanical properties are improved. The fine grains of about 4μm were obtained of the final 0.9 mm sheets.

Progress in twin roll casting of magnesium alloys: A review

Twin roll casting was commercialized for a strip production from ferrous and non-ferrous alloys in the 1950 s;however,its application to magnesium has proven difficult and still creates major challenges.This report describes global efforts in expanding manufacturing capabilities of magnesium sheet through twin roll casting path,offering many benefits,including a reduction in number of processing steps and energy savings.In addition to hardware design,alloy transformation during processing,product microstructure and properties,examples of successful solutions along with present technology and knowledge limitations are discussed.A particular attention is paid to developments at Canmet MATERIALS,having the only in North America pilot scale twin roll casting facility,devoted to magnesium.Efforts are described that aim at design of new magnesium alloys,which could take advantage of unique processing conditions during twin roll casting and contribute to the overall progress in magnesium sheet manufacturing.

Mathematic model of rolling pressure during a semisolid shearing-rolling process

A mathematic model of rolling pressure during a novel semisolid shearing-rolling process was established. The rolling pressure in this process is higher than that in the conventional rolling. The increment of rolling pressure in the backward slip zone is higher than that in the forward slip zone, and the neutral plane moves toward to the roll gap entrance. The maximum and the average rolling pressures increase with the decrease of strip thickness, and the effects of strip thickness on the rolling pressure is more obvious in the forward slip zone than in the backward slip zone. Meanwhile, the neutral plane moves toward the roll gap exit with the decrease of strip thickness. The maximum and average rolling pressures increase with the decrease of strip width, and the strip width affects the pressure more obviously in the backward slip zone than in the forward slip zone. At the same time, the neutral plane moves toward the roll gap entrance with the decrease of strip width. The maximum and average rolling pressures increase with increasing roll radius, and the neutral plane moves toward the roll gap exit.

Improvement of material properties and cladded flat product productivity with roll-bonding technology

Taking advantage of the progress of roll-bonding technology, the integrity of the material technology, and the development of the production and examination facilities of all the main carbon steels, stainless steels and specialty alloys in Baosteel, the cladded flat new products, which combined both properties of base material and clad material ,have been developed and produced in large quantities. The product categories includes heavy plates with high alloy content and homogeneous distribution in thickness and carbon steel plates cladded with all kinds of stainless steels ,nickel alloys ,and titanium alloys. The double-sided and single-sided cladding hot roiled strips and cold rolled sheets were also commercially produced. Due to the combined properties of both the cladding material and backing material, all products show obvious improvement in properties when compared with solid material. The comparability with the existing production process and equipment laid a very solid foundation for high productivity.

汽车薄板钢中游离渗碳体的评定方法解析

为了更好地对汽车薄板产品中游离渗碳体组织进行微观评价,结合国内外相关标准中的评定方法介绍了3种评定渗碳体的方法,即级别评定法、定量法和最大限定尺寸法。对每种方法的评定内容进行了详细说明,并分别采用3种方法对一般用冷轧碳钢薄板及钢带中的游离渗碳体进行评定,便于读者更好地理解和使用,为汽车板等产品质量的提升提供可靠的微观评价方法。

冷轧厂薄带钢高效生产的问题及解决方案分析

热镀锌板具有抗腐蚀强、易于深加工、使用寿命长、成本低以及表面美观等特点,主要用于家用电器、汽车等产品的内部构件和面板应用。随着家电板、汽车板工业的发展,家电和汽车所用的镀锌板占全国钢产量的比例逐步提升。随着国内外家电板、汽车板轻质化和高质量的要求,客户对产品表面质量要求越来越严格。针对生产线在提速增产过程中出现的入口跑偏、工艺段带钢表面质量缺陷和薄带钢薄锌层产速受限问题,提出了相应的改进措施。优化后,不仅提高了产量,而且提高了产品质量。

基于铝板带箔轧制油添加剂的简易测定方法研究

随着科学技术和国民经济的快速发展,用户对铝板带箔表面质量的要求越来越高,轧制生产过程中的润滑技术之一正受到世界各国的重视。轧制油是铝板带箔制造流程中十分关键的辅助材料,直接关系工序运行速度和最后制品的质量,轧制油中的添加剂含量也是轧制压油的关键技术指标。因此,本文对于铝板带箔轧制油添加剂的简易测定方法进行相应的研究与分析,仅供参考。

基于共轭梯度算法的镁板热轧压下量PID控制优化

为了进一步提高镁合金板热轧厚度成形控制能力,设计了一种基于共轭梯度算法的镁合金板热轧压下量PID控制方法。基于共轭梯度算法对压下量PID控制优化,引入到双辊热轧镁合金板带横向厚度分布的预测与控制中。研究结果表明:板带预测压下量分布和真实情况相吻合,说明基于共轭梯度算法的导电用镁合金板热轧压下量PID控制优化设计具有良好可靠性。该预测模型平均绝对误差为4.2μm,这验证了基于共轭梯度算法的导电用镁合金板热轧压下量PID控制优化是可行的。该研究有助于提高热轧镁合金板材的成形效率,也可托找到其它的合金轧制领域,具有很好的应用推广价值。

两步升温热轧工艺对AZ31镁合金薄板各向异性及成形性能影响

采用两步梯度升温轧制工艺对AZ31镁合金板材进行轧制,探究轧制过程对镁合金板材显微组织织演化、各向异性及成形性能的影响。第I步轧制在300℃开展,其每道次压下量为15%;第II步轧制在550℃进行,其每道次压下量为40%。经过共4道次轧制后,最终获得厚度为1 mm的镁合金薄板。结果显示,第I步低温轧制过程不更换轧制方向时,试样中生成大量剪切带;而更换轧制方向时,组织内部主要为孪晶和再结晶晶粒。随着II步轧制温度的升高,由于动态再结晶急剧激发,剪切带数量及尺寸逐渐减小,晶粒明显细化。根据IGMA分析得出,非基面滑移,特别是棱柱面滑移活动增强。轧制退火后的AZ31镁合金薄板的力学性能得到提高,各向异性减小,冲压成形性能得到明显改善。

易拉罐盖料及拉环料用铝合金板带材生产概述

文章概述了易拉罐盖料及拉环料用铝合金板带材的主要生产工艺,包括热轧、冷轧、涂层、成型生产工艺,并展望了生产工艺的发展方向。

Effect of the width on AZ31 sheet rolling

A pyramid sheet has been used in experiments and three-dimensional finite element simulation to study the edge cracks and effects of width on AZ31 sheet under rolling. Results show that the edge cracks of Mg sheet comply with the Normalized Crockroft ＆ Latham theory. It can be predicted by D=-0.124＋0.09X - 0.008X2, if D ;〉 0, the edge cracks occur. The sheet shearing deformation at the edge brings about cracks. The strain rate changes periodically with different X. With initial width increases, the recrystallized grain size decreases. The finite element model has been validated by the experiment results.