The influence of different rare earth amounts on microstructure and mechanical properties of 5Cr21Mn9Ni4N steel was studied. The microstructure and composition and shape of inclusions under as-cast, as well as hot rol...The influence of different rare earth amounts on microstructure and mechanical properties of 5Cr21Mn9Ni4N steel was studied. The microstructure and composition and shape of inclusions under as-cast, as well as hot rolling state of 5Cr21Mn9Ni4N steel were observed under metallographic microscope and SEM. The results indicate that dendrite of as-cast condition is refined obviously, the extent of segregation is lightened, dimension of inclusions is lessened, and the shape of inclusions is changed from polygon to ellipse when appropriate amount of mixed rare earth is added. Appropriate rare earth also can lighten the extent of hot rolling texture and improve distribution of carbide under hot rolling state. The results of room temperature and 500 ℃ tensile test show that room temperature tensile strength is firstly improved and then appreciably descended. The elongation percentage decreased with the increase of rare earth amount. Appropriate rare earth amount can improve the high temperature tensile strength and ductility of 5Cr21Mn9Ni4N. Fracture surface observation and energy spectrum analysis indicate that complicated rare earth inclusions appear in the fracture surface when 0.10% (mass fraction) rare earth is added in experimental steels, and tough nests of fracture surface become fine without big hole.展开更多
718 H Pre-ha rdened mold steels with diffe rent Rare Earth(RE) contents were prepared to investigate the influence of RE on microstructure evolution and mechanical properties through a series of experiments and theore...718 H Pre-ha rdened mold steels with diffe rent Rare Earth(RE) contents were prepared to investigate the influence of RE on microstructure evolution and mechanical properties through a series of experiments and theoretical analysis.The results indicated that the toal oxygen(T.O) content decreased from 15 ppm to 6 ppm with 0.022 wt% RE addition,which is attributed to the active chemical properties of RE elements.For test steels,RE additions of 0.012 wt% and 0.022 wt% were significantly effective for refining inclusions by eliminating 11.5% large-sized inclusions with diameter exceeding 10 μm compared with that of ORE steel.RE addition contributed to modify irregular MnS and Al2 O3 inclusions into ellipsoidal RE-inclusions(RE2 O,RES,RE2 O2 S and REAlO3).The purification of molten steel and the modification of inclusions by RE treatment have significant effects on improvement of the fatigue crack growth tests(FCG) inhibition ability and impact energy as well as the isotropy.However,excessive addition of RE elements(0.07 wt%)seriously reduced the impact energy,ultimate tensile strength and FCG inhibition ability due to rapidly increase of the volume fraction of large-sized inclusions.In addition to the inclusions formed by RE treatment,trace solid solution RE atoms improve the stability of undercooled austenite,resulting in the transformation region of bainite and perlite of 0.07 RE steel shifting to the bottom right and prolonging the incubation period compared with that of ORE steel.展开更多
文摘The influence of different rare earth amounts on microstructure and mechanical properties of 5Cr21Mn9Ni4N steel was studied. The microstructure and composition and shape of inclusions under as-cast, as well as hot rolling state of 5Cr21Mn9Ni4N steel were observed under metallographic microscope and SEM. The results indicate that dendrite of as-cast condition is refined obviously, the extent of segregation is lightened, dimension of inclusions is lessened, and the shape of inclusions is changed from polygon to ellipse when appropriate amount of mixed rare earth is added. Appropriate rare earth also can lighten the extent of hot rolling texture and improve distribution of carbide under hot rolling state. The results of room temperature and 500 ℃ tensile test show that room temperature tensile strength is firstly improved and then appreciably descended. The elongation percentage decreased with the increase of rare earth amount. Appropriate rare earth amount can improve the high temperature tensile strength and ductility of 5Cr21Mn9Ni4N. Fracture surface observation and energy spectrum analysis indicate that complicated rare earth inclusions appear in the fracture surface when 0.10% (mass fraction) rare earth is added in experimental steels, and tough nests of fracture surface become fine without big hole.
基金financially supported by China Postdoctoral Science Foundation (No. 2019M661153)National Natural Science Foundation of China (No. 51701225)Project to Strengthen Industrial Development at the Grass-roots Level (No. TC190A4DA/35)。
文摘718 H Pre-ha rdened mold steels with diffe rent Rare Earth(RE) contents were prepared to investigate the influence of RE on microstructure evolution and mechanical properties through a series of experiments and theoretical analysis.The results indicated that the toal oxygen(T.O) content decreased from 15 ppm to 6 ppm with 0.022 wt% RE addition,which is attributed to the active chemical properties of RE elements.For test steels,RE additions of 0.012 wt% and 0.022 wt% were significantly effective for refining inclusions by eliminating 11.5% large-sized inclusions with diameter exceeding 10 μm compared with that of ORE steel.RE addition contributed to modify irregular MnS and Al2 O3 inclusions into ellipsoidal RE-inclusions(RE2 O,RES,RE2 O2 S and REAlO3).The purification of molten steel and the modification of inclusions by RE treatment have significant effects on improvement of the fatigue crack growth tests(FCG) inhibition ability and impact energy as well as the isotropy.However,excessive addition of RE elements(0.07 wt%)seriously reduced the impact energy,ultimate tensile strength and FCG inhibition ability due to rapidly increase of the volume fraction of large-sized inclusions.In addition to the inclusions formed by RE treatment,trace solid solution RE atoms improve the stability of undercooled austenite,resulting in the transformation region of bainite and perlite of 0.07 RE steel shifting to the bottom right and prolonging the incubation period compared with that of ORE steel.
文摘以含镍低碳铸钢为研究对象,通过改变一号稀土加入量,经过金相组织观察、拉伸试验、冲击试验、夹杂物形貌分析、能谱分析等,研究RE含量变化对铸钢试样组织和性能的影响.研究结果表明:铸钢试样经调质处理后,组织为细小回火索氏体,存在少量铁素体.随着一号稀土质量分数增加,回火索氏体含量增多,晶粒尺寸减小;长条状或者尖角状夹杂物减少,稀土夹杂物主要是以球状或者近球状的形态存在,大小在5~10μm.抗拉强度、屈服强度和布氏硬度总体上呈现不断增加的趋势,在一号稀土含量为0.5%时,其值最高,抗拉强度为905.2 MPa,屈服强度为776.7 MPa,布氏硬度为274.冲击功先增加后降低,一号稀土质量分数在0.3%时,冲击功值为80 J.