A semisolid slurry of AZ31 magnesium alloy was prepared by vibrating wavelike sloping plate process,and the semisolid die forging process,microstructures,and properties of the magnesium alloy mobile telephone shell we...A semisolid slurry of AZ31 magnesium alloy was prepared by vibrating wavelike sloping plate process,and the semisolid die forging process,microstructures,and properties of the magnesium alloy mobile telephone shell were investigated.The semisolid forging process was performed on a YA32-315 four-column universal hydraulic press.The microstructures were observed by optical microscopy,the hardness was analyzed with a model 450SVD Vickers hardometer,the mechanical properties was measured with a CMT5105 tensile test machine,and the fractograph of elongated specimens was observed by scanning electron microscopy (SEM).The results reveal that with the increase of die forging force,the microstructures of the product become fine and dense.A lower preheating temperature and a longer dwell time are favorable to the formation of fine and dense microstructures.The optimum process conditions of preparing mobile telephone shells with excellent surface quality and microstructures are a die forging force of 2000 kN,a die preheating temperature of 250℃,and a dwell time of 240 s.After solution treatment at 430℃ and aging at 220℃ for 8 h,the Vickers hardness is 61.7 and the ultimate tensile strength of the product is 193MPa.Tensile fractographs show the mixing mechanisms of quasi-cleavage fracture and ductile fracture.展开更多
The effects of ultrasonic vibration temperature on the microstructure of semisolid Sn-52 Bi alloy and mechanical properties were investigated. The results show that the microstructure and mechanical properties are imp...The effects of ultrasonic vibration temperature on the microstructure of semisolid Sn-52 Bi alloy and mechanical properties were investigated. The results show that the microstructure and mechanical properties are improved obviously after the ultrasonic treatment. Nearly round and uniformly distributed primary Sn phase particles were obtained under the cavitation and acoustic streaming caused by ultrasonic treatment. The best effects of ultrasonic treatment on microstructure and mechanical properties were obtained with the ultrasonic vibration for 120 s at 140 ℃. The elongation of semisolid Sn-52 Bi alloy treated by ultrasonic vibration for 120 s at 140 ℃ was 42% and increased by 156.09% compared to conventional liquid casting Sn-52 Bi alloy without ultrasonic vibration. It is a feasible and effective method to adopt the semisolid metal forming technology assisted with ultrasonic vibration to improve the ductility of Sn-Bi alloys.展开更多
6061 aluminum alloy semisolid billet was prepared by the equal-channel angular processing(ECAP)-recrystallization and partial(RAP)process(a combination of equal-channel angular processing and recrystallization and par...6061 aluminum alloy semisolid billet was prepared by the equal-channel angular processing(ECAP)-recrystallization and partial(RAP)process(a combination of equal-channel angular processing and recrystallization and partial remelting).The effects of different process parameters on the alloy microstructure were studied and the quantitative relationship between the process parameters and microstructure was established by response surface methodology(RSM)to optimize the process parameters.According to the orthogonal test,the holding temperature and holding time of the four ECAP-RAP process parameters were found to have the greatest impact on the microstructural characteristics,including average grain size and average shape factor.Through RSM,it was also found that when the average grain size or the average shape factor is optimized separately,another will be degraded.When the two indexes were simultaneously considered,the optimal process parameters were found to be a holding temperature of 623°C and holding time of 13 min,and the corresponding average grain size and average shape factor were 35.97μm and 0.8535,respectively.Moreover,comparing the experimental and predicted values,the reliability of the established response surface model was verified.展开更多
The evolution of semisolid microstructure during partial remelting of(CNTs+Sip)/AZ91 D powder compacts prepared by cold pressing was studied.The results indicate that rapid grain coarsening is driven by the dissolutio...The evolution of semisolid microstructure during partial remelting of(CNTs+Sip)/AZ91 D powder compacts prepared by cold pressing was studied.The results indicate that rapid grain coarsening is driven by the dissolution of eutecticβphase material during the initial heating period of 0-10 min,so the AZ91 D powders with fine equiaxed grains surrounded by intergranular eutectic phases evolve into compact particles.As the heating time proceeds,α-Mg particles were gradually separated by liquid due to the phase transformations ofα-Mg+β→L andα-Mg→L.The primary particles coarsened rather slowly and the as-received Mg powder evolved into nearly spheroidal particles surrounded by liquid phase after partial remelting.The in situ synthesized Mg2 Sip were distributed homogeneously around the CNTs with maintained structural integrity during partial remelting.Moreover,this microstructural evolution was accompanied by densification through pore filling.An ideal semisolid ingot suitable for thixoforming can therefore be obtained by partially remelting a(CNTs+Sip)/Mg powder compact.展开更多
基金supported by the National Natural Science Foundation of China (Nos.51034002 and 50974038)the New Century Talents Support Program Project of the Ministry of Education of China (No.NCET-08-0097)
文摘A semisolid slurry of AZ31 magnesium alloy was prepared by vibrating wavelike sloping plate process,and the semisolid die forging process,microstructures,and properties of the magnesium alloy mobile telephone shell were investigated.The semisolid forging process was performed on a YA32-315 four-column universal hydraulic press.The microstructures were observed by optical microscopy,the hardness was analyzed with a model 450SVD Vickers hardometer,the mechanical properties was measured with a CMT5105 tensile test machine,and the fractograph of elongated specimens was observed by scanning electron microscopy (SEM).The results reveal that with the increase of die forging force,the microstructures of the product become fine and dense.A lower preheating temperature and a longer dwell time are favorable to the formation of fine and dense microstructures.The optimum process conditions of preparing mobile telephone shells with excellent surface quality and microstructures are a die forging force of 2000 kN,a die preheating temperature of 250℃,and a dwell time of 240 s.After solution treatment at 430℃ and aging at 220℃ for 8 h,the Vickers hardness is 61.7 and the ultimate tensile strength of the product is 193MPa.Tensile fractographs show the mixing mechanisms of quasi-cleavage fracture and ductile fracture.
基金Funded by the National Natural Science Foundation of China(No.51104049)
文摘The effects of ultrasonic vibration temperature on the microstructure of semisolid Sn-52 Bi alloy and mechanical properties were investigated. The results show that the microstructure and mechanical properties are improved obviously after the ultrasonic treatment. Nearly round and uniformly distributed primary Sn phase particles were obtained under the cavitation and acoustic streaming caused by ultrasonic treatment. The best effects of ultrasonic treatment on microstructure and mechanical properties were obtained with the ultrasonic vibration for 120 s at 140 ℃. The elongation of semisolid Sn-52 Bi alloy treated by ultrasonic vibration for 120 s at 140 ℃ was 42% and increased by 156.09% compared to conventional liquid casting Sn-52 Bi alloy without ultrasonic vibration. It is a feasible and effective method to adopt the semisolid metal forming technology assisted with ultrasonic vibration to improve the ductility of Sn-Bi alloys.
基金the National Key Research and Development Program of China(Nos.2017YFB0701803 and 2016YFB0701403)the State Key Laboratory of Nickel and Cobalt Resources Comprehensive Utilization,China。
文摘6061 aluminum alloy semisolid billet was prepared by the equal-channel angular processing(ECAP)-recrystallization and partial(RAP)process(a combination of equal-channel angular processing and recrystallization and partial remelting).The effects of different process parameters on the alloy microstructure were studied and the quantitative relationship between the process parameters and microstructure was established by response surface methodology(RSM)to optimize the process parameters.According to the orthogonal test,the holding temperature and holding time of the four ECAP-RAP process parameters were found to have the greatest impact on the microstructural characteristics,including average grain size and average shape factor.Through RSM,it was also found that when the average grain size or the average shape factor is optimized separately,another will be degraded.When the two indexes were simultaneously considered,the optimal process parameters were found to be a holding temperature of 623°C and holding time of 13 min,and the corresponding average grain size and average shape factor were 35.97μm and 0.8535,respectively.Moreover,comparing the experimental and predicted values,the reliability of the established response surface model was verified.
基金financially supported by the Ningxia Natural Science Foundation of China(No.2018AAC03031)the Basic Scientific Fund of Ningxia university(No.NGY2018009)the Natural Science Foundation of Ningxia University(No.ZR1702)。
文摘The evolution of semisolid microstructure during partial remelting of(CNTs+Sip)/AZ91 D powder compacts prepared by cold pressing was studied.The results indicate that rapid grain coarsening is driven by the dissolution of eutecticβphase material during the initial heating period of 0-10 min,so the AZ91 D powders with fine equiaxed grains surrounded by intergranular eutectic phases evolve into compact particles.As the heating time proceeds,α-Mg particles were gradually separated by liquid due to the phase transformations ofα-Mg+β→L andα-Mg→L.The primary particles coarsened rather slowly and the as-received Mg powder evolved into nearly spheroidal particles surrounded by liquid phase after partial remelting.The in situ synthesized Mg2 Sip were distributed homogeneously around the CNTs with maintained structural integrity during partial remelting.Moreover,this microstructural evolution was accompanied by densification through pore filling.An ideal semisolid ingot suitable for thixoforming can therefore be obtained by partially remelting a(CNTs+Sip)/Mg powder compact.