Boosting kinetic separation of ethylene and ethane on microporous materials via crystal size control

The adsorptive separation of C_(2)H_(4)and C_(2)H_(6),as an alternative to distillation units consuming high energy,is a promising yet challenging research.The great similarity in the molecular size of C_(2)H_(4)and C_(2)H_(6)brings challenges to the regulation of adsorbents to realize efficient dynamic separation.Herein,we reported the enhancement of the kinetic separation of C_(2)H_(4)/C_(2)H_(6)by controlling the crystal size of ZnAtzPO_(4)(Atz=3-amino-1,2,4-triazole)to amplify the diffusion difference of C_(2)H_(4)and C_(2)H_(6).Through adjusting the synthesis temperature,reactant concentration,and ligands/metal ions molar ratio,ZnAtzPO4 crystals with different sizes were obtained.Both single-component kinetic adsorption tests and binary-component dynamic breakthrough experiments confirmed the enhancement of the dynamic separation of C_(2)H_(4)/C_(2)H_(6)with the increase in the crystal size of ZnAtzPO_(4).The separation selectivity of C_(2)H_(4)/C_(2)H_(6)increased from 1.3 to 98.5 with the increase in the crystal size of ZnAtzPO_(4).This work demonstrated the role of morphology and size control of adsorbent crystals in the improvement of the C_(2)H_(4)/C_(2)H_(6)kinetic separation performance.

Analysis of flow separation control using nanosecond-pulse discharge plasma actuators on a flying wing

Dielectric barrier discharge （DBD） plasma is one of most promising flow control method for its several advantages. The present work investigates the control authority of nanosecond pulse DBD plasma actuators on a flying wing model＇s aerodynamic characteristics. The aerodynamic forces and moments are studied by means of experiment and numerical simulation. The numerical simulation results are in good agreement with experiment results. Both results indicate that the NS-DBD plasma actuators have negligible effect on aerodynamic forces and moment at the angles of attack smaller than 16-. However, significant changes can be achieved with actuation when the model＇s angle of attack is larger than 16° where the flow separation occurs. The spatial flow field structure results from numerical simulation suggest that the volumetric heat produced by NS-DBD plasma actuator changes the local temperature and density and induces several vortex structures, which strengthen the mixing of the shear layer with the main flow and delay separation or even reattach the separated flow.

Optimization of Control Loops and Operating Parameters for Three-Phase Separators Used in Oilfield Central Processing Facilities

In this study,the Stokes formula is used to analyze the separation effect of three-phase separators used in a Oilfield Central Processing Facility.The considered main influencing factors include(but are not limited to)the typical size of oil and water droplets,the residence time and temperature of fluid and the dosage of demulsifier.Using the“Specification for Oil and Gas Separators”as a basis,the control loops and operating parameters of each separator are optimized Considering the Halfaya Oilfield as a testbed,it is shown that the proposed approach can lead to good results in the production stage.

Experimental Investigation of Flow Separation Control Using Dielectric Barrier Discharge Plasma Actuators

Influence of plasma actuators as a flow separation control device was investigated experimentally. Hump model was used to demonstrate the effect of plasma actuators on external flow separation, while for internal flow separation a set of compressor cascade was adopted. In order to investigate the modification of the flow structure by the plasma actuator, the flow field was examined non-intrusively by particle image velocimetry measurements in the hump model experiment and by a hot film probe in the compressor cascade experiment. The results showed that the plasma actuator could be effective in controlling the flow separation both over the hump and in the compressor cascade when the incoming velocity was low. As the incoming velocity increased, the plasma actuator was less effective. It is urgent to enhance the intensity of the plasma actuator for its better application. Methods to increase the intensity of plasma actuator were also studied.

Flow separation control over an airfoil using continuous alternating current plasma actuator

The flow separation control over an NACA 0015 airfoil using continuous alternating current(AC)dielectric barrier discharge(DBD)plasma actuator is investigated experimentally and numerically.This work is intended to report some observations made from our experiment,to which little attention is paid in the previous studies,but which is thought to be important to the understanding of control of complex flow separation with AC DBD.To this end,the response of separated flow to AC plasma actuation is visualized through the time-resolved particle image velocimetry(PIV)measurement,whereas numerical simulation is carried out to complement the experiment.The flow control process at chord-based Reynolds number(Re)of 3.31×105 is investigated.It is found that the response of external flow to plasma forcing is delayed for up to tens of milliseconds and the delay time increases with angle of attack increasing.Also observed is that at the intermediate angle of attack near stall,the forced flow features a well re-organized flow pattern.However,for airfoil at high post-stall angle of attack,the already well suppressed flow field can recover to the massively separated flow state and then reattach to airfoil surface with the flow pattern fluctuating between the two states in an irregular manner.This is contrary to one’s first thought that the forced flow at any angles of attack will become well organized and regular,and reflects the complexity of flow separation control.

Stimuli-responsive Membranes： Smart Tools for Controllable Mass-transfer and Separation Processes

As emerging artificial biomimetic membranes, smart or intelligent membranes that are able to respond to environmental stimuli are attracting ever-increasing interests from various fields. Their permeation properties including hydraulic permeability and diffusional permeability can be dramatically controlled or adjusted self-regulatively in response to small chemical and/or physical stimuli in their environments. Such environmental stimuli-responsive smart membranes could find myriad applications in numerous fields ranging from controlled release to separations. Here the trans-membrane mass-transfer and membrane separation is introduced as the beginning to initiate the requirement of smart membranes, and then bio-inspired design of environmental stimuli-responsive smart membranes and four essential elements for smart membranes are introduced and discussed. Next, smart membrane types and their applications as smart tools for controllable mass-transfer in controlled release and separations are reviewed. The research topics in the near future are also suggested.

Fuzzy self-tuning PID control of the operation temperatures in a two-staged membrane separation process

为从精炼厂气体的氢恢复的一个二阶段的膜分离过程被介绍。煤气的膜分离过程的原则和操作温度的影响被分析。因为常规 PID 控制器是困难的使操作温度稳定，一个模糊自我调节的 PID 控制算法被建议。申请证明算法是有效的，两个阶段的操作温度能稳定地被控制，并且氢恢复单位的操作灵活性和适应性安全地被提高。这研究打一个基础优化膜分离进程的控制并且因此保证膜性能。

SEPARATION CONTROL FOR THE OUTWING OF A STRAKE－WING BY ROTATING CONE PLACED NEAR THE LEADING EDGE

Based on the research result on the strake-wing, when the size of a strakeis not large, there is a separation zone near the leading edge of the outwing of thestrake-wing at middle angles of attack. So the idea on separation control by rotating acone placed near the leading edge is presented. The cone surface consists of the part ofthe wing. The effect of rotating the cone on aerodynamic characteristics of thestrake-wing is investigated. The results show that a rotating surface could play an important role in controlling the flow separation for a 3-dimensional wing. For example,the relative increment in maximum lift coefficient attains 30%. The separation zone issuppressed to a certain extent.

Capillary Electrophoretic Separation of Proteins under the Control of Radial Electric Field

Separation of basic proteins was performed using a homemade field-modulated capillary electrophoresis system. The resolution. elution and even wall adsorption can be regulated by ad-lusting the radial rather than axial voltage applied. Selection of running buffer and pH was found to be critical.

Optimum Duty Cycle of Unsteady Plasma Aerodynamic Actuation for NACA0015 Airfoil Stall Separation Control

Unsteady dielectric barrier discharge（DBD） plasma aerodynamic actuation technology is employed to suppress airfoil stall separation and the technical parameters are explored with wind tunnel experiments on an NACA0015 airfoil by measuring the surface pressure distribution of the airfoil.The performance of the DBD aerodynamic actuation for airfoil stall separation suppression is evaluated under DBD voltages from 2000 V to 4000 V and the duty cycles varied in the range of 0.1 to 1.0.It is found that higher lift coefficients and lower threshold voltages are achieved under the unsteady DBD aerodynamic actuation with the duty cycles less than 0.5as compared to that of the steady plasma actuation at the same free-stream speeds and attack angles,indicating a better flow control performance.By comparing the lift coefficients and the threshold voltages,an optimum duty cycle is determined as 0.25 by which the maximum lift coefficient and the minimum threshold voltage are obtained at the same free-stream speed and attack angle.The non-uniform DBD discharge with stronger discharge in the positive half cycle due to electrons deposition on the dielectric slabs and the suppression of opposite momentum transfer due to the intermittent discharge with cutoff of the negative half cycle are responsible for the observed optimum duty cycle.

Type selection and maintenance of the control system of large-scale air separation units

Based on the practice of Baosteel＇ s 60000 m3/h air separation unit （ASU） ,which is the first domestically- integrated unit of such a scale, this paper studies the principles of type selection of the distribution control system （DCS）. It discusses the design of the unit＇s control system,which involves a compressor system,a purification system （molecular sieving）, a turbo expansion system and an air separation system. The final part of the paper discusses the maintenance and future development of the ASU control system at Baosteel.

Control of Corner Separation by Optimized Slot Configuration in a Linear Compressor Cascade

为控制压气机叶片吸力面与端壁处所形成的三维角区分离,本文在叶根处引入了从压力面到吸力面的槽道来控制角区分离流动。基于利用优化算法对叶根处槽道几何的优化结果,本文通过数值模拟和实验来分析槽道在不同进口攻角下对角区分离的控制效果。本文通过对比原始和开槽叶栅中总压损失、静压升和三维角区分离特征表明叶根处引入的槽道对角区分离有明显的控制效果。

Design and control of fraction cutting for the separation of mixed alcohols from the Fischer-Tropsch aqueous by-products

Since the minimum-boiling azeotropes of C2-C8 alcohols with water and high-water content(up to 95%(mass))in the Fischer-Tropsch aqueous by-products,the separation is energy-intensive and challenging.The energy-saving strategy for the complete separation of the Fischer-Tropsch aqueous by-products has received massive attention in recent decades.In this study,a stripper-sidestream decanter process is proposed by exploiting homogeneous azeotropes(C2-C3 alcohols-water)and heterogeneous azeotropes(C4-C8 alcohols-water).The introduction of the stripping column for pre-dehydration avoids the revaporization of the mixture,and energy carried by the overhead vapor is conserved instead of being removed in a condenser.The precise fraction cutting of C1-C3 alcohol-water mixture,C4-C8 alcohols,and water is realized by the sidestream distillation column.The C4-C8 alcohols rich mixture withdrawn from the sidestream flows into the decanter to break the distillation boundary,where the organic phase returns to the sidestream distillation column to obtain the dehydrated C4-C8 alcohols,and the aqueous phase enters the stripping column.Steady-state optimization based on total annual cost(TAC)minimization shows that the stripper-sidestream decanter process reduces TAC by 17.00%and saves energy by 21.27%compared with the conventional three-column distillation process.Further,a control structure of the process is established,and dynamic simulations show that the control structure combining a differential controller with a low-selector exhibits robust co ntrol.This study provides a novel design scheme and deepens the insights into the efficient separation of aqueous by-products of the Fischer-Tropsch synthesis.

A Virtual Router Cluster System Based on the Separation of the Control Plane and the Data Plane

This paper proposes a virtual router cluster system based on the separation of the control plane and the data plane from multiple perspectives,such as architecture,key technologies,scenarios and standardization.To some extent,the virtual cluster simplifies network topology and management,achieves automatic conFig.uration and saves the IP address.It is a kind of low-cost expansion method of aggregation equipment port density.

Influence of separator control on the characteristics of severe slugging flow

Due to the special structure of offshore multiphase pipes, it is easy for severe slugging to occur in the riser at low gas-liquid velocity. Violent pressure fluctuations and dramatic changes of flow rate are the main characteristics of severe slugging, leading to the risk of serious damage. In this paper, the separator control is adopted to accurately control the separator liquid level and pressure under severe slugging flow conditions. This indicates that the separator liquid level control alone does not have a significant impact on the upstream flow, but it is beneficial for normal operation and pressure control of the separator. As the separator pressure increases, the peak pressure in the riser apparently diminishes, and the amplitude of pressure fluctuation gradually decreases, which means that severe slugging is inhibited. During the slug blowing out, the gas/liquid slipping in the riser intensifies. The long gas plug quickly flows through the riser, and then tends to morph into short and slowly flowing gas bubbles. The elimination effect of the pressure control strategy on severe slugging is related to the relative rate of the superficial gas/liquid flow.

The research progress and prospect for the technology of controlling surface subsidence by grouting separated layer in overburden at coal mines in China

The developed process and theoretical achievement for the technology of controlling surface subsidence by grouting separated layer in overburden is summarized in this paper. The research progress of the technology is discussed synthetically on the basis of practice and research results obtained at coal mine of China in recent years. According to the development tendency of mining under buildings, water bodies and railroads and the properties of the technology, the future research direction is proposed.

Application of the dividing wall column to olefin separation in fluidization methanol to propylene(FMTP) process

Dividing wall column(DWC)is shown to be energy efficient compared to conventional column sequence for multi components separation,which is used for olefin separation in fluidization methanol to propylene process in the present work.Detailed design for pilot DWC was performed and five control structures,i.e.composition control(CC),temperature control(TC),composition-temperature control(CC-TC),temperature difference control(TDC),double temperature difference control(DTDC)were proposed to circumvent feed disturbance.Sensitivity analysis and singular value decomposition(SVD)were used as criterion to select the controlled temperature locations in TC,CC-TC,TDC and DTDC control loops.The steady simulation result demonstrates that 25.7% and 30.2% duty can be saved for condenser and reboiler by substituting conventional column sequence with DWC,respectively.As for control structure selection,TC and TDC perform better than other three control schemes with smaller maximum deviation and shorter settling time.

ETH-GQS: An estimation of geoid-to-quasigeoid separation over Ethiopia

The determination of accurate orthometric or normal heights remains one of the main challenges for the geodetic community in Ethiopia.These heights are required for geodetic and geodynamic scientific research as well as for extensive engineering applications.The main objective of this study is to estimate the geoid-to-quasi geoid separation(GQS)in Ethiopia(ETH-GQS).Such separation would be required for the conversion between geoid and quasigeoid models,which is mandatory for the determination of accurate geodetic heights in mountain regions.The airborne free-air gravity anomalies and the topo-graphic information retrieved from the SRTM3(Shuttle Radar Topography Mission of a spatial resolution 3 arc-second)digital elevation model were used to compute the ETH-GQS model according to the Sjoberg's strict formula for the geoid-to-quasigeoid separation.The ETH-GQS was then validated using GNSS-levelling data as well as geoid heights determined from different Global Geopotential Models(GGMs),namely the EGM2008,EIGEN-6C4 and GECO.The results reveal that the standard deviation of differences between the geoid heights obtained from the EIGEN-6C4 model and the geometric geoid heights obtained from GNSS-levelling data were improved by~75%(i.e.from~24 to~6 cm)when considering GQS values obtained from the ETH-GQS.

DOUBLE LOOP ACTIVE VIBRATION CONTROL OF PNEUMATIC ISOLATOR WITH TWO SEPARATE CHAMBERS

A newly designed pneumatic spring with two separate chambers is promoted and double-loop active control is introduced to overcome the following drawbacks of passive pneumatic isolation： ① The low frequency resonances introduced into the system; ② Conflict between lower isolation frequency and stiffness high enough to limit quasi-static stroke;③ Inconsistent isolation level with different force load. The design of two separate chambers is for the purpose of tuning support frequency and force independently and each chamber is controlled by a different valve. The inner one of double-loop structure is pressure control, and in order to obtain good performance, nonlinearities compensation and motion flow rate compensation （MFRC） are added besides the basic cascade compensation, and the influence of tube length is studied. The outer loop has two functions： one is to eliminate the resonance caused by isolation support and to broaden the isolation frequency band by payload velocity feedback and base velocity feed forward, and the other is to tune support force and support stiffness simultaneously and independently, which means the support force will have no effect on support stiffness. Theoretical analysis and experiment results show that the three drawbacks are overcome simultaneously.