Micron TiNi alloy blocks were fabricated at high temperature by equal channel angular extrusion （ECAE） using hotforged Ti-50.3at%Ni alloy as the raw material and the effects of deformation temperature and postdeform...Micron TiNi alloy blocks were fabricated at high temperature by equal channel angular extrusion （ECAE） using hotforged Ti-50.3at%Ni alloy as the raw material and the effects of deformation temperature and postdeformation annealing on the severely deformed TiNi alloy by ECAE were investigated. The results show that the TiNi alloy processed by ECAE undergoes severe plastic deformation, and lowering the deformation temperature and increasing the number of extrusions contribute to grain refinement. When the annealing temperature is below 873 K, static recovery is the main restoration process; when the temperature rises to 973 K, static recrystallization occurs. It is found that fine particles are precipitated when the TiNi alloy processed by ECAE is annealed at 773 K.展开更多
Ti Ni shape memory alloys（SMAs） have been normally used as the competent elements in large part of the industries due to outstanding properties, such as super elasticity and shape memory effects. However, traditiona...Ti Ni shape memory alloys（SMAs） have been normally used as the competent elements in large part of the industries due to outstanding properties, such as super elasticity and shape memory effects. However, traditional machining of SMAs is quite complex due to these properties. Hence, the wire electric discharge machining（WEDM） characteristics of Ti Ni SMA was studied. The experiments were planned as per L27 orthogonal array to minimize the experiments, each experiment was performed under different conditions of pulse duration, pulse off time, servo voltage, flushing pressure and wire speed. A multi-response optimization method using Taguchi design with utility concept has been proposed for simultaneous optimization. The analysis of means（ANOM） and analysis of variance（ANOVA） on signal to noise（S/N） ratio were performed for determining the optimal parameter levels. Taguchi analysis reveals that a combination of 1 μs pulse duration, 3.8 μs pulse off time, 40 V servo voltage, 1.8×105 Pa flushing pressure and 8 m/min wire speed is beneficial for simultaneously maximizing the material removal rate（MRR） and minimizing the surface roughness. The optimization results of WEDM of Ti Ni SMA also indicate that pulse duration significantly affects the material removal rate and surface roughness. The discharged craters, micro cracks and recast layer were observed on the machined surface at large pulse duration.展开更多
采用 DSC、弯曲实验和扫描电镜分析研究了热处理工艺对医用 TiNi 合金细丝显微组织、相变温度和形状记忆效应的影响。结果表明,400℃~500℃,30 min^120 min 热处理时,随着温度的升高和时间的增长,TiNi 合金细丝中 Ti3Ni4析出相增多,相...采用 DSC、弯曲实验和扫描电镜分析研究了热处理工艺对医用 TiNi 合金细丝显微组织、相变温度和形状记忆效应的影响。结果表明,400℃~500℃,30 min^120 min 热处理时,随着温度的升高和时间的增长,TiNi 合金细丝中 Ti3Ni4析出相增多,相变温度也升高。细丝经 500℃,30 min 处理后的最大可回复应变量值最大。随弯曲变形量的增加,疲劳寿命缩短。500℃处理的试样疲劳寿命最长。展开更多
基金This work was financially supported by the National Natural Science Foundation of China (No.A50071034)
文摘Micron TiNi alloy blocks were fabricated at high temperature by equal channel angular extrusion （ECAE） using hotforged Ti-50.3at%Ni alloy as the raw material and the effects of deformation temperature and postdeformation annealing on the severely deformed TiNi alloy by ECAE were investigated. The results show that the TiNi alloy processed by ECAE undergoes severe plastic deformation, and lowering the deformation temperature and increasing the number of extrusions contribute to grain refinement. When the annealing temperature is below 873 K, static recovery is the main restoration process; when the temperature rises to 973 K, static recrystallization occurs. It is found that fine particles are precipitated when the TiNi alloy processed by ECAE is annealed at 773 K.
文摘Ti Ni shape memory alloys（SMAs） have been normally used as the competent elements in large part of the industries due to outstanding properties, such as super elasticity and shape memory effects. However, traditional machining of SMAs is quite complex due to these properties. Hence, the wire electric discharge machining（WEDM） characteristics of Ti Ni SMA was studied. The experiments were planned as per L27 orthogonal array to minimize the experiments, each experiment was performed under different conditions of pulse duration, pulse off time, servo voltage, flushing pressure and wire speed. A multi-response optimization method using Taguchi design with utility concept has been proposed for simultaneous optimization. The analysis of means（ANOM） and analysis of variance（ANOVA） on signal to noise（S/N） ratio were performed for determining the optimal parameter levels. Taguchi analysis reveals that a combination of 1 μs pulse duration, 3.8 μs pulse off time, 40 V servo voltage, 1.8×105 Pa flushing pressure and 8 m/min wire speed is beneficial for simultaneously maximizing the material removal rate（MRR） and minimizing the surface roughness. The optimization results of WEDM of Ti Ni SMA also indicate that pulse duration significantly affects the material removal rate and surface roughness. The discharged craters, micro cracks and recast layer were observed on the machined surface at large pulse duration.
文摘采用 DSC、弯曲实验和扫描电镜分析研究了热处理工艺对医用 TiNi 合金细丝显微组织、相变温度和形状记忆效应的影响。结果表明,400℃~500℃,30 min^120 min 热处理时,随着温度的升高和时间的增长,TiNi 合金细丝中 Ti3Ni4析出相增多,相变温度也升高。细丝经 500℃,30 min 处理后的最大可回复应变量值最大。随弯曲变形量的增加,疲劳寿命缩短。500℃处理的试样疲劳寿命最长。
