We demonstrated a scheme of phase-locked terahertz quantum cascade lasers(THz QCLs)array,with a single-mode pulse power of 108 mW at 13 K.The device utilizes a Talbot cavity to achieve phase locking among five ridge l...We demonstrated a scheme of phase-locked terahertz quantum cascade lasers(THz QCLs)array,with a single-mode pulse power of 108 mW at 13 K.The device utilizes a Talbot cavity to achieve phase locking among five ridge lasers with first-order buried distributed feedback(DFB)grating,resulting in nearly five times amplification of the single-mode power.Due to the optimum length of Talbot cavity depends on wavelength,the combination of Talbot cavity with the DFB grating leads to better power amplification than the combination with multimode Fabry-Perot(F-P)cavities.The Talbot cavity facet reflects light back to the ridge array direction and achieves self-imaging in the array,enabling phase-locked operation of ridges.We set the spacing between adjacent elements to be 220μm,much larger than the free-space wavelength,ensuring the operation of the fundamental supermode throughout the laser's dynamic range and obtaining a high-brightness far-field distribution.This scheme provides a new approach for enhancing the single-mode power of THz QCLs.展开更多
The generation of electricity based on renewable energy sources,parti-cularly Photovoltaic(PV)system has been greatly increased and it is simply insti-gated for both domestic and commercial uses.The power generated fr...The generation of electricity based on renewable energy sources,parti-cularly Photovoltaic(PV)system has been greatly increased and it is simply insti-gated for both domestic and commercial uses.The power generated from the PV system is erratic and hence there is a need for an efficient converter to perform the extraction of maximum power.An improved interleaved Single-ended Primary Inductor-Converter(SEPIC)converter is employed in proposed work to extricate most of power from renewable source.This proposed converter minimizes ripples,reduces electromagnetic interference due tofilter elements and the contin-uous input current improves the power output of PV panel.A Crow Search Algo-rithm(CSA)based Proportional Integral(PI)controller is utilized for controlling the converter switches effectively by optimizing the parameters of PI controller.The optimized PI controller reduces ripples present in Direct Current(DC)vol-tage,maintains constant voltage at proposed converter output and reduces over-shoots with minimum settling and rise time.This voltage is given to single phase grid via 1�Voltage Source Inverter(VSI).The command pulses of 1�VSI are produced by simple PI controller.The response of the proposed converter is thus improved with less input current.After implementing CSA based PI the efficiency of proposed converter obtained is 96%and the Total Harmonic Distor-tion(THD)is found to be 2:4%.The dynamics and closed loop operation is designed and modeled using MATLAB Simulink tool and its behavior is performed.展开更多
Two experimental single crystal superalloys, the Ru-free alloy and the Ru-containing alloy with [001 ] orientation, were cast in a directionally solidified furnace, while other alloying element contents were kept unch...Two experimental single crystal superalloys, the Ru-free alloy and the Ru-containing alloy with [001 ] orientation, were cast in a directionally solidified furnace, while other alloying element contents were kept unchanged. The effects of Ru on the microstructure and phase stability of the single crystal superalloy were investigated, y' directional coarsening and rafting were observed in the Ru-free alloy and Ru-containing alloy after long-term aging at 1070~C for 800 h. Needle-shaped o topologically close packed (TCP) phases precipitated and grew along the fixed direction in both the alloys. The precipitating rate and volume fraction of TCP phases decreased significantly by adding Ru. The compositions ofy and y' phases measured using an energy-dispersive X-ray spectroscope (EDS) in transmission electron microscopy (TEM) analysis showed that the addition of Ru lessened the partition ratio of TCP forming elements, Re, W and Mo, and decreased the satu- ration degrees of these elements in y phase, which can enable the Ru-containing alloy to be more resistant to the formation of TCP phases. It is indicated that the addition of Ru to the Ni-based single crystal superalloy with high content of the refractory alloying element can enhance phase stability.展开更多
Solidification structure variation of single phase alloy with undercooling prior to nucleation has been widely studied. The progress, especially during the last decade, is reviewed so as to give a comprehensive knowle...Solidification structure variation of single phase alloy with undercooling prior to nucleation has been widely studied. The progress, especially during the last decade, is reviewed so as to give a comprehensive knowledge for it, in which the emphases are laid on the structure evolution mechanism and the potential application. Lastly, the future interesting subjects are presented.展开更多
Microstructure of transient liquid phase( TLP) diffusion bonded a third generation single crystal superalloy joint was investigated using scanning electron microscopy( SEM),and mechanical properties test of joint was ...Microstructure of transient liquid phase( TLP) diffusion bonded a third generation single crystal superalloy joint was investigated using scanning electron microscopy( SEM),and mechanical properties test of joint was carried out,for obtaining relationship between microstructure and mechanical properties of joint. The results showed that the joint contained bonding zone and base metal. The diffusion zone was obviously observed. When it was not finished for isothermal solidification process,the bonding zone would contain isothermal solidification zone and rapid solidification zone. Metallographic examination revealed that isothermal solidification zone was consisted of γ and γ' phase. Rapid solidification zone was consisted of two different structures,which were ternary eutectic of borides,γ and γ' phase developing at the edge of joint,binary eutectic of γ and γ' phase appearing in the portion of joint. When it was not enough for homogenization process under the condition of finishing isothermal solidification process,the bonding zone would contain isothermal solidification zone and borides at the interface. Under the conditions of relatively high welding temperature and long welding time,average tensile strength of joint was equivalent to that of parent material.展开更多
A new method based on phase difference analysis is proposed for the single-channel mixed signal separation of single-channel radar fuze.This method is used to estimate the mixing coefficients of de-noised signals thro...A new method based on phase difference analysis is proposed for the single-channel mixed signal separation of single-channel radar fuze.This method is used to estimate the mixing coefficients of de-noised signals through the cumulants of mixed signals,solve the candidate data set by the mixing coefficients and signal analytical form,and resolve the problem of vector ambiguity by analyzing the phase differences.The signal separation is realized by exchanging data of the solutions.The waveform similarity coefficients are calculated,and the time鈥攆requency distributions of separated signals are analyzed.The results show that the proposed method is effective.展开更多
In this paper, we have proposed a class of ratio-cum-product estimator for estimating population mean of study variable for single phase sampling using multi-auxiliary attributes. The expressions for mean square error...In this paper, we have proposed a class of ratio-cum-product estimator for estimating population mean of study variable for single phase sampling using multi-auxiliary attributes. The expressions for mean square error are derived. An empirical study is given to compare the performance of the estimator with existing estimators. It has been found that the ratio-cum-product estimator using multiple auxiliary attributes is more efficient than mean per unit, product and ratio estimators using one auxiliary attribute, and Product and Ratio estimators using multiple auxiliary attributes in single phase sampling.展开更多
The solution of the intermetallic phase and the homogenization of composition are important for Mg alloy biomaterials.A single-phase Mg-6Zn alloy with the average grain size of about 20μm was prepared by ECAP process...The solution of the intermetallic phase and the homogenization of composition are important for Mg alloy biomaterials.A single-phase Mg-6Zn alloy with the average grain size of about 20μm was prepared by ECAP processed for six passes at 320°C.It indicated that the ECAP could significantly promote the process of solid solution in Mg-Zn alloy.The results showed that complete dissolution of the intermetallic phase improved the corrosion resistance of Mg-6Zn alloy in 0.9%NaCl solution by turning the corrosion behavior into uniform corrosion and increased the hardness in combination with its smaller grain size.展开更多
When, in a coal mine distribution network whose neutral point is grounded by an arc suppression coil (ASC), a fault occurs in the ASC, compensation cannot be properly realized. Furthermore, it can damage the safe and ...When, in a coal mine distribution network whose neutral point is grounded by an arc suppression coil (ASC), a fault occurs in the ASC, compensation cannot be properly realized. Furthermore, it can damage the safe and reliable run of the network. We first introduce a three-phase five-column arc suppression coil (TPFCASC) and discuss its autotracking compensation theory. Then we compare the single phase to ground fault of the coal mine distribution network with an open phase fault at the TPFCASC using the Thévenin theory, the symmetrical-component method and the complex sequence network respectively. The results show that, in both types of faults, zero-sequence voltage of the network will appear and the maximum magnitude of this zero-sequence voltage is different in both faults. Based on this situation, a protection for the open phase fault at the TPFCASC should be estab-lished.展开更多
In this paper, TitaiJum dioxide (TiO2) rutile single crystal was irradiated by infrared femtosecond laser pulses with repetition rate of 250 kHz. For a P-polarized femtosecond laser, the periodic nanograting structu...In this paper, TitaiJum dioxide (TiO2) rutile single crystal was irradiated by infrared femtosecond laser pulses with repetition rate of 250 kHz. For a P-polarized femtosecond laser, the periodic nanograting structure on the ablation crater surface was formed . The periodicity is much less than the laser wavelength. The direction of nanograting alignment depends on the polarization laser beam. Micro-Raman spectra show that the intensity of Eg Raman vibrating mode of rutile phase increases and that of Alg Raman vibrating mode decreases apparently within the ablation crater. With the increase of irradiation time and laser average power, the Raman vibrating modes of anatase phase emerged. Rutile phase of TiO2 single crystal is partly transformed into anatase phase.展开更多
Most of traditional traveling wave piezoelectric transducers are driven by two phase different excitation signals,leading to a complex control system and seriously limiting their applications in industry.To overcome t...Most of traditional traveling wave piezoelectric transducers are driven by two phase different excitation signals,leading to a complex control system and seriously limiting their applications in industry.To overcome these issues,a novel traveling wave sandwich piezoelectric transducer with a single-phase drive is proposed in this study.Traveling waves are produced in two driving rings of the transducer while the longitudinal vibration is excited in its sandwich composite beam,due to the coupling property of the combined structure.This results in the production of elliptical motions in the two driving rings to achieve the drive function.An analytical model is firstly developed using the transfer matrix method to analyze the dynamic behavior of the proposed transducer.Its vibration characteristics are measured and compared with computational results to validate the effectiveness of the proposed analytical model.Besides,the driving concept of the transducer is investigated by computing the motion trajectory of surface points of the driving ring and the quality of traveling wave of the driving ring.Additionally,application example investigations on the driving effect of the proposed transducer are carried out by constructing and assembling a tracked mobile system.Experimental results indicated that 1)the assembled tracked mobile system moved in the driving frequency of 19410 Hz corresponding to its maximum mean velocity through frequency sensitivity experiments;2)motion characteristic and traction performance measurements of the system prototype presented its maximum mean velocity with 59 mm/s and its maximum stalling traction force with 1.65 N,at the excitation voltage of 500 V_(RMS).These experimental results demonstrate the feasibility of the proposed traveling wave sandwich piezoelectric transducer.展开更多
A novel method for the preparation of single-phase ammonium dimolybdate with industrial ammonium molybdate was studied. Various in- fluential factors were evaluated in the paper, including reaction temperature, reacti...A novel method for the preparation of single-phase ammonium dimolybdate with industrial ammonium molybdate was studied. Various in- fluential factors were evaluated in the paper, including reaction temperature, reaction time, initial molybdenum concentration, initial NH_3 /Mo molar ratio, and stirring speed. Under the optimum experimental conditions, the crystallization rate of product is 85.23%. The X-ray diffraction (XRD) analysis and chemical analysis show that the product is single-phase ammonium dimolybdate, and no impurity phases exist. The scanning electronic microscope (SEM) image reveals uniform particle size, good particle dispersion, and no agglomeration between particles. Meanwhile, the final pH value of acidification was investigated. The total molybdenum recovery can reach up to 99.40%, and the main phases of acidification product are the same as those of raw material with the final pH value of 1.5. This determines that the acidification product can be used as a raw material to produce single-phase ammonium dimolybdate.展开更多
为提高单相动态电压恢复器(dynamic voltage restorer,DVR)的补偿性能,提出一种基于等效基波及奇次谐波谐振器组的数字控制方法。采用可等效为一组谐振器的延时模块,能够有效抑制电网基波和谐波扰动。给出一种包含两个控制参数和一组...为提高单相动态电压恢复器(dynamic voltage restorer,DVR)的补偿性能,提出一种基于等效基波及奇次谐波谐振器组的数字控制方法。采用可等效为一组谐振器的延时模块,能够有效抑制电网基波和谐波扰动。给出一种包含两个控制参数和一组零相移陷波滤波器的结构及其设计方法,使系统在保证稳定性的同时,获得较大的谐振增益。其中,延时环节衰减系数可增加谐振器组鲁棒性;控制器比例增益可解决零相移陷波器中使用延时带来的问题;零相移陷波器组既能对消LC谐振峰,也能解决等效谐振器组高增益在高频处的稳定性问题。同时,引入电源电压和负载电流双前馈来保证响应速度,增加了对扰动的抑制能力。所提控制策略结构简单,谐波补偿能力强,动态响应快,易于实现。在2kW单相DVR实验装置上的实验结果验证了该控制方法的正确性。展开更多
A single-drop liquid phase micro-extraction procedure using 1-butyl-3-methylimidazolium hexafluorophosphate ([C4MIM][PF6]) was demonstrated for the sensitive determination of four phenols in water samples. Under the...A single-drop liquid phase micro-extraction procedure using 1-butyl-3-methylimidazolium hexafluorophosphate ([C4MIM][PF6]) was demonstrated for the sensitive determination of four phenols in water samples. Under the optimized conditions, the linear range of proposed method was excellent in the range of 0.5-100 μg·L^-1, the reproducibility (RSD, n=6) were in the range 5.4%-8.9% and detection limits (S/N=3) were 0.3, 0.3, 0.5 and 0.5 μg·L^-1 for 2, 4-dichlorophenol, 2-naphthol, 2-nitrophenol and 4-chlorophenol, respectively. The experimental results indicated that the effect of complex matrices natural water samples could be resolved with addition of sodium ethylene diamine tetracetate (EDTA) into the samples. Excellent spiked recoveries were achieved for these four phenols ranged from 86.2%-114.9 %. All these facts demonstrated that the proposed method with merits of low cost, simplicity and easy operating would be a competitive alternative procedure for the determination of such compounds at trace level.展开更多
An investigation has been made into strengthening mechanism in a single crystal nickel-base superalloy DD8 by transmission electron microscopy. The results show that the stress rupture strength of the alloy increases ...An investigation has been made into strengthening mechanism in a single crystal nickel-base superalloy DD8 by transmission electron microscopy. The results show that the stress rupture strength of the alloy increases with decreasing misfit, and the antiphase boundaries (APBs) formed in the ordered γ' phase, rather than the misfits, play a dominate role in strengthening of the single crystal Ni-base superalloy DD8.There are three kinds of mechanisms for forming the APBs which were observed in the present materials. One is mis-arrangement of the local ordered atoms in the γ' precipitates due to the local strain; the second arises from the 1/2<110> dislocations cutting into the γ', and the third is the formation of the APBs induced by the 1/2<110> matrix dislocation network. The contribution of the antiphase boundary energy to the strength of the alloy can be expressed by:where τ is the resistance to deformation provided by the APB energy; S is the long-range order degree in γ'; Tc is the transition temperature from order to disorder; f is the volume fraction of γ'; rs is the radius of γ'; b is the Burgers vector; a is the lattice constant; G is the shear modulus, and k is the proportional constant.展开更多
Superconducting La1.937Sr0.063CuO4 crystals grown by the travelling-solvent floating-zone technique were thermally treated under various temperatures and oxygen pressures for moderately adjusting the oxygen content. T...Superconducting La1.937Sr0.063CuO4 crystals grown by the travelling-solvent floating-zone technique were thermally treated under various temperatures and oxygen pressures for moderately adjusting the oxygen content. The response of intrinsic electronic property of the crystals to the change of hole density in La2-xSrxCuO4 in the vicinity of the magic doping of x= 1/16 (= 0.0625) is studied in detail by magnetic measurements under various fields up to 1 T. It is found that when the superconducting critical temperature (Tc) increases with the oxygen content, there appears also a new subtle electronic state that can be detected from the differential curves of diamagnetic susceptibility dx/dT of the crystal sample. In contrast with the intrinsic state, the new subtle electronic state is very fragile under the magnetic fields. Our results indicate that a moderate change in oxygen doping does not significantly modify the intrinsic electronic state originally existing at the magic doping level.展开更多
Single-walled carbon nanotubes(SWNTs) have a high adsorption ability and nanoscale interactions. Cellulose trisphenylcarbamates possess high enantioseparation ability in high-performance liquid chromatography(HPLC...Single-walled carbon nanotubes(SWNTs) have a high adsorption ability and nanoscale interactions. Cellulose trisphenylcarbamates possess high enantioseparation ability in high-performance liquid chromatography(HPLC). Single-walled carbon nanotubes mixed with cellulose trisphenylcarbamate are coated on the silica gel as chiral stationary phases and higher enantioseparation factors are obtained. After a single-walled carbon nanotube is linked to the 6-pesition of cellulose 2,3-bisphenylcarbamate, its enantioseparation resolution increases compared to that of the cellulose trisphenylcarbamate. It is the first time that SWNTs have been applied to enantioseparation. The results indicate that the single-walled carbon nanotubes are good promoters of chiral recognition. This method can be used to improve the enantioseparation efficiency of the polysaccharide chiral stationary phases.展开更多
Complex dynamical phenomenon was studied in the single phase H-bridge inverter which was controlled by either a peak current or a valley current. The state functions and the discrete iterative map equations were estab...Complex dynamical phenomenon was studied in the single phase H-bridge inverter which was controlled by either a peak current or a valley current. The state functions and the discrete iterative map equations were established to analyze the dynamical phenomenon in the single phase H-bridge inverter. The dynamical characteristics of the single phase H- bridge inverter, such as time domain waveform diagram, bifurcation diagram, and folding map, were obtained by using the numerical calculation when the circuit parameters varied in specific range. Moreover, the simulation results were obtained by using the OrCAD-PSpice software to validate the numerical calculation. Both the numerical calculation and the circuit simulation show that the symmetrical dynamical phenomenon occurs in the single phase H-bridge inverter controlled by the peak current or the valley current.展开更多
基金funded by National Natural Science Foundation of China, grant numbers 62335006, 62274014, 62235016, 61734006, 61835011, 61991430funded by Key Program of the Chinese Academy of Sciences, grant numbers XDB43000000, QYZDJSSW-JSC027Beijing Municipal Science & Technology Commission, grant number Z221100002722018
文摘We demonstrated a scheme of phase-locked terahertz quantum cascade lasers(THz QCLs)array,with a single-mode pulse power of 108 mW at 13 K.The device utilizes a Talbot cavity to achieve phase locking among five ridge lasers with first-order buried distributed feedback(DFB)grating,resulting in nearly five times amplification of the single-mode power.Due to the optimum length of Talbot cavity depends on wavelength,the combination of Talbot cavity with the DFB grating leads to better power amplification than the combination with multimode Fabry-Perot(F-P)cavities.The Talbot cavity facet reflects light back to the ridge array direction and achieves self-imaging in the array,enabling phase-locked operation of ridges.We set the spacing between adjacent elements to be 220μm,much larger than the free-space wavelength,ensuring the operation of the fundamental supermode throughout the laser's dynamic range and obtaining a high-brightness far-field distribution.This scheme provides a new approach for enhancing the single-mode power of THz QCLs.
文摘The generation of electricity based on renewable energy sources,parti-cularly Photovoltaic(PV)system has been greatly increased and it is simply insti-gated for both domestic and commercial uses.The power generated from the PV system is erratic and hence there is a need for an efficient converter to perform the extraction of maximum power.An improved interleaved Single-ended Primary Inductor-Converter(SEPIC)converter is employed in proposed work to extricate most of power from renewable source.This proposed converter minimizes ripples,reduces electromagnetic interference due tofilter elements and the contin-uous input current improves the power output of PV panel.A Crow Search Algo-rithm(CSA)based Proportional Integral(PI)controller is utilized for controlling the converter switches effectively by optimizing the parameters of PI controller.The optimized PI controller reduces ripples present in Direct Current(DC)vol-tage,maintains constant voltage at proposed converter output and reduces over-shoots with minimum settling and rise time.This voltage is given to single phase grid via 1�Voltage Source Inverter(VSI).The command pulses of 1�VSI are produced by simple PI controller.The response of the proposed converter is thus improved with less input current.After implementing CSA based PI the efficiency of proposed converter obtained is 96%and the Total Harmonic Distor-tion(THD)is found to be 2:4%.The dynamics and closed loop operation is designed and modeled using MATLAB Simulink tool and its behavior is performed.
文摘Two experimental single crystal superalloys, the Ru-free alloy and the Ru-containing alloy with [001 ] orientation, were cast in a directionally solidified furnace, while other alloying element contents were kept unchanged. The effects of Ru on the microstructure and phase stability of the single crystal superalloy were investigated, y' directional coarsening and rafting were observed in the Ru-free alloy and Ru-containing alloy after long-term aging at 1070~C for 800 h. Needle-shaped o topologically close packed (TCP) phases precipitated and grew along the fixed direction in both the alloys. The precipitating rate and volume fraction of TCP phases decreased significantly by adding Ru. The compositions ofy and y' phases measured using an energy-dispersive X-ray spectroscope (EDS) in transmission electron microscopy (TEM) analysis showed that the addition of Ru lessened the partition ratio of TCP forming elements, Re, W and Mo, and decreased the satu- ration degrees of these elements in y phase, which can enable the Ru-containing alloy to be more resistant to the formation of TCP phases. It is indicated that the addition of Ru to the Ni-based single crystal superalloy with high content of the refractory alloying element can enhance phase stability.
基金This work was supported by the National Natural Science Foundation of China under grant No. 50171043 and the Open Foundation from State Key Laboratory of Solidification Process-ing.
文摘Solidification structure variation of single phase alloy with undercooling prior to nucleation has been widely studied. The progress, especially during the last decade, is reviewed so as to give a comprehensive knowledge for it, in which the emphases are laid on the structure evolution mechanism and the potential application. Lastly, the future interesting subjects are presented.
文摘Microstructure of transient liquid phase( TLP) diffusion bonded a third generation single crystal superalloy joint was investigated using scanning electron microscopy( SEM),and mechanical properties test of joint was carried out,for obtaining relationship between microstructure and mechanical properties of joint. The results showed that the joint contained bonding zone and base metal. The diffusion zone was obviously observed. When it was not finished for isothermal solidification process,the bonding zone would contain isothermal solidification zone and rapid solidification zone. Metallographic examination revealed that isothermal solidification zone was consisted of γ and γ' phase. Rapid solidification zone was consisted of two different structures,which were ternary eutectic of borides,γ and γ' phase developing at the edge of joint,binary eutectic of γ and γ' phase appearing in the portion of joint. When it was not enough for homogenization process under the condition of finishing isothermal solidification process,the bonding zone would contain isothermal solidification zone and borides at the interface. Under the conditions of relatively high welding temperature and long welding time,average tensile strength of joint was equivalent to that of parent material.
文摘A new method based on phase difference analysis is proposed for the single-channel mixed signal separation of single-channel radar fuze.This method is used to estimate the mixing coefficients of de-noised signals through the cumulants of mixed signals,solve the candidate data set by the mixing coefficients and signal analytical form,and resolve the problem of vector ambiguity by analyzing the phase differences.The signal separation is realized by exchanging data of the solutions.The waveform similarity coefficients are calculated,and the time鈥攆requency distributions of separated signals are analyzed.The results show that the proposed method is effective.
文摘In this paper, we have proposed a class of ratio-cum-product estimator for estimating population mean of study variable for single phase sampling using multi-auxiliary attributes. The expressions for mean square error are derived. An empirical study is given to compare the performance of the estimator with existing estimators. It has been found that the ratio-cum-product estimator using multiple auxiliary attributes is more efficient than mean per unit, product and ratio estimators using one auxiliary attribute, and Product and Ratio estimators using multiple auxiliary attributes in single phase sampling.
基金The authors gratefully acknowledge financial support from the National Natural Science Foundation of China(Grant no.51301151)Jiangsu Province Natural Science Foundation of China(Grant nos.BK20130447 and BK20160869).
文摘The solution of the intermetallic phase and the homogenization of composition are important for Mg alloy biomaterials.A single-phase Mg-6Zn alloy with the average grain size of about 20μm was prepared by ECAP processed for six passes at 320°C.It indicated that the ECAP could significantly promote the process of solid solution in Mg-Zn alloy.The results showed that complete dissolution of the intermetallic phase improved the corrosion resistance of Mg-6Zn alloy in 0.9%NaCl solution by turning the corrosion behavior into uniform corrosion and increased the hardness in combination with its smaller grain size.
文摘When, in a coal mine distribution network whose neutral point is grounded by an arc suppression coil (ASC), a fault occurs in the ASC, compensation cannot be properly realized. Furthermore, it can damage the safe and reliable run of the network. We first introduce a three-phase five-column arc suppression coil (TPFCASC) and discuss its autotracking compensation theory. Then we compare the single phase to ground fault of the coal mine distribution network with an open phase fault at the TPFCASC using the Thévenin theory, the symmetrical-component method and the complex sequence network respectively. The results show that, in both types of faults, zero-sequence voltage of the network will appear and the maximum magnitude of this zero-sequence voltage is different in both faults. Based on this situation, a protection for the open phase fault at the TPFCASC should be estab-lished.
基金Project supported by Shanghai Leading Academic Discipline Project, China (Grant No T0104), the Shanghai Nano-technology Promotion Center and Science & Technology of Shanghai Municipality, China (Grant No 0652nm005), Science Foundation of Shanghai Municipal Commission Education and Science and Technology Commission of Shanghai Municipal, China (Grant No 06PJ14042).
文摘In this paper, TitaiJum dioxide (TiO2) rutile single crystal was irradiated by infrared femtosecond laser pulses with repetition rate of 250 kHz. For a P-polarized femtosecond laser, the periodic nanograting structure on the ablation crater surface was formed . The periodicity is much less than the laser wavelength. The direction of nanograting alignment depends on the polarization laser beam. Micro-Raman spectra show that the intensity of Eg Raman vibrating mode of rutile phase increases and that of Alg Raman vibrating mode decreases apparently within the ablation crater. With the increase of irradiation time and laser average power, the Raman vibrating modes of anatase phase emerged. Rutile phase of TiO2 single crystal is partly transformed into anatase phase.
基金Supported by the National Science Foundation of China(Grants Nos.51905262 and U2037603)the Natural Science Foundation of Jiangsu Province(Grant No.BK20190398)the State Key Laboratory of Mechanical System and Vibration(Grant No.MSV202011).
文摘Most of traditional traveling wave piezoelectric transducers are driven by two phase different excitation signals,leading to a complex control system and seriously limiting their applications in industry.To overcome these issues,a novel traveling wave sandwich piezoelectric transducer with a single-phase drive is proposed in this study.Traveling waves are produced in two driving rings of the transducer while the longitudinal vibration is excited in its sandwich composite beam,due to the coupling property of the combined structure.This results in the production of elliptical motions in the two driving rings to achieve the drive function.An analytical model is firstly developed using the transfer matrix method to analyze the dynamic behavior of the proposed transducer.Its vibration characteristics are measured and compared with computational results to validate the effectiveness of the proposed analytical model.Besides,the driving concept of the transducer is investigated by computing the motion trajectory of surface points of the driving ring and the quality of traveling wave of the driving ring.Additionally,application example investigations on the driving effect of the proposed transducer are carried out by constructing and assembling a tracked mobile system.Experimental results indicated that 1)the assembled tracked mobile system moved in the driving frequency of 19410 Hz corresponding to its maximum mean velocity through frequency sensitivity experiments;2)motion characteristic and traction performance measurements of the system prototype presented its maximum mean velocity with 59 mm/s and its maximum stalling traction force with 1.65 N,at the excitation voltage of 500 V_(RMS).These experimental results demonstrate the feasibility of the proposed traveling wave sandwich piezoelectric transducer.
基金supported by the National Natural Science Foundation of China(No.51072233)
文摘A novel method for the preparation of single-phase ammonium dimolybdate with industrial ammonium molybdate was studied. Various in- fluential factors were evaluated in the paper, including reaction temperature, reaction time, initial molybdenum concentration, initial NH_3 /Mo molar ratio, and stirring speed. Under the optimum experimental conditions, the crystallization rate of product is 85.23%. The X-ray diffraction (XRD) analysis and chemical analysis show that the product is single-phase ammonium dimolybdate, and no impurity phases exist. The scanning electronic microscope (SEM) image reveals uniform particle size, good particle dispersion, and no agglomeration between particles. Meanwhile, the final pH value of acidification was investigated. The total molybdenum recovery can reach up to 99.40%, and the main phases of acidification product are the same as those of raw material with the final pH value of 1.5. This determines that the acidification product can be used as a raw material to produce single-phase ammonium dimolybdate.
文摘为提高单相动态电压恢复器(dynamic voltage restorer,DVR)的补偿性能,提出一种基于等效基波及奇次谐波谐振器组的数字控制方法。采用可等效为一组谐振器的延时模块,能够有效抑制电网基波和谐波扰动。给出一种包含两个控制参数和一组零相移陷波滤波器的结构及其设计方法,使系统在保证稳定性的同时,获得较大的谐振增益。其中,延时环节衰减系数可增加谐振器组鲁棒性;控制器比例增益可解决零相移陷波器中使用延时带来的问题;零相移陷波器组既能对消LC谐振峰,也能解决等效谐振器组高增益在高频处的稳定性问题。同时,引入电源电压和负载电流双前馈来保证响应速度,增加了对扰动的抑制能力。所提控制策略结构简单,谐波补偿能力强,动态响应快,易于实现。在2kW单相DVR实验装置上的实验结果验证了该控制方法的正确性。
文摘A single-drop liquid phase micro-extraction procedure using 1-butyl-3-methylimidazolium hexafluorophosphate ([C4MIM][PF6]) was demonstrated for the sensitive determination of four phenols in water samples. Under the optimized conditions, the linear range of proposed method was excellent in the range of 0.5-100 μg·L^-1, the reproducibility (RSD, n=6) were in the range 5.4%-8.9% and detection limits (S/N=3) were 0.3, 0.3, 0.5 and 0.5 μg·L^-1 for 2, 4-dichlorophenol, 2-naphthol, 2-nitrophenol and 4-chlorophenol, respectively. The experimental results indicated that the effect of complex matrices natural water samples could be resolved with addition of sodium ethylene diamine tetracetate (EDTA) into the samples. Excellent spiked recoveries were achieved for these four phenols ranged from 86.2%-114.9 %. All these facts demonstrated that the proposed method with merits of low cost, simplicity and easy operating would be a competitive alternative procedure for the determination of such compounds at trace level.
文摘An investigation has been made into strengthening mechanism in a single crystal nickel-base superalloy DD8 by transmission electron microscopy. The results show that the stress rupture strength of the alloy increases with decreasing misfit, and the antiphase boundaries (APBs) formed in the ordered γ' phase, rather than the misfits, play a dominate role in strengthening of the single crystal Ni-base superalloy DD8.There are three kinds of mechanisms for forming the APBs which were observed in the present materials. One is mis-arrangement of the local ordered atoms in the γ' precipitates due to the local strain; the second arises from the 1/2<110> dislocations cutting into the γ', and the third is the formation of the APBs induced by the 1/2<110> matrix dislocation network. The contribution of the antiphase boundary energy to the strength of the alloy can be expressed by:where τ is the resistance to deformation provided by the APB energy; S is the long-range order degree in γ'; Tc is the transition temperature from order to disorder; f is the volume fraction of γ'; rs is the radius of γ'; b is the Burgers vector; a is the lattice constant; G is the shear modulus, and k is the proportional constant.
基金Project supported by the Ministry of Science and Technology of China (973 project Grant No 2006CB0L0302)the National Natural Science Foundation of China (Grant No 10574149)Chinese Academy of Sciences (Grant No KJCX2-SW-W18)
文摘Superconducting La1.937Sr0.063CuO4 crystals grown by the travelling-solvent floating-zone technique were thermally treated under various temperatures and oxygen pressures for moderately adjusting the oxygen content. The response of intrinsic electronic property of the crystals to the change of hole density in La2-xSrxCuO4 in the vicinity of the magic doping of x= 1/16 (= 0.0625) is studied in detail by magnetic measurements under various fields up to 1 T. It is found that when the superconducting critical temperature (Tc) increases with the oxygen content, there appears also a new subtle electronic state that can be detected from the differential curves of diamagnetic susceptibility dx/dT of the crystal sample. In contrast with the intrinsic state, the new subtle electronic state is very fragile under the magnetic fields. Our results indicate that a moderate change in oxygen doping does not significantly modify the intrinsic electronic state originally existing at the magic doping level.
基金Supported by the National Natural Science Foundation of China(No.30160092)the Natural Science Foundation of Yunnan Province,China(No.2005E0006Z).
文摘Single-walled carbon nanotubes(SWNTs) have a high adsorption ability and nanoscale interactions. Cellulose trisphenylcarbamates possess high enantioseparation ability in high-performance liquid chromatography(HPLC). Single-walled carbon nanotubes mixed with cellulose trisphenylcarbamate are coated on the silica gel as chiral stationary phases and higher enantioseparation factors are obtained. After a single-walled carbon nanotube is linked to the 6-pesition of cellulose 2,3-bisphenylcarbamate, its enantioseparation resolution increases compared to that of the cellulose trisphenylcarbamate. It is the first time that SWNTs have been applied to enantioseparation. The results indicate that the single-walled carbon nanotubes are good promoters of chiral recognition. This method can be used to improve the enantioseparation efficiency of the polysaccharide chiral stationary phases.
基金Project supported by the National Natural Science Foundation of China(Grant No.51107016)the National Basic Research Program of China(Grant No.2013CB035605)the Postdoctoral Science Research Developmental Foundation of Heilongjiang Province,China(Grant No.LHB-Q12086)
文摘Complex dynamical phenomenon was studied in the single phase H-bridge inverter which was controlled by either a peak current or a valley current. The state functions and the discrete iterative map equations were established to analyze the dynamical phenomenon in the single phase H-bridge inverter. The dynamical characteristics of the single phase H- bridge inverter, such as time domain waveform diagram, bifurcation diagram, and folding map, were obtained by using the numerical calculation when the circuit parameters varied in specific range. Moreover, the simulation results were obtained by using the OrCAD-PSpice software to validate the numerical calculation. Both the numerical calculation and the circuit simulation show that the symmetrical dynamical phenomenon occurs in the single phase H-bridge inverter controlled by the peak current or the valley current.