The semi-solid slurry of A356 alloy, which is grain-refined by Al-Ti-B master alloy, is prepared by low superheat pouring and slight electromagnetic stirring. The effects of grain refining on the morphology and the gr...The semi-solid slurry of A356 alloy, which is grain-refined by Al-Ti-B master alloy, is prepared by low superheat pouring and slight electromagnetic stirring. The effects of grain refining on the morphology and the grain size of the primary α phase in the slurry manufactured are researched. The results indicate that the slurry with particle-like and rosette-like primary α phases can be prepared by low superheat pouring and slight electromagnetic stirring from liquid A356 alloy grain-refined, in which the pouring temperature can be suitably raised. Compared with the A356 samples without grain refining, the grain size and particle morphology of primary α phase as well as the distribution of the grain with particle-like or rosette-like along radial in the ingot in A356 are markedly improved by grain refining.展开更多
The grain growth behavior in reactive spray formed 7075+2.91 vol percent TiCAl alloy was studied and compared with that of spray formed 7075 Al alloy at semi-solid state. Theeffects of in-situ TiC particles on the mic...The grain growth behavior in reactive spray formed 7075+2.91 vol percent TiCAl alloy was studied and compared with that of spray formed 7075 Al alloy at semi-solid state. Theeffects of in-situ TiC particles on the microstructure of spray formed 7075 Al alloy were alsoinvestigated. The specimens were heat-treated isothermally at various temperatures between thesolidus and liquidus of 7075 Al alloy for times in the range of 10-60 min, then quenched in water.The microstructure of reheated specimens was characterized using scanning electron microscopy andoptical microscopy. The grain size was measured using a mean linear intercept method. Results showthat the in-situ TiC particles can effectively retard grain growth and refine the grain at a limitedsize. The grain growth exponent in Arrhenius equation increases from 2 to 3, which indicates thatthe in-situ TiC particles have the significant pinning effect on grain coarsening in the semi-solidstate.展开更多
The microstructure and room-temperature tensile properties of Ti14,a new α＋Ti2Cu alloy,were investigated after conventional forging at 950°C and semi-solid forging at 1000 and 1050°C,respectively.Results s...The microstructure and room-temperature tensile properties of Ti14,a new α＋Ti2Cu alloy,were investigated after conventional forging at 950°C and semi-solid forging at 1000 and 1050°C,respectively.Results show that coarse grains and grain boundaries are obtained in the semi-solid alloys.The coarse grain boundaries are attributed to Ti2Cu phase precipitations occurred on the grain boundaries during the solidification.It is found that more Ti2Cu phase precipitates on the grain boundaries at a higher semi-solid forging temperature,which forms precipitated zones and coarsens the grain boundaries.Tensile tests exhibit high strength and low ductility for the semi-solid forged alloys,especially after forging at 1000°C.Fracture analysis reveals the evidence of ductile failure mechanisms for the conventional forged alloy and cleavage fracture mechanisms for the alloy after semi-solid forging at 1050°C.展开更多
The role of Nd solid-solution and grain-boundary segregation in binary NiAl alloy was studied based on microhardness and compressive macrostrain. X-ray and Auger spectra studies indicate that Nd not only is soluble in...The role of Nd solid-solution and grain-boundary segregation in binary NiAl alloy was studied based on microhardness and compressive macrostrain. X-ray and Auger spectra studies indicate that Nd not only is soluble in grain interiors, but also segregates to the grain boundaries. Nd solid-solution induces an increase of the microhardness from 269 to 290 HV in grain interiors and segregation results in an enhancement of hardness from 252 to 342 HV on grain boundaries. Thus, the cohesion of grain boundaries is enhanced by Nd segregation, which make the alloy doped with 0.05 wt pct Nd exhibit more compressive microstrain, i.e. the higher the compressive ductility at room temperature, the better the final surface condition at elevated temperature. Finally, a discussion was made on the reason that Nd strengthens the grain boundaries in NiAl intermetallic alloy.展开更多
The instable combustion or oscillation combustion which occurs in three high capacity solid rocket motors using high energy composite propellant with finocyl grain is studied. The reasons of the acoustic combustion in...The instable combustion or oscillation combustion which occurs in three high capacity solid rocket motors using high energy composite propellant with finocyl grain is studied. The reasons of the acoustic combustion instability are also discussed. Three engineering methods that can eliminate combustion instability are proposed and discussed. The study shows that the combustion instability mainly depends on the propellant grain shape and nozzle structure. Some measures to reduce the acoustic energy and mass generation rate of combustion gas can be adopted. The test results indicate that the modified rocket motors can significantly eliminate the instable combustion and improve the motor internal ballistic performance.展开更多
Through studying on the heating process of titanium microalloyed steels, the influence of heating temperature on the austenite grain size and the solid dissolution, precipitation law of Ti microalloying element were a...Through studying on the heating process of titanium microalloyed steels, the influence of heating temperature on the austenite grain size and the solid dissolution, precipitation law of Ti microalloying element were analyzed, and the results showed that, the austenite grain size increased with the increase of heating temperature, When the heating temperature reached 1050°C and 1250°C, the austenite grains appeared the obvious coarsening process twice. TiC particles dissolved gradually as the heating temperature increased. When the heating temperature rose to 1100°C, TiC particles disappeared basically, When the heating temperature rose to 1250°C, TiN particles began to be dissolved and grow up.展开更多
基金financially supported by National High Technical Research and Development Program of China(No.G2002AA336080)National Natural Science Foundation of China(No.50374012)Natural Science Foundation of Jiangxi Province(No.0650047).
文摘The semi-solid slurry of A356 alloy, which is grain-refined by Al-Ti-B master alloy, is prepared by low superheat pouring and slight electromagnetic stirring. The effects of grain refining on the morphology and the grain size of the primary α phase in the slurry manufactured are researched. The results indicate that the slurry with particle-like and rosette-like primary α phases can be prepared by low superheat pouring and slight electromagnetic stirring from liquid A356 alloy grain-refined, in which the pouring temperature can be suitably raised. Compared with the A356 samples without grain refining, the grain size and particle morphology of primary α phase as well as the distribution of the grain with particle-like or rosette-like along radial in the ingot in A356 are markedly improved by grain refining.
基金This work was financially supported by the National Natural Science Foundation of China (No.50171010)
文摘The grain growth behavior in reactive spray formed 7075+2.91 vol percent TiCAl alloy was studied and compared with that of spray formed 7075 Al alloy at semi-solid state. Theeffects of in-situ TiC particles on the microstructure of spray formed 7075 Al alloy were alsoinvestigated. The specimens were heat-treated isothermally at various temperatures between thesolidus and liquidus of 7075 Al alloy for times in the range of 10-60 min, then quenched in water.The microstructure of reheated specimens was characterized using scanning electron microscopy andoptical microscopy. The grain size was measured using a mean linear intercept method. Results showthat the in-situ TiC particles can effectively retard grain growth and refine the grain at a limitedsize. The grain growth exponent in Arrhenius equation increases from 2 to 3, which indicates thatthe in-situ TiC particles have the significant pinning effect on grain coarsening in the semi-solidstate.
基金supported by the Major State Basic Research and Development Program of China (No.2007CB613807)the Special Fund for Basic Scientific Research of Central Colleges, Chan'an University (No.CHD2010JC115)
文摘The microstructure and room-temperature tensile properties of Ti14,a new α＋Ti2Cu alloy,were investigated after conventional forging at 950°C and semi-solid forging at 1000 and 1050°C,respectively.Results show that coarse grains and grain boundaries are obtained in the semi-solid alloys.The coarse grain boundaries are attributed to Ti2Cu phase precipitations occurred on the grain boundaries during the solidification.It is found that more Ti2Cu phase precipitates on the grain boundaries at a higher semi-solid forging temperature,which forms precipitated zones and coarsens the grain boundaries.Tensile tests exhibit high strength and low ductility for the semi-solid forged alloys,especially after forging at 1000°C.Fracture analysis reveals the evidence of ductile failure mechanisms for the conventional forged alloy and cleavage fracture mechanisms for the alloy after semi-solid forging at 1050°C.
文摘The role of Nd solid-solution and grain-boundary segregation in binary NiAl alloy was studied based on microhardness and compressive macrostrain. X-ray and Auger spectra studies indicate that Nd not only is soluble in grain interiors, but also segregates to the grain boundaries. Nd solid-solution induces an increase of the microhardness from 269 to 290 HV in grain interiors and segregation results in an enhancement of hardness from 252 to 342 HV on grain boundaries. Thus, the cohesion of grain boundaries is enhanced by Nd segregation, which make the alloy doped with 0.05 wt pct Nd exhibit more compressive microstrain, i.e. the higher the compressive ductility at room temperature, the better the final surface condition at elevated temperature. Finally, a discussion was made on the reason that Nd strengthens the grain boundaries in NiAl intermetallic alloy.
文摘The instable combustion or oscillation combustion which occurs in three high capacity solid rocket motors using high energy composite propellant with finocyl grain is studied. The reasons of the acoustic combustion instability are also discussed. Three engineering methods that can eliminate combustion instability are proposed and discussed. The study shows that the combustion instability mainly depends on the propellant grain shape and nozzle structure. Some measures to reduce the acoustic energy and mass generation rate of combustion gas can be adopted. The test results indicate that the modified rocket motors can significantly eliminate the instable combustion and improve the motor internal ballistic performance.
文摘Through studying on the heating process of titanium microalloyed steels, the influence of heating temperature on the austenite grain size and the solid dissolution, precipitation law of Ti microalloying element were analyzed, and the results showed that, the austenite grain size increased with the increase of heating temperature, When the heating temperature reached 1050°C and 1250°C, the austenite grains appeared the obvious coarsening process twice. TiC particles dissolved gradually as the heating temperature increased. When the heating temperature rose to 1100°C, TiC particles disappeared basically, When the heating temperature rose to 1250°C, TiN particles began to be dissolved and grow up.
