Aluminum alloy tubes were prepared by tube spinning.The intergranular and electrochemical corrosion tests were used to investigate the intergranular corrosion behavior of the 5A06 aluminum alloy blank sample and the s...Aluminum alloy tubes were prepared by tube spinning.The intergranular and electrochemical corrosion tests were used to investigate the intergranular corrosion behavior of the 5A06 aluminum alloy blank sample and the spinning sample.Results showed that the intergranular corrosion resistance of the spinning sample was higher than that of the blank sample.In addition,the electrochemical corrosion resistance of the spinning sample was higher than that of the blank sample.The EDS maps indicated a uniform element distribution pattern of aluminum and magnesium.Moreover,the phase composition and lattice constant of the samples were obtained by XRD analysis.The differences in microstructure between the aluminum alloy subjected to the spinning process and the untreated aluminum alloy were determined by EBSD.The differences were mainly attributed to the complex interactions among grain size,dislocations and grain boundaries.展开更多
Spinning has a significant influence on all textile processes. Combinations of all the capital equipment display the process’ critical condition. By transforming unprocessed fibers into carded sliver and yarn, the ca...Spinning has a significant influence on all textile processes. Combinations of all the capital equipment display the process’ critical condition. By transforming unprocessed fibers into carded sliver and yarn, the carding machine serves a critical role in the textile industry. The carding machine’s licker-in and flat speeds are crucial operational factors that have a big influence on the finished goods’ quality. The purpose of this study is to examine the link between licker-in and flat speeds and how they affect the yarn and carded sliver quality. A thorough experimental examination on a carding machine was carried out to accomplish this. The carded sliver and yarn produced after experimenting with different licker-in and flat speed combinations were assessed for important quality factors including evenness, strength, and flaws. To account for changes in material qualities and machine settings, the study also took into consideration the impact of various fiber kinds and processing circumstances. The findings of the investigation showed a direct relationship between the quality of the carded sliver and yarn and the licker-in and flat speeds. Within a limited range, greater licker-in speeds were shown to increase carding efficiency and decrease fiber tangling. On the other hand, extremely high speeds led to more fiber breakage and neps. Higher flat speeds, on the other hand, helped to enhance fiber alignment, which increased the evenness and strength of the carded sliver and yarn. Additionally, it was discovered that the ideal blend of licker-in and flat rates varied based on the fiber type and processing circumstances. When being carded, various fibers displayed distinctive behaviors that necessitated adjusting the operating settings in order to provide the necessary quality results. The study also determined the crucial speed ratios between the licker-in and flat speeds that reduced fiber breakage and increased the caliber of the finished goods. The results of this study offer useful information for textile producers and process engineers to improve the quality of carded sliver and yarn while maximizing the performance of carding machines. Operators may choose machine settings and parameter adjustments wisely by knowing the impacts of licker-in and flat speeds, which will increase textile industry efficiency, productivity, and product quality.展开更多
Spinning has a significant influence on all textile processes. Combinations of all the capital equipment display the process’ critical condition. By transforming unprocessed fibers into carded sliver and yarn, the ca...Spinning has a significant influence on all textile processes. Combinations of all the capital equipment display the process’ critical condition. By transforming unprocessed fibers into carded sliver and yarn, the carding machine serves a critical role in the textile industry. The carding machine’s licker-in and flat speeds are crucial operational factors that have a big influence on the finished goods’ quality. The purpose of this study is to examine the link between licker-in and flat speeds and how they affect the yarn and carded sliver quality. A thorough experimental examination on a carding machine was carried out to accomplish this. The carded sliver and yarn produced after experimenting with different licker-in and flat speed combinations were assessed for important quality factors including evenness, strength, and flaws. To account for changes in material qualities and machine settings, the study also took into consideration the impact of various fiber kinds and processing circumstances. The findings of the investigation showed a direct relationship between the quality of the carded sliver and yarn and the licker-in and flat speeds. Within a limited range, greater licker-in speeds were shown to increase carding efficiency and decrease fiber tangling. On the other hand, extremely high speeds led to more fiber breakage and neps. Higher flat speeds, on the other hand, helped to enhance fiber alignment, which increased the evenness and strength of the carded sliver and yarn. Additionally, it was discovered that the ideal blend of licker-in and flat rates varied based on the fiber type and processing circumstances. When being carded, various fibers displayed distinctive behaviors that necessitated adjusting the operating settings in order to provide the necessary quality results. The study also determined the crucial speed ratios between the licker-in and flat speeds that reduced fiber breakage and increased the caliber of the finished goods. The results of this study offer useful information for textile producers and process engineers to improve the quality of carded sliver and yarn while maximizing the performance of carding machines. Operators may choose machine settings and parameter adjustments wisely by knowing the impacts of licker-in and flat speeds, which will increase textile industry efficiency, productivity, and product quality.展开更多
Finite element method is used to simulate the high-speed melt spinning process, based on the equation system proposed by Doufas et al. Calculation predicts a neck-like deformation, as well as the related profiles of v...Finite element method is used to simulate the high-speed melt spinning process, based on the equation system proposed by Doufas et al. Calculation predicts a neck-like deformation, as well as the related profiles of velocity, diameter, temperature, chain orientation, and crystallinity in the fiber spinning process. Considering combined effects on the process such as flow-induced crystallization, viscoelasticity, filament cooling, air drag, inertia, surface tension and gravity, the simulated material flow behaviors are consistent with those observed for semi-crystalline polymers under various spinning conditions, The structure change of polymer coils in the necking region described by the evolution of conformation tensor is also investigated. Based on the relaxation mechanism of macromolecules in flow field different types of morphology change of polymer chains before and in the neck are proposed, giving a complete prospect of structure evolution and crystallization of semi-crystalline polymer in the high speed fiber spinning process.展开更多
Uncontrolled residual stresses have significant effects on the service time and defects of the spun parts.Nowadays,X-Ray Diffraction(XRD)method has been widely used in the residual stress measurement of industry produ...Uncontrolled residual stresses have significant effects on the service time and defects of the spun parts.Nowadays,X-Ray Diffraction(XRD)method has been widely used in the residual stress measurement of industry products with different forming processes.The calculated residual stress is usually obtained from the data fitting slope of strain and angle with Ordinary Least Squares(OLS)method.But this fitting method is not always suitable for the big fluctuant data.In this paper,the Weighted Least Square(WLS)method is used for the data fitting and compared with the OLS method.The nickel-based superalloy GH3030 and iron-based superalloy GH1140 are applied in the multi-pass cold spinning experiments.The residual stress distributions of normal,potential crack and wrinkle workpieces are discussed with the grain structure.The results show that WLS method has better goodness of fit compared with OLS method.The residual stress distributions have special relationship with potential crack,wrinkle workpiece and grain structure.展开更多
Competings or frustrated interactions are common for condensed matter systems. In consideration of the effect of dipole–dipole interaction, the static properties of square lattice spin systems are investigated using ...Competings or frustrated interactions are common for condensed matter systems. In consideration of the effect of dipole–dipole interaction, the static properties of square lattice spin systems are investigated using the Wang–Landau algorithm. The dynamic hysteresis is also simulated using the Monte Carlo(MC) method. The step-like magnetization under a DC magnetic field and two distinct peaks in hysteresis dispersion under an AC magnetic field are observed. Then, the formation of the properties of the frustrated dipolar array are discussed.展开更多
The effects of spinning deformation and subsequent heat treatments on the mechanical properties and microstructure of 18Ni Co-free Maraging steel (T250) tube were evaluated comparatively with the perform. An obvious...The effects of spinning deformation and subsequent heat treatments on the mechanical properties and microstructure of 18Ni Co-free Maraging steel (T250) tube were evaluated comparatively with the perform. An obvious radial shrinkage is detected in spun tubes after heat treatment and the magnitude of the shrinkage induced by solution treatment is almost the same as that by aging. Plastic deformation during spinning elongated the grains severely in the direction of metal flow. The solution treatment resulted in a drastically refined grain and recrystallised microstructure, removing the effect of plastic deformation, relieving the tangential residual stress and strain and improving hardness. Subsequent aging obtained a tempered microstructure, enhancing hardness values strikingly for precipitation strengthening. XRD (X-ray diffraction) analysis indicated that the reversed austenite formed in a plate-like along the grain boundaries and the volume fraction of austenite in spun tube was more than double that in the preform. These results imply that the residual stress and stain induced by spinning process and reversed austenite forming during aging might have the similar contribution to the radical shrinkage.展开更多
A series of polyamic acid copolymers(co-PAAs) containing phosphorous groups in the side chains were synthesized from [2,5-bis(4-aminophenoxy) phenyl] diphenylphosphine oxide(DATPPO) and 4,4′-oxydianiline(ODA) with 3,...A series of polyamic acid copolymers(co-PAAs) containing phosphorous groups in the side chains were synthesized from [2,5-bis(4-aminophenoxy) phenyl] diphenylphosphine oxide(DATPPO) and 4,4′-oxydianiline(ODA) with 3,3′,4,4′-biphenyltetracarboxylic dianhydride(s-BPDA) through the polycondensation in N,N′-dimethyacetamide(DMAc). The co-PAA solutions were spun into fibers by a dry-jet wet spinning process followed by thermal imidization to obtain co-polyimide(co-PI) fibers. FTIR spectra and elemental analysis confirmed the chemical structure of PI fibers. SEM results indicated that the resulting PI fibers had a smooth and dense surface, a uniform and circle-shape diameter. The thermogravimetric measurements showed that with the increase of DATPPO content, the resulting PI fibers possessed high decomposition temperature and residual char yield, indicating that the PI fibers had good thermal stability. The corresponding limiting oxygen index(LOI) values from the experiment results showed that the co-PI fibers possessed good flame-retardant property. Furthermore, the mechanical properties of the co-PI fibers were investigated systematically. When the DATPPO content increased, the tensile strength and initial modulus of the co-PI fibers decreased. However, the mechanical properties were improved by increasing the draw ratio of the fibers. When the draw ratio was up to 2.5, the tensile strength and initial modulus of the co-PI fibers reached up to 0.64 and 10.02 GPa, respectively. The WAXD results showed that the order degree of amorphous matter increased with increased stretching. In addition, the SAXS results displayed that valuably drawing the fibers could eliminate the voids inside and lead to better mechanical property. WAXD revealed that the orientation of the amorphous polymer influenced the mechanical properties of the fibers.展开更多
基金Funded by the National Natural Science Foundation of China(No.51802189)the Shanghai Lingang Innovation Program(No.SH-LG-GK-2020-28)。
文摘Aluminum alloy tubes were prepared by tube spinning.The intergranular and electrochemical corrosion tests were used to investigate the intergranular corrosion behavior of the 5A06 aluminum alloy blank sample and the spinning sample.Results showed that the intergranular corrosion resistance of the spinning sample was higher than that of the blank sample.In addition,the electrochemical corrosion resistance of the spinning sample was higher than that of the blank sample.The EDS maps indicated a uniform element distribution pattern of aluminum and magnesium.Moreover,the phase composition and lattice constant of the samples were obtained by XRD analysis.The differences in microstructure between the aluminum alloy subjected to the spinning process and the untreated aluminum alloy were determined by EBSD.The differences were mainly attributed to the complex interactions among grain size,dislocations and grain boundaries.
文摘Spinning has a significant influence on all textile processes. Combinations of all the capital equipment display the process’ critical condition. By transforming unprocessed fibers into carded sliver and yarn, the carding machine serves a critical role in the textile industry. The carding machine’s licker-in and flat speeds are crucial operational factors that have a big influence on the finished goods’ quality. The purpose of this study is to examine the link between licker-in and flat speeds and how they affect the yarn and carded sliver quality. A thorough experimental examination on a carding machine was carried out to accomplish this. The carded sliver and yarn produced after experimenting with different licker-in and flat speed combinations were assessed for important quality factors including evenness, strength, and flaws. To account for changes in material qualities and machine settings, the study also took into consideration the impact of various fiber kinds and processing circumstances. The findings of the investigation showed a direct relationship between the quality of the carded sliver and yarn and the licker-in and flat speeds. Within a limited range, greater licker-in speeds were shown to increase carding efficiency and decrease fiber tangling. On the other hand, extremely high speeds led to more fiber breakage and neps. Higher flat speeds, on the other hand, helped to enhance fiber alignment, which increased the evenness and strength of the carded sliver and yarn. Additionally, it was discovered that the ideal blend of licker-in and flat rates varied based on the fiber type and processing circumstances. When being carded, various fibers displayed distinctive behaviors that necessitated adjusting the operating settings in order to provide the necessary quality results. The study also determined the crucial speed ratios between the licker-in and flat speeds that reduced fiber breakage and increased the caliber of the finished goods. The results of this study offer useful information for textile producers and process engineers to improve the quality of carded sliver and yarn while maximizing the performance of carding machines. Operators may choose machine settings and parameter adjustments wisely by knowing the impacts of licker-in and flat speeds, which will increase textile industry efficiency, productivity, and product quality.
文摘Spinning has a significant influence on all textile processes. Combinations of all the capital equipment display the process’ critical condition. By transforming unprocessed fibers into carded sliver and yarn, the carding machine serves a critical role in the textile industry. The carding machine’s licker-in and flat speeds are crucial operational factors that have a big influence on the finished goods’ quality. The purpose of this study is to examine the link between licker-in and flat speeds and how they affect the yarn and carded sliver quality. A thorough experimental examination on a carding machine was carried out to accomplish this. The carded sliver and yarn produced after experimenting with different licker-in and flat speed combinations were assessed for important quality factors including evenness, strength, and flaws. To account for changes in material qualities and machine settings, the study also took into consideration the impact of various fiber kinds and processing circumstances. The findings of the investigation showed a direct relationship between the quality of the carded sliver and yarn and the licker-in and flat speeds. Within a limited range, greater licker-in speeds were shown to increase carding efficiency and decrease fiber tangling. On the other hand, extremely high speeds led to more fiber breakage and neps. Higher flat speeds, on the other hand, helped to enhance fiber alignment, which increased the evenness and strength of the carded sliver and yarn. Additionally, it was discovered that the ideal blend of licker-in and flat rates varied based on the fiber type and processing circumstances. When being carded, various fibers displayed distinctive behaviors that necessitated adjusting the operating settings in order to provide the necessary quality results. The study also determined the crucial speed ratios between the licker-in and flat speeds that reduced fiber breakage and increased the caliber of the finished goods. The results of this study offer useful information for textile producers and process engineers to improve the quality of carded sliver and yarn while maximizing the performance of carding machines. Operators may choose machine settings and parameter adjustments wisely by knowing the impacts of licker-in and flat speeds, which will increase textile industry efficiency, productivity, and product quality.
基金This work was financially supported by the National Natural Science Foundation of China(Nos.20204007,50390090,20490220,10590355)the Doctoral Foundation of National Education Committee of China(No.20030248008)the 863 Project of China(No.2002AA336120).
文摘Finite element method is used to simulate the high-speed melt spinning process, based on the equation system proposed by Doufas et al. Calculation predicts a neck-like deformation, as well as the related profiles of velocity, diameter, temperature, chain orientation, and crystallinity in the fiber spinning process. Considering combined effects on the process such as flow-induced crystallization, viscoelasticity, filament cooling, air drag, inertia, surface tension and gravity, the simulated material flow behaviors are consistent with those observed for semi-crystalline polymers under various spinning conditions, The structure change of polymer coils in the necking region described by the evolution of conformation tensor is also investigated. Based on the relaxation mechanism of macromolecules in flow field different types of morphology change of polymer chains before and in the neck are proposed, giving a complete prospect of structure evolution and crystallization of semi-crystalline polymer in the high speed fiber spinning process.
基金supported by the Zhejiang Provincial Natural Science Foundation,China(No.LZ17E050001)the National Natural Science Foundation of China(No.51975301 and No.52075359)。
文摘Uncontrolled residual stresses have significant effects on the service time and defects of the spun parts.Nowadays,X-Ray Diffraction(XRD)method has been widely used in the residual stress measurement of industry products with different forming processes.The calculated residual stress is usually obtained from the data fitting slope of strain and angle with Ordinary Least Squares(OLS)method.But this fitting method is not always suitable for the big fluctuant data.In this paper,the Weighted Least Square(WLS)method is used for the data fitting and compared with the OLS method.The nickel-based superalloy GH3030 and iron-based superalloy GH1140 are applied in the multi-pass cold spinning experiments.The residual stress distributions of normal,potential crack and wrinkle workpieces are discussed with the grain structure.The results show that WLS method has better goodness of fit compared with OLS method.The residual stress distributions have special relationship with potential crack,wrinkle workpiece and grain structure.
文摘Competings or frustrated interactions are common for condensed matter systems. In consideration of the effect of dipole–dipole interaction, the static properties of square lattice spin systems are investigated using the Wang–Landau algorithm. The dynamic hysteresis is also simulated using the Monte Carlo(MC) method. The step-like magnetization under a DC magnetic field and two distinct peaks in hysteresis dispersion under an AC magnetic field are observed. Then, the formation of the properties of the frustrated dipolar array are discussed.
基金Item Sponsored by National Natural Science Foundation of China(50871076)
文摘The effects of spinning deformation and subsequent heat treatments on the mechanical properties and microstructure of 18Ni Co-free Maraging steel (T250) tube were evaluated comparatively with the perform. An obvious radial shrinkage is detected in spun tubes after heat treatment and the magnitude of the shrinkage induced by solution treatment is almost the same as that by aging. Plastic deformation during spinning elongated the grains severely in the direction of metal flow. The solution treatment resulted in a drastically refined grain and recrystallised microstructure, removing the effect of plastic deformation, relieving the tangential residual stress and strain and improving hardness. Subsequent aging obtained a tempered microstructure, enhancing hardness values strikingly for precipitation strengthening. XRD (X-ray diffraction) analysis indicated that the reversed austenite formed in a plate-like along the grain boundaries and the volume fraction of austenite in spun tube was more than double that in the preform. These results imply that the residual stress and stain induced by spinning process and reversed austenite forming during aging might have the similar contribution to the radical shrinkage.
基金financially supported by the National Basic Research Program of China(973 Program,Key Project:2014CB643604)the National Natural Science Foundation of China(No.51373164)
文摘A series of polyamic acid copolymers(co-PAAs) containing phosphorous groups in the side chains were synthesized from [2,5-bis(4-aminophenoxy) phenyl] diphenylphosphine oxide(DATPPO) and 4,4′-oxydianiline(ODA) with 3,3′,4,4′-biphenyltetracarboxylic dianhydride(s-BPDA) through the polycondensation in N,N′-dimethyacetamide(DMAc). The co-PAA solutions were spun into fibers by a dry-jet wet spinning process followed by thermal imidization to obtain co-polyimide(co-PI) fibers. FTIR spectra and elemental analysis confirmed the chemical structure of PI fibers. SEM results indicated that the resulting PI fibers had a smooth and dense surface, a uniform and circle-shape diameter. The thermogravimetric measurements showed that with the increase of DATPPO content, the resulting PI fibers possessed high decomposition temperature and residual char yield, indicating that the PI fibers had good thermal stability. The corresponding limiting oxygen index(LOI) values from the experiment results showed that the co-PI fibers possessed good flame-retardant property. Furthermore, the mechanical properties of the co-PI fibers were investigated systematically. When the DATPPO content increased, the tensile strength and initial modulus of the co-PI fibers decreased. However, the mechanical properties were improved by increasing the draw ratio of the fibers. When the draw ratio was up to 2.5, the tensile strength and initial modulus of the co-PI fibers reached up to 0.64 and 10.02 GPa, respectively. The WAXD results showed that the order degree of amorphous matter increased with increased stretching. In addition, the SAXS results displayed that valuably drawing the fibers could eliminate the voids inside and lead to better mechanical property. WAXD revealed that the orientation of the amorphous polymer influenced the mechanical properties of the fibers.