C13H17N3O,Mr=231.30,monoclinic,P21/,a=7.094(5).b =32.14(l),c=5.894(4)A,β=112.84(4)°,Z=4,Dx=l.24 gcm-3,V=1238(l) A 3,λ(MoKα)=0.71069 A,μ=0.76 cm-1.F(000)=496,T=293K,R=0.060,Rω=0.062 for 1205 reflections(I】3...C13H17N3O,Mr=231.30,monoclinic,P21/,a=7.094(5).b =32.14(l),c=5.894(4)A,β=112.84(4)°,Z=4,Dx=l.24 gcm-3,V=1238(l) A 3,λ(MoKα)=0.71069 A,μ=0.76 cm-1.F(000)=496,T=293K,R=0.060,Rω=0.062 for 1205 reflections(I】3σ(I)).The cyclohexane ring shows a slightly distorted chair conformation.The NHCONH2 group has a conformation with the C=O bond trans to the N-N bond.The molecules in the crystal are linked together by the O…H-N hydrogen bonding.forming an infinite ribbon.展开更多
文摘C13H17N3O,Mr=231.30,monoclinic,P21/,a=7.094(5).b =32.14(l),c=5.894(4)A,β=112.84(4)°,Z=4,Dx=l.24 gcm-3,V=1238(l) A 3,λ(MoKα)=0.71069 A,μ=0.76 cm-1.F(000)=496,T=293K,R=0.060,Rω=0.062 for 1205 reflections(I】3σ(I)).The cyclohexane ring shows a slightly distorted chair conformation.The NHCONH2 group has a conformation with the C=O bond trans to the N-N bond.The molecules in the crystal are linked together by the O…H-N hydrogen bonding.forming an infinite ribbon.
