The nose temperature for σ-phase precipitation in super-duplex stainless steel (SDSS) UNS S32750 was evaluated by hardness method.Color-optical microscopy,scanning electron microscopy,energy spectrum analysis,impac...The nose temperature for σ-phase precipitation in super-duplex stainless steel (SDSS) UNS S32750 was evaluated by hardness method.Color-optical microscopy,scanning electron microscopy,energy spectrum analysis,impact and corrosion testing were carried out to investigate characteristics of microstructure and properties of the SDSS aged at the nose temperature.The experimental results indicate that the nose temperature of precipitation is 920℃ and aging at this temperature tiny σ phases can precipitate at phase interfaces or ferrite grain boundaries within 2min.Prolonging aging duration the amount ofσ-phase increases and a dual structure with σ and γ is obtained when aging for 120min.The precipitation ofσ-phase leads to severe deterioration in impact toughness (longitudinal/transverse direction) and corrosion resistance of SDSS.展开更多
采用Gleeble 3800热力模拟机对超级双相不锈钢SAF2507焊接热影响区组织进行模拟,研究了不同热输入条件下焊接热影响区显微组织和合金元素含量的变化,通过电化学循环伏安法评价了该组织的耐蚀性。研究结果表明,热输入由0.807 k J/mm增加...采用Gleeble 3800热力模拟机对超级双相不锈钢SAF2507焊接热影响区组织进行模拟,研究了不同热输入条件下焊接热影响区显微组织和合金元素含量的变化,通过电化学循环伏安法评价了该组织的耐蚀性。研究结果表明,热输入由0.807 k J/mm增加至2.552 k J/mm时,模拟热影响区上奥氏体以晶内奥氏体、晶界奥氏体和魏氏奥氏体3种形貌析出,含量由40%增加到52%。各个热输入时奥氏体的PRE值均大于铁素体的PRE值,因此奥氏体含量的增加使热影响区组织的点蚀电位从1030 m V提高至1082 m V。但是继续增加热输入至2.965 k J/mm时,在两相交界处观察到有粒状的χ相析出。虽然该组织上奥氏体含量仍有增加,但是χ相的析出却导致组织的点蚀电位降至1065 m V。展开更多
基金Founded by the Special Project of Shaanxi Education Department(07JK309)Xi'an University of Architecture and Technology (JC0714)
文摘The nose temperature for σ-phase precipitation in super-duplex stainless steel (SDSS) UNS S32750 was evaluated by hardness method.Color-optical microscopy,scanning electron microscopy,energy spectrum analysis,impact and corrosion testing were carried out to investigate characteristics of microstructure and properties of the SDSS aged at the nose temperature.The experimental results indicate that the nose temperature of precipitation is 920℃ and aging at this temperature tiny σ phases can precipitate at phase interfaces or ferrite grain boundaries within 2min.Prolonging aging duration the amount ofσ-phase increases and a dual structure with σ and γ is obtained when aging for 120min.The precipitation ofσ-phase leads to severe deterioration in impact toughness (longitudinal/transverse direction) and corrosion resistance of SDSS.
文摘采用Gleeble 3800热力模拟机对超级双相不锈钢SAF2507焊接热影响区组织进行模拟,研究了不同热输入条件下焊接热影响区显微组织和合金元素含量的变化,通过电化学循环伏安法评价了该组织的耐蚀性。研究结果表明,热输入由0.807 k J/mm增加至2.552 k J/mm时,模拟热影响区上奥氏体以晶内奥氏体、晶界奥氏体和魏氏奥氏体3种形貌析出,含量由40%增加到52%。各个热输入时奥氏体的PRE值均大于铁素体的PRE值,因此奥氏体含量的增加使热影响区组织的点蚀电位从1030 m V提高至1082 m V。但是继续增加热输入至2.965 k J/mm时,在两相交界处观察到有粒状的χ相析出。虽然该组织上奥氏体含量仍有增加,但是χ相的析出却导致组织的点蚀电位降至1065 m V。