The effects of low frequency electromagnetic field on the macro-physical fields in the semi-continuous casting process of aluminum alloys and the microstructure and crack in the billets were studied and analyzed by th...The effects of low frequency electromagnetic field on the macro-physical fields in the semi-continuous casting process of aluminum alloys and the microstructure and crack in the billets were studied and analyzed by the numerical and experimental methods.Comparison of the results for the macro-physical fields in the low frequency electromagnetic casting(LFEC) process with the conventional DC casting process indicates the following characters due to the application of electromagnetic field:an entirely changed direction and remarkably increased velocity of melt flow;a uniform distribution and a decreased gradient of temperature;elevated isothermal lines;a reduced sump depth;decreased stress and plastic deformation.Further,the microstructure of the billets is refined remarkably and the crack in the billets is eliminated in LFEC process because of modification of the macro-physical fields induced by the application of low frequency electromagnetic field.展开更多
[Objective] This study was conducted to construct a super-high yield population of Japnica rice in cold regions of North China and to explore its characteristics. [Method] The super rice variety Longjing 21 was select...[Objective] This study was conducted to construct a super-high yield population of Japnica rice in cold regions of North China and to explore its characteristics. [Method] The super rice variety Longjing 21 was selected as the experimental material. Different row spacing(two levels), plant spacing(three levels) and seedling number per hill(three levels) were designed in field trials. Then, the growth stages,dry matter accumulation, leaf area, yield and yield components of these different treatments were measured. [Result] Rice yield had significantly negative correlation with plant spacing and row spacing, but no significant correlation with seedling number per hill. Rice yield was mainly affected by plant spacing, and less affected by seedling number per hill. The best recommended specifications for plant spacing of super rice variety Longjing 21 were 24 cm for row spacing, 12 cm for plant spacing and five seedlings per hill, and the expected yield was 10 473.0 kg/hm^2.The increased number of total spikelets(4.5×108hm2or more) in populations was the major reason for high yield. Super-high yield populations had fewer tillers at the early growth stage and achieved the expected number of productive tillers at critical leaf-age(June 25), and tiller number peaked at jointing stage(July 6) and was about 1.2 times of the expected number. The percentage of productive tillers in total tillers of super-high yield population was more than 85% at heading stage. At middle growth stage(from jointing to heading stage), the dry matter accumulation, leaf area index(LAI) at heading stage, effective leaf area, spikelet number of population,spikelet number per leaf area unit(cm2), and culm-sheath weight per stem of super-high yield population were significantly higher than those of other populations.At late growth stage(from heading to maturity stage), the leaf area decreasing rate of super-high yield population was significantly smaller than that of other populations. At late growth stage(from heading to maturity stage), the leaf area decreasing rate, crop growth rate, net assimilation rate, biomass accumulation, number of filled grains per leaf area unit(cm^2) and grain weight per leaf area unit(cm^2) of high-yield population were significantly higher than those of other populations. Output and translocation of dry matter(weight per stem and sheath and total filling rate at maturity) from heading to milky stage of super-high yield population were significantly higher than those of other populations. [Conclusion] The characteristics of superhigh yield rice in cold region of North China are enriching the amount of actual filling of sink through improving photosynthetic efficiency from heading to maturity stage on the basis of enough panicle numbers.展开更多
With better understanding of the quality and physico-mechanical properties of rocks of dam foundation,and the physico-mechanical properties and structure design of arch dam in association with the foundation excavatio...With better understanding of the quality and physico-mechanical properties of rocks of dam foundation,and the physico-mechanical properties and structure design of arch dam in association with the foundation excavation of Xiluodu arch dam,the excavation optimization design was proposed for the foundation surface on the basis of feasibility study.Common analysis and numerical analysis results demonstrated the feasibility of using the weakly weathered rocks III1and III2as the foundation surface of super-high arch dam.In view of changes in the geological conditions at the dam foundation along the riverbed direction,the design of extending foundation surface excavation area and using consolidating grouting and optimizing structure of dam bottom was introduced,allowing for harmonization of the arch dam and foundation.Three-dimensional(3D)geomechanics model test and fi nite element analysis results indicated that the dam body and foundation have good overload stability and high bearing capacity.The monitoring data showed that the behaviors of dam and foundation correspond with the designed patterns in the construction period and the initial operation period.展开更多
Super-high collapse resistant casings were developed by using Ti, Nb and V microalloyed CrMo steel and cross rolling techniques. A transmission electron microscope(TEM) and X-ray diffractometer were used to observe ...Super-high collapse resistant casings were developed by using Ti, Nb and V microalloyed CrMo steel and cross rolling techniques. A transmission electron microscope(TEM) and X-ray diffractometer were used to observe the characteristics of the microstructure. It was found that the ( 111 ) texture and the nano-scale precipitates distribute in a way that is beneficial to the collapse resistance, and the collapse strength of the prepared casing had a measurement, which was approximately 60% higher than the API standard value. A design concept to attain super-high collapse resistance is proposed based on the texture design and microstructure control.展开更多
In order to understand the stress corrosion behavior of super-high strength aluminum alloys by spray forming, different aluminum alloys by different heat treatment was made. The results showed that the alloy with peak...In order to understand the stress corrosion behavior of super-high strength aluminum alloys by spray forming, different aluminum alloys by different heat treatment was made. The results showed that the alloy with peak aging has the most sensitive stress corrosion cracking, the crack can even be seen using eyes;the alloys with two step aging were better than one step aging alloys, the alloys has not been found stress corrosion cracking.展开更多
Super-high pressure(SHP)technique plays an increasing role in the fields of materials science and engineering.Herein,the Mg_(97)Zn_(1)Y_(2) alloy was heat-treated under SHP(6 GPa)by cubic-anvil large-volume press with...Super-high pressure(SHP)technique plays an increasing role in the fields of materials science and engineering.Herein,the Mg_(97)Zn_(1)Y_(2) alloy was heat-treated under SHP(6 GPa)by cubic-anvil large-volume press with six rams for 2 h in the temperature range of 500–1200℃.The microstructure and mechanical properties were investigated.The results indicated that the as-cast sample consists of α-Mg equiaxed dendrites and continuous lamellar long period stacking ordered(LPSO)phase in grain boundaries.After the SHP treatment,the LPSO phase is gradually replaced by eutectic phase(Mg,Zn)_(3)Y with increasing temperature.The microhardness and strength of sample prepared at 1100℃ under SHP treatment are significantly improved compared with the as-cast one at room temperature.The improved mechanical behaviors are mainly attributed to LPSO phase kink-banding strengthening at low temperature and the precipitation strengthening of a large amount of fine(Mg,Zn)_(3)Y particles at high temperature after SHP treatment.It reveals the SHP is an effective approach to prepare high performance Mg alloys.展开更多
To deal with the problem that the initial velocity of the bullet is difficult to increase,the research on the super-high initial velocity propulsion in the barrel weapon with an adaptive pressure-maintaining chamber a...To deal with the problem that the initial velocity of the bullet is difficult to increase,the research on the super-high initial velocity propulsion in the barrel weapon with an adaptive pressure-maintaining chamber are conducted.Considering the law of gun-powder burning and the flow characteristics of gun-powder gas in multi-chamber,the scheme of super-high initial velocity propulsion with an adaptive pressure-maintaining chamber is designed,the ballistic model of the barrel weapon with super-high velocity bullet propulsion is established.The research results show that the technical scheme can greatly increase the initial velocity of the bullet with the peak pressure keeping nearly the same as the tradition barrel weapon.The research results can provide a theoretical foundation to significantly increase the initial velocity in barrel weapons using solid propellants,and have an important reference value to comprehensively increase the power of the barrel weapons.展开更多
Horizontal segregation has been a constraint to the development and application of super-high bed sintering.To eliminate the horizontal segregation of super-high bed sintering,several typical sintering machines were s...Horizontal segregation has been a constraint to the development and application of super-high bed sintering.To eliminate the horizontal segregation of super-high bed sintering,several typical sintering machines were sampled and analyzed,and theoretical calculation was made to compare the bed depth and their differences in different areas within the mixture bin.Then,solutions were proposed and applied to a 265 m^(2) sintering machine.The results showed that the horizontal seg-regation of the 265 m^(2) sintering machine was dominated by particles larger than 8 mm with horizontal segregation degree of 0.48,while 360 and 550 m^(2) sintering machines were affected by 5-8 mm and 1-3 mm particles with horizontal segregation degree of 0.27 and 0.31,respectively.Causes analysis indicated the different segregation distribution results from the matching of the bed depth of each area within the mixture bin.Finally,the horizontal segregation degree not larger than 0.06 was achieved by optimizing the time parameters and the division of three zones on the 265 m^(2) sintering machine.展开更多
Super-high bed sintering process is an important development direction of iron ore sintering for its lower emission and higher yield.However,there is a lack of deep understanding of the uneven quality of super-high be...Super-high bed sintering process is an important development direction of iron ore sintering for its lower emission and higher yield.However,there is a lack of deep understanding of the uneven quality of super-high bed sintering products,and the deterioration of reduction disintegration performance,the thickening of hearth layer and the reduction in energy-saving effect are perplexing enterprises and researchers.To ascertain the problems of super-high bed sintering,ten sintering machines with the areas of 265,280,360,550 and 660 m^(2)and bed depth above 900 mm were sampled and analyzed.The results showed that problems were mainly shown in the unevenness of chemical composition,macrostructure,mechanical strength and metallurgical performance.The chemical composition exhibits severe segregation in both horizontal and vertical directions,with basicity segregation reaching as high as 0.81.The uneven macrostructure of sinter is reflected in a 10%difference in porosity and mechanical strength increase in 16%–19%along the vertical direction.The reducibility and reduction disintegration performance gradually deteriorate along the bed depth,with a difference of 10.5%in reducibility and 7.3%in RDI−0.5 mm(reduction disintegration index of sinter with size smaller than 0.5 mm).展开更多
The inhomogeneous sinter properties in super-high bed sintering have been reported in our previous research.To inves-tigate the reasons for the inhomogeneous phenomena,detailed sampling and analysis of mixed material ...The inhomogeneous sinter properties in super-high bed sintering have been reported in our previous research.To inves-tigate the reasons for the inhomogeneous phenomena,detailed sampling and analysis of mixed material bed and sintered bed in super-high bed sintering plant were executed.The results indicated that the higher porosity and thinner dendrite of silico-ferrite of calcium and aluminum in the upper layer as well as dense structure and higher secondary hematite content in the lower layer led to the heterogeneities of mechanical strength and reduction properties exceeding 20%and 10%,respectively.From the bed top downward,the basicity of mixed material decreased from 2.13 to 1.68 because the average particle size increased from 2.65 to 4.56 mm.Fluxes and fuels gathered in finer particles(-3 mm)of mixed material,and the-3 mm particles of mixed material generated more liquid phase than+3 mm ones.The heat input of super-high sintering bed was inhomogeneous due to the heat accumulation effect and unreasonable fuel distribution.The inhomo-geneous sintering heat condition in sintering bed resulted in the different quantities and properties of liquid phase.The inhomogeneous quantities and properties of liquid phase that were influenced by inhomogeneous distribution of chemical composition,particle size,and heat input led to inhomogeneous mineralizing results.Homogeneous mineralizing condition is the key for homogeneous super-high bed sintering.展开更多
Based on break characteristics of roofs in fully mechanized top-coal mining of thick shallow coal seams, a fracture mechanics model was built, and the criterion of crack propagation in the main roof was derived using ...Based on break characteristics of roofs in fully mechanized top-coal mining of thick shallow coal seams, a fracture mechanics model was built, and the criterion of crack propagation in the main roof was derived using the fracture mechanics theory. The relationships between the fracture length of the roof and the working resistance of the supports were discovered, and the correlations between the load on the overlying strata and the ratio of the crack's length to the thickness of the roof were obtained. Using a working face of Jindi Coal Mine, Xing county Shanxi province as an example, the relationships between the fracture length of the roof and the working resistance of the supports were analysed in detail. The results give a design basis in hydraulic top coal caving supports, which could provide useful references in the practical application. On-site experiment proves that the periodic weighting step interval of the caving face is 15–16 m, which is basically consistent with the theoretical analysis results, and indicates that the mechanized caving hydraulic support is capable of meeting the support requirements in the mining of a super-thick but shallowly buried coal seam.展开更多
High-efficiency abrasive process with CBN grinding wheel is one of the important techniques of advanced manufacture. Combined with raw and finishing machining, it can attain high material removal rate like turning, mi...High-efficiency abrasive process with CBN grinding wheel is one of the important techniques of advanced manufacture. Combined with raw and finishing machining, it can attain high material removal rate like turning, milling and planning. The difficult-to-grinding materials can also be ground by means of this method with high performance. In the present paper, development status and latest progresses on high-efficiency abrasive machining technologies with CBN grinding wheel relate to high speed and super-high speed grinding, quick point-grinding, high efficiency deep-cut grinding, creep feed deep grinding, heavy-duty snagging and abrasive belt grinding were summarized. The efficiency and parameters range of these abrasive machining processes were compared. The key technologies of high efficiency abrasive machining, including grinding wheel, spindle and bearing, grinder, coolant supplying, installation and orientation of wheel and workpiece and safety defended, as well as intelligent monitor and NC grinding were investigated. It is concluded that high efficiency abrasive machining is a promising technology in the future.展开更多
Based on the space spherical symmetry of 3-dimensional and the translational symmetry of time and the uncertainty principle, a 4-dimensional space-time cylinder model of quarks and leptons is established. With this mo...Based on the space spherical symmetry of 3-dimensional and the translational symmetry of time and the uncertainty principle, a 4-dimensional space-time cylinder model of quarks and leptons is established. With this model, equations of the special relativity can be extended more perfectly, thereby achieving a unity of the special relativity and quantum mechanics in deeper level. New equations can not only interpret issues explained by old equations but also solve several important pending problems. For example, a formula to strictly calculate the coefficient ξ of Lorentz invariance violation (LIV) is derived, to above 4 × 1019 eV UHECR protons the calculated |ξ| -30, although there is the LIV effect it is too weak to change the GZK cutoff, which is consistent with observations of HiRes and Auger;Also, a relation formula between the Hubble constant and several basic constants is derived, thus theoretically calculated H0 = 70.937 km·s-1·Mpc-1, which is well consistent with the final observation result of HST Key Project. In addition, an unusual effect predicted by new equations can be experimentally tested in the electron storage ring;a preliminary experiment result has hinted its signs of existence.展开更多
The microstructure of Mg-8Zn-1Y alloy solidified under super-high pressure was analyzed through X-ray diffraction(XRD), scanning electron microscopy(SEM) and energy dispersive spectroscopy(EDS). And, compression...The microstructure of Mg-8Zn-1Y alloy solidified under super-high pressure was analyzed through X-ray diffraction(XRD), scanning electron microscopy(SEM) and energy dispersive spectroscopy(EDS). And, compression deformation behavior at room-temperature was studied. The results showed that the microstructure of Mg-8Zn-1Y alloy solidified under ambient pressure and super-high pressure was both mainly composed of ■-Mg and quasicrystal I-Mg3Zn6 Y. Solidification under super-high pressure contributed to refining solidified microstructure and changing morphology of the intergranular second phase. The morphology of intergranular second phase(quasicrystal I-Mg3Zn6Y) was transformed from continuous network(ambient pressure) to long island(high pressure) and finally to granular(super-high pressure) with the increase in pressure. The compressive strength, yield strength and rupture strain of the samples solidified under ambient pressure were significantly improved from 262.6 MPa, 244.4 MPa and 13.3% to 437.3 MPa, 368.9 MPa and 24.7% under the pressure of 6 GPa, respectively. Under ambient pressure, cleavage plane on compressive fracture was large and smooth. When it was solidified under the pressure ranging from 4 to 6 GPa, cleavage plane on compressive fracture was small and coarse. In addition, dimple, tear ridge and lobate patterns existed.展开更多
The Laguerre-Gaussian(LG)mode beam has very important applications in many research fields.Here,the Theon sieve is first introduced into the laser resonator to generate petal-like laser beams by coherently superimposi...The Laguerre-Gaussian(LG)mode beam has very important applications in many research fields.Here,the Theon sieve is first introduced into the laser resonator to generate petal-like laser beams by coherently superimposing two high-order LG modes.The effectiveness was verified by GLAD software.The petal-like laser beam is derived from the light field redistribution and coherent superposition caused by the diffraction effect of the Theon sieve.The relationship between the order of the petal-like laser and the cavity structures has also been investigated in detail.Light field operation in the laser cavity greatly simplifies the optical structure and is more beneficial to optical diagnostics and imaging.展开更多
CO2-shielded welding experiments of newly developed, 780 MPa super-high strength heavy-duty truck crossbeam steel were conducted, and the microstructure, microhardness, mechanical properties, and impact tough- hess of...CO2-shielded welding experiments of newly developed, 780 MPa super-high strength heavy-duty truck crossbeam steel were conducted, and the microstructure, microhardness, mechanical properties, and impact tough- hess of the welded joint were studied. The evolution of the microstructure of the welded joint occurred as follows.. welding seam (acicular ferrite+proeutectoid ferrite)→fusion zone (granular bainite-long strip M/A island)→coarse grain zone (granular bainite-long strip or short bar M/A island)→fine grain zone (ferrite+ pearlite+ blocky M/A is- land)→mixed grained zone (ferrite+granular bainite+blocky M/A island)→base metal (proeutectoid ferrite+gran- ular bainite-hlocky or granular M/A island). Increasing the density of the grain boundaries can effectively improve the impact toughness, and the blocky M/A island hindered crack propagation more effectively than the long strip M/A island. The new hot-rolled 780 MPa super-high strength steel had excellent weldability. The welding technology was applied under the following conditions: welding voltage was 20 to 21 V, welding current was 200 to 210 A, and the gas flow rate was 25 L/rain.展开更多
An aqueous nanosuspension of agrochemicals unlike pharmaceutics has to achieve massive production in an effective way,capable to ensure sufficient profits in commercialization.This work implements the flash nanoprecip...An aqueous nanosuspension of agrochemicals unlike pharmaceutics has to achieve massive production in an effective way,capable to ensure sufficient profits in commercialization.This work implements the flash nanoprecipitation(FNP)technique to effectively generate agrochemical nanosuspension,anticipatedly overcoming such an obstacle.Azoxystrobin,a broad spectrum fungicide,in either acetone or ethanol is used herein as a mode agrochemical.To ensure a green and practical utilization,three kinds of commercially available and eco-friendly surfactants,i.e.,poly(ethylene glycol)-block-poly(lactic-co-glycolic acid)(PEG-b-PLGA),Tween 80 and alkyl polyglucosides(APGs),are employed for stabilizing the nanoparticles.The results show that the polymeric stabilizer,PEG-b-PLGA,has the best stabilization efficiency,and can maintain the particles below 100 nm for at least three weeks.The azoxystrobin load of the nanoparticles reaches as high as 77 wt.%,beneficial to enhancing the biological potency.Moreover,the FNP brings the particles a much smaller size,narrower size distribution,better size stability,and higher biological efficacy than the ones made via a traditional method of the drop and stir(DS).The nanosuspensions present superior fungicidal performances over a prevailing counterpart from Syngenta.This study proves an enhanced biological potency and reduced dosage of agrochemical nanosuspension made via the FNP,indicating a remarkable advantage of the FNP over the conventional preparation.The integration of a super-high load,eco-friendly excipients,intensified preparation process,enhanced potency,and reduced dosage creates a promising pathway to generate a green aqueous nanosuspension of agrochemicals.展开更多
With the support by the National Natural Science Foundation of China,the research team led by Prof.Fang QianRong(方千荣)at the State Key Laboratory of Inorganic Synthesis and Preparative Chemistry,Jilin University,dev...With the support by the National Natural Science Foundation of China,the research team led by Prof.Fang QianRong(方千荣)at the State Key Laboratory of Inorganic Synthesis and Preparative Chemistry,Jilin University,developed a crystalline porous material(CPM)with super-high chemical stability,which was published in Nat Chem(2019,11,doi:10.1038/s41557-019-0238-5).展开更多
We demonstrate a new and simple method for pre-treating the carbon material and iron precursor to prepare oxygen reduction reaction(ORR) catalysts, which can produce super-high performance and stability in alkaline so...We demonstrate a new and simple method for pre-treating the carbon material and iron precursor to prepare oxygen reduction reaction(ORR) catalysts, which can produce super-high performance and stability in alkaline solution, with high performance in acid solution. This strategy using cheap materials is simply controllable. Moreover, it has achieved smaller uniform nanoparticles to exhibit high stability, and the synergetic effect of Fe and N offered much higher performance in ORR than commercial Pt/C, with high maximum power density in alkaline and acid fuel cell test. So it can make this kind of catalysts be the most promising alternatives of Pt-based catalysts with best performance/price.展开更多
基金Project(2005CB623707)supported by National Basic Research Project of China
文摘The effects of low frequency electromagnetic field on the macro-physical fields in the semi-continuous casting process of aluminum alloys and the microstructure and crack in the billets were studied and analyzed by the numerical and experimental methods.Comparison of the results for the macro-physical fields in the low frequency electromagnetic casting(LFEC) process with the conventional DC casting process indicates the following characters due to the application of electromagnetic field:an entirely changed direction and remarkably increased velocity of melt flow;a uniform distribution and a decreased gradient of temperature;elevated isothermal lines;a reduced sump depth;decreased stress and plastic deformation.Further,the microstructure of the billets is refined remarkably and the crack in the billets is eliminated in LFEC process because of modification of the macro-physical fields induced by the application of low frequency electromagnetic field.
基金Supported by National Key Technology Research and Development Program of China(2011BAD16B11-02YJ01,2012BAD04B01-02)Key Science and Technology Program of Heilongjiang Province+2 种基金China(GA13B101)Heilongjiang Postdoctoral Sustentation Fund(LBH-Z10038)the Funds of Heilongjiang Academy of Agricultural Sciences for Distinguished Young Scholars(2014)~~
文摘[Objective] This study was conducted to construct a super-high yield population of Japnica rice in cold regions of North China and to explore its characteristics. [Method] The super rice variety Longjing 21 was selected as the experimental material. Different row spacing(two levels), plant spacing(three levels) and seedling number per hill(three levels) were designed in field trials. Then, the growth stages,dry matter accumulation, leaf area, yield and yield components of these different treatments were measured. [Result] Rice yield had significantly negative correlation with plant spacing and row spacing, but no significant correlation with seedling number per hill. Rice yield was mainly affected by plant spacing, and less affected by seedling number per hill. The best recommended specifications for plant spacing of super rice variety Longjing 21 were 24 cm for row spacing, 12 cm for plant spacing and five seedlings per hill, and the expected yield was 10 473.0 kg/hm^2.The increased number of total spikelets(4.5×108hm2or more) in populations was the major reason for high yield. Super-high yield populations had fewer tillers at the early growth stage and achieved the expected number of productive tillers at critical leaf-age(June 25), and tiller number peaked at jointing stage(July 6) and was about 1.2 times of the expected number. The percentage of productive tillers in total tillers of super-high yield population was more than 85% at heading stage. At middle growth stage(from jointing to heading stage), the dry matter accumulation, leaf area index(LAI) at heading stage, effective leaf area, spikelet number of population,spikelet number per leaf area unit(cm2), and culm-sheath weight per stem of super-high yield population were significantly higher than those of other populations.At late growth stage(from heading to maturity stage), the leaf area decreasing rate of super-high yield population was significantly smaller than that of other populations. At late growth stage(from heading to maturity stage), the leaf area decreasing rate, crop growth rate, net assimilation rate, biomass accumulation, number of filled grains per leaf area unit(cm^2) and grain weight per leaf area unit(cm^2) of high-yield population were significantly higher than those of other populations. Output and translocation of dry matter(weight per stem and sheath and total filling rate at maturity) from heading to milky stage of super-high yield population were significantly higher than those of other populations. [Conclusion] The characteristics of superhigh yield rice in cold region of North China are enriching the amount of actual filling of sink through improving photosynthetic efficiency from heading to maturity stage on the basis of enough panicle numbers.
文摘With better understanding of the quality and physico-mechanical properties of rocks of dam foundation,and the physico-mechanical properties and structure design of arch dam in association with the foundation excavation of Xiluodu arch dam,the excavation optimization design was proposed for the foundation surface on the basis of feasibility study.Common analysis and numerical analysis results demonstrated the feasibility of using the weakly weathered rocks III1and III2as the foundation surface of super-high arch dam.In view of changes in the geological conditions at the dam foundation along the riverbed direction,the design of extending foundation surface excavation area and using consolidating grouting and optimizing structure of dam bottom was introduced,allowing for harmonization of the arch dam and foundation.Three-dimensional(3D)geomechanics model test and fi nite element analysis results indicated that the dam body and foundation have good overload stability and high bearing capacity.The monitoring data showed that the behaviors of dam and foundation correspond with the designed patterns in the construction period and the initial operation period.
文摘Super-high collapse resistant casings were developed by using Ti, Nb and V microalloyed CrMo steel and cross rolling techniques. A transmission electron microscope(TEM) and X-ray diffractometer were used to observe the characteristics of the microstructure. It was found that the ( 111 ) texture and the nano-scale precipitates distribute in a way that is beneficial to the collapse resistance, and the collapse strength of the prepared casing had a measurement, which was approximately 60% higher than the API standard value. A design concept to attain super-high collapse resistance is proposed based on the texture design and microstructure control.
文摘In order to understand the stress corrosion behavior of super-high strength aluminum alloys by spray forming, different aluminum alloys by different heat treatment was made. The results showed that the alloy with peak aging has the most sensitive stress corrosion cracking, the crack can even be seen using eyes;the alloys with two step aging were better than one step aging alloys, the alloys has not been found stress corrosion cracking.
基金NSFC(51101142 and 50821001)New Century Excellent Talents in University of Ministry of Education of China(NCET-12-0690)+1 种基金Hebei province scientific program(13961002D and Y2012019)Hebei Province Technology Foundation for Selected Overseas Chinese and Outstanding Young Scholar.
文摘Super-high pressure(SHP)technique plays an increasing role in the fields of materials science and engineering.Herein,the Mg_(97)Zn_(1)Y_(2) alloy was heat-treated under SHP(6 GPa)by cubic-anvil large-volume press with six rams for 2 h in the temperature range of 500–1200℃.The microstructure and mechanical properties were investigated.The results indicated that the as-cast sample consists of α-Mg equiaxed dendrites and continuous lamellar long period stacking ordered(LPSO)phase in grain boundaries.After the SHP treatment,the LPSO phase is gradually replaced by eutectic phase(Mg,Zn)_(3)Y with increasing temperature.The microhardness and strength of sample prepared at 1100℃ under SHP treatment are significantly improved compared with the as-cast one at room temperature.The improved mechanical behaviors are mainly attributed to LPSO phase kink-banding strengthening at low temperature and the precipitation strengthening of a large amount of fine(Mg,Zn)_(3)Y particles at high temperature after SHP treatment.It reveals the SHP is an effective approach to prepare high performance Mg alloys.
基金Supported by the National Natural Science Foundation of China(51676099,51376090)the Natural Science Foundation of Jiangsu Province(BK20180473)。
文摘To deal with the problem that the initial velocity of the bullet is difficult to increase,the research on the super-high initial velocity propulsion in the barrel weapon with an adaptive pressure-maintaining chamber are conducted.Considering the law of gun-powder burning and the flow characteristics of gun-powder gas in multi-chamber,the scheme of super-high initial velocity propulsion with an adaptive pressure-maintaining chamber is designed,the ballistic model of the barrel weapon with super-high velocity bullet propulsion is established.The research results show that the technical scheme can greatly increase the initial velocity of the bullet with the peak pressure keeping nearly the same as the tradition barrel weapon.The research results can provide a theoretical foundation to significantly increase the initial velocity in barrel weapons using solid propellants,and have an important reference value to comprehensively increase the power of the barrel weapons.
基金supported by the National Natural Science Foundation of China (Grant No.52274290)the Basic Science Center Project for the National Natural Science Foundation of China (No.72088101).
文摘Horizontal segregation has been a constraint to the development and application of super-high bed sintering.To eliminate the horizontal segregation of super-high bed sintering,several typical sintering machines were sampled and analyzed,and theoretical calculation was made to compare the bed depth and their differences in different areas within the mixture bin.Then,solutions were proposed and applied to a 265 m^(2) sintering machine.The results showed that the horizontal seg-regation of the 265 m^(2) sintering machine was dominated by particles larger than 8 mm with horizontal segregation degree of 0.48,while 360 and 550 m^(2) sintering machines were affected by 5-8 mm and 1-3 mm particles with horizontal segregation degree of 0.27 and 0.31,respectively.Causes analysis indicated the different segregation distribution results from the matching of the bed depth of each area within the mixture bin.Finally,the horizontal segregation degree not larger than 0.06 was achieved by optimizing the time parameters and the division of three zones on the 265 m^(2) sintering machine.
基金supported by the National Natural Science Foundation of China(Grant No.52274290)the Basic Science Center Project for the National Natural Science Foundation of China(No.72088101).
文摘Super-high bed sintering process is an important development direction of iron ore sintering for its lower emission and higher yield.However,there is a lack of deep understanding of the uneven quality of super-high bed sintering products,and the deterioration of reduction disintegration performance,the thickening of hearth layer and the reduction in energy-saving effect are perplexing enterprises and researchers.To ascertain the problems of super-high bed sintering,ten sintering machines with the areas of 265,280,360,550 and 660 m^(2)and bed depth above 900 mm were sampled and analyzed.The results showed that problems were mainly shown in the unevenness of chemical composition,macrostructure,mechanical strength and metallurgical performance.The chemical composition exhibits severe segregation in both horizontal and vertical directions,with basicity segregation reaching as high as 0.81.The uneven macrostructure of sinter is reflected in a 10%difference in porosity and mechanical strength increase in 16%–19%along the vertical direction.The reducibility and reduction disintegration performance gradually deteriorate along the bed depth,with a difference of 10.5%in reducibility and 7.3%in RDI−0.5 mm(reduction disintegration index of sinter with size smaller than 0.5 mm).
基金This work was supported by the National Natural Science Foundation of China(Grant No.52274290).
文摘The inhomogeneous sinter properties in super-high bed sintering have been reported in our previous research.To inves-tigate the reasons for the inhomogeneous phenomena,detailed sampling and analysis of mixed material bed and sintered bed in super-high bed sintering plant were executed.The results indicated that the higher porosity and thinner dendrite of silico-ferrite of calcium and aluminum in the upper layer as well as dense structure and higher secondary hematite content in the lower layer led to the heterogeneities of mechanical strength and reduction properties exceeding 20%and 10%,respectively.From the bed top downward,the basicity of mixed material decreased from 2.13 to 1.68 because the average particle size increased from 2.65 to 4.56 mm.Fluxes and fuels gathered in finer particles(-3 mm)of mixed material,and the-3 mm particles of mixed material generated more liquid phase than+3 mm ones.The heat input of super-high sintering bed was inhomogeneous due to the heat accumulation effect and unreasonable fuel distribution.The inhomo-geneous sintering heat condition in sintering bed resulted in the different quantities and properties of liquid phase.The inhomogeneous quantities and properties of liquid phase that were influenced by inhomogeneous distribution of chemical composition,particle size,and heat input led to inhomogeneous mineralizing results.Homogeneous mineralizing condition is the key for homogeneous super-high bed sintering.
文摘Based on break characteristics of roofs in fully mechanized top-coal mining of thick shallow coal seams, a fracture mechanics model was built, and the criterion of crack propagation in the main roof was derived using the fracture mechanics theory. The relationships between the fracture length of the roof and the working resistance of the supports were discovered, and the correlations between the load on the overlying strata and the ratio of the crack's length to the thickness of the roof were obtained. Using a working face of Jindi Coal Mine, Xing county Shanxi province as an example, the relationships between the fracture length of the roof and the working resistance of the supports were analysed in detail. The results give a design basis in hydraulic top coal caving supports, which could provide useful references in the practical application. On-site experiment proves that the periodic weighting step interval of the caving face is 15–16 m, which is basically consistent with the theoretical analysis results, and indicates that the mechanized caving hydraulic support is capable of meeting the support requirements in the mining of a super-thick but shallowly buried coal seam.
文摘High-efficiency abrasive process with CBN grinding wheel is one of the important techniques of advanced manufacture. Combined with raw and finishing machining, it can attain high material removal rate like turning, milling and planning. The difficult-to-grinding materials can also be ground by means of this method with high performance. In the present paper, development status and latest progresses on high-efficiency abrasive machining technologies with CBN grinding wheel relate to high speed and super-high speed grinding, quick point-grinding, high efficiency deep-cut grinding, creep feed deep grinding, heavy-duty snagging and abrasive belt grinding were summarized. The efficiency and parameters range of these abrasive machining processes were compared. The key technologies of high efficiency abrasive machining, including grinding wheel, spindle and bearing, grinder, coolant supplying, installation and orientation of wheel and workpiece and safety defended, as well as intelligent monitor and NC grinding were investigated. It is concluded that high efficiency abrasive machining is a promising technology in the future.
文摘Based on the space spherical symmetry of 3-dimensional and the translational symmetry of time and the uncertainty principle, a 4-dimensional space-time cylinder model of quarks and leptons is established. With this model, equations of the special relativity can be extended more perfectly, thereby achieving a unity of the special relativity and quantum mechanics in deeper level. New equations can not only interpret issues explained by old equations but also solve several important pending problems. For example, a formula to strictly calculate the coefficient ξ of Lorentz invariance violation (LIV) is derived, to above 4 × 1019 eV UHECR protons the calculated |ξ| -30, although there is the LIV effect it is too weak to change the GZK cutoff, which is consistent with observations of HiRes and Auger;Also, a relation formula between the Hubble constant and several basic constants is derived, thus theoretically calculated H0 = 70.937 km·s-1·Mpc-1, which is well consistent with the final observation result of HST Key Project. In addition, an unusual effect predicted by new equations can be experimentally tested in the electron storage ring;a preliminary experiment result has hinted its signs of existence.
基金supported by the National Natural Science Foundation of China (62175040, 61805044, 12064027, and 62065014)the Science and Technology Program of Guangzhou(202201010242)+3 种基金Guangdong Basic and Applied Basic Research Foundation(2022A1515110981)2022 Jiangxi Province High-level and High-skilled Leading Talent Training Project Selected (No. 63)Jiangxi Provincial Department of Education Science and Technology Key Project (GJJ2204302)Jiujiang Municipal Science and Technology Program (Natural Science Foundation, Innovative Talents)(2022-2023)。
基金Project supported by National Natural Science Foundation of China(51475486)Natural Science Foundation of Hebei Province(E2013501096)
文摘The microstructure of Mg-8Zn-1Y alloy solidified under super-high pressure was analyzed through X-ray diffraction(XRD), scanning electron microscopy(SEM) and energy dispersive spectroscopy(EDS). And, compression deformation behavior at room-temperature was studied. The results showed that the microstructure of Mg-8Zn-1Y alloy solidified under ambient pressure and super-high pressure was both mainly composed of ■-Mg and quasicrystal I-Mg3Zn6 Y. Solidification under super-high pressure contributed to refining solidified microstructure and changing morphology of the intergranular second phase. The morphology of intergranular second phase(quasicrystal I-Mg3Zn6Y) was transformed from continuous network(ambient pressure) to long island(high pressure) and finally to granular(super-high pressure) with the increase in pressure. The compressive strength, yield strength and rupture strain of the samples solidified under ambient pressure were significantly improved from 262.6 MPa, 244.4 MPa and 13.3% to 437.3 MPa, 368.9 MPa and 24.7% under the pressure of 6 GPa, respectively. Under ambient pressure, cleavage plane on compressive fracture was large and smooth. When it was solidified under the pressure ranging from 4 to 6 GPa, cleavage plane on compressive fracture was small and coarse. In addition, dimple, tear ridge and lobate patterns existed.
基金supported by the National Natural Science Foundation of China(NSFC)(No.61775222)Youth Innovation Promotion Association of the ChineseAcademy of Sciences(No.2017292)the International Partnership Program of Chinese Academy of Sciences(No.18123IKYSB20170022)。
文摘The Laguerre-Gaussian(LG)mode beam has very important applications in many research fields.Here,the Theon sieve is first introduced into the laser resonator to generate petal-like laser beams by coherently superimposing two high-order LG modes.The effectiveness was verified by GLAD software.The petal-like laser beam is derived from the light field redistribution and coherent superposition caused by the diffraction effect of the Theon sieve.The relationship between the order of the petal-like laser and the cavity structures has also been investigated in detail.Light field operation in the laser cavity greatly simplifies the optical structure and is more beneficial to optical diagnostics and imaging.
基金Sponsored by National Key Technology Research and Development Program in 11th Five-Year Plan of China (2006BAE03A08)Special Program for Key Research of National Basic Research Program of China (2011CB606306-2)Fundamental Research Funds for Central Universities of China (N090607003)
文摘CO2-shielded welding experiments of newly developed, 780 MPa super-high strength heavy-duty truck crossbeam steel were conducted, and the microstructure, microhardness, mechanical properties, and impact tough- hess of the welded joint were studied. The evolution of the microstructure of the welded joint occurred as follows.. welding seam (acicular ferrite+proeutectoid ferrite)→fusion zone (granular bainite-long strip M/A island)→coarse grain zone (granular bainite-long strip or short bar M/A island)→fine grain zone (ferrite+ pearlite+ blocky M/A is- land)→mixed grained zone (ferrite+granular bainite+blocky M/A island)→base metal (proeutectoid ferrite+gran- ular bainite-hlocky or granular M/A island). Increasing the density of the grain boundaries can effectively improve the impact toughness, and the blocky M/A island hindered crack propagation more effectively than the long strip M/A island. The new hot-rolled 780 MPa super-high strength steel had excellent weldability. The welding technology was applied under the following conditions: welding voltage was 20 to 21 V, welding current was 200 to 210 A, and the gas flow rate was 25 L/rain.
基金The work was financially supported by the National Natural Science Foundation of China(No.21544005)the Basic Research Program(Natural Science Foundation for Young Scholars)of Jiangsu Province(No.BK20170489)+3 种基金the Materials and Chemical Engineering Research Center of Xinjiang Production and Construction Corps(No.2018BTRC003)the Joint Project of Yangzhou City and Higher Education Institutions(No.YZ2019127)the Innovation Incubation Project of Yangzhou University(No.2019CXJ025)the Priority Academic Program Development of Jiangsu Higher Education Institutions.
文摘An aqueous nanosuspension of agrochemicals unlike pharmaceutics has to achieve massive production in an effective way,capable to ensure sufficient profits in commercialization.This work implements the flash nanoprecipitation(FNP)technique to effectively generate agrochemical nanosuspension,anticipatedly overcoming such an obstacle.Azoxystrobin,a broad spectrum fungicide,in either acetone or ethanol is used herein as a mode agrochemical.To ensure a green and practical utilization,three kinds of commercially available and eco-friendly surfactants,i.e.,poly(ethylene glycol)-block-poly(lactic-co-glycolic acid)(PEG-b-PLGA),Tween 80 and alkyl polyglucosides(APGs),are employed for stabilizing the nanoparticles.The results show that the polymeric stabilizer,PEG-b-PLGA,has the best stabilization efficiency,and can maintain the particles below 100 nm for at least three weeks.The azoxystrobin load of the nanoparticles reaches as high as 77 wt.%,beneficial to enhancing the biological potency.Moreover,the FNP brings the particles a much smaller size,narrower size distribution,better size stability,and higher biological efficacy than the ones made via a traditional method of the drop and stir(DS).The nanosuspensions present superior fungicidal performances over a prevailing counterpart from Syngenta.This study proves an enhanced biological potency and reduced dosage of agrochemical nanosuspension made via the FNP,indicating a remarkable advantage of the FNP over the conventional preparation.The integration of a super-high load,eco-friendly excipients,intensified preparation process,enhanced potency,and reduced dosage creates a promising pathway to generate a green aqueous nanosuspension of agrochemicals.
文摘With the support by the National Natural Science Foundation of China,the research team led by Prof.Fang QianRong(方千荣)at the State Key Laboratory of Inorganic Synthesis and Preparative Chemistry,Jilin University,developed a crystalline porous material(CPM)with super-high chemical stability,which was published in Nat Chem(2019,11,doi:10.1038/s41557-019-0238-5).
基金supported by the National Basic Research Program of China (2012CB932800, 2014CB932700)the National Natural Science Foundation of China (21503212, 21503211, 21433003, 21422307, and 21303180)the financial support from U.S. Department of Energy, Office of Energy Efficiency and Renewable Energy, Fuel Cell Technologies Office
文摘We demonstrate a new and simple method for pre-treating the carbon material and iron precursor to prepare oxygen reduction reaction(ORR) catalysts, which can produce super-high performance and stability in alkaline solution, with high performance in acid solution. This strategy using cheap materials is simply controllable. Moreover, it has achieved smaller uniform nanoparticles to exhibit high stability, and the synergetic effect of Fe and N offered much higher performance in ORR than commercial Pt/C, with high maximum power density in alkaline and acid fuel cell test. So it can make this kind of catalysts be the most promising alternatives of Pt-based catalysts with best performance/price.