Transparent ZnO/glass surface acoustic wave based high performance ultraviolet light sensors

Surface acoustic wave （SAW） resonators are a type of ultraviolet （UV） light sensors with high sensitivity, and they have been extensively studied. Transparent SAW devices are very useful and can be developed into various sensors and microfluidics for sensing/monitoring and lab-on-chip applications. We report the fabrication of high sensitivity SAW UV sensors based on piezoelectric （PE） ZnO thin films deposited on glass substrates. The sensors were fabricated and their performances against the post-deposition annealing condition were investigated. It was found that the UV-light sensitivity is improved by more than one order of magnitude after annealing. The frequency response increases significantly and the response becomes much faster. The optimized devices also show a small temperature coefficient of frequency and excellent repeatability and stability, demonstrating its potential for UV-light sensing application.

Surface Acoustic Wave Humidity Sensors Based on(1120) ZnO Piezoelectric Films Sputtered on R-Sapphire Substrates

ZnO films on R-sapphire substrates are prepared and characterized by x-ray diffraction and scanning electron microscopy, which indicate that the thin films are well crystallized with （1120） texture. Love wave and Rayleigh wave are used for fabrications of humidity sensors, which are excited in [1100] and [0001] directions of the （1120） ZnO piezoelectric films, respectively. The experimental results show that both kinds of sensors have good humidity response and repeatability, and the performances of the Love wave sensors are better than those of the Rayleigh wave sensors at room temperature. Moreover, the theoretical calculations of the mass sensitivity of the sensors are a/so carried out and the calculated results are in good agreement with the experimental measurements.

Viscoelastic Analysis of a Surface Acoustic Wave Gas Sensor Coated by a New Deposition Technique

与聚合物涂的声学的波浪传感器基于新涂层免职(自我装配、分子地印的技术) 拍摄的表面的反应的分析被描述，反应公式因此被推出。用真实部分砍模量，聚合物能被分类进三种类型：玻璃质的电影，玻璃质似橡胶的电影和似橡胶的电影。试验性的结果比在马丁的理论，而是速度反应不确切与计算一致的证明变细反应在有模拟的更好的坚固性。也许，它被试验性的方法和环境影响。另外，为聚合物电影的煤气的吸着的模拟被执行。，至于玻璃质似橡胶的电影和似橡胶的电影至于玻璃质的电影，有增加电影厚度的锯传感器反应增加，和在传感器反应和气体的集中之间的关系是相当线性的，在传感器敏感和气体的集中之间的关系是很复杂的。最终计算的结果显示在传感器反应和频率之间的关系不由于聚合物的粘弹性的性质总是是线性的。

Strain transfer mechanism of passive wireless surface acoustic wave torque sensors using shear lag theory

A shear-lag theory was developed to investigate the strain transfer from the metal substrate to the surface acoustic wave （SAW） resonator through a bonding layer. A three-layer model of host structure-adhesive layer-resonator layer was established. The strain transfer was theoretically analyzed, and the main factors impacting the SAW sensor measurement were studied. The relationship between the sensor response and the individual effect of all these factors under static loads was discussed. Results showed that better accuracy could be achieved with increase in the adhesive stiffness or resonator length, or decrease in the adhesive thickness. The values of the strain transfer rate calculated from the analytical model agreed well with that from the available experiment data.

Development of A Surface Acoustic Wave LB Membrane Immunity Sensor

Summary: A new kind of biosensor for immunology was developed by ultrasonic technique and LB membrane. A double delay-line resonator was made by using ST-cut quartz crystal with working frequency of 149. 7 MHz. Then a layer of LB membrane was covered on it. When anti-IgM anti- body of various concentrations was added to it, the sensor can be used to detect IgM antigen. The biosensor was highly sensitive, small and light. The experimental results showed that the working frequency change of the sensor was proportional to the concentration of antibody with its dilution ratio between 1: 10000 and 1: 100. It was also first observed that the frequency curve of the sen- sor resulting from the reaction of IgM antigen and antibody undulated in the experiment.

基于软件无线电方案无线无源SAW温度阅读器设计

目前谐振型声表面波(SAW)阅读器射频电路大多采取分立器件设计,针对系统整体工作频段受限,硬件设计繁琐的问题,该文提出了一种软件无线电方案。软件无线电系统主体由ZYNQ和AD9361组成,射频收发端口添加LNA、PA进行信号功率放大,使用射频开关隔离收发。通过发射步进频率5 kHz、带宽1 MHz扫频信号,并对回波进行频谱分析求取最大值,最终得到谐振频率。针对SAW传感器回波持续时间较短而导致FFT计算分辨率的不足,使用重复采集增加数据长度,将阅读器的分辨率提高到468.75 Hz。实验结果表明,该阅读器能够正确探测传感器温度变化。

Temperature Characteristics of Surface Acoustic Waves Propagating on La_3Ga_5SiO_4 Substrates

Langasite (LGS) is a novel piezoelectric crystal. The authors numerically analyses the temperature stability of surface acoustic waves (SAW) and the relation of SAW propagation with temperature on certain optimal cuts on LGS in this paper. The results show that LGS has better temperature stability than traditional piezo crystals. The results also demonstrate that the velocity of SAW decrease with temperature, the electro-mechanical coupling constant (k2) and temperature coefficient of frequency increases parabolically and the power flow angle increases linearly on certain optimal cuts of LGS. The calculation result compared with the experimental and show good agreement.

基于IDT/ZnO/AlN/Diamond结构的混合SAW/BAW压力敏感元件特性研究

利用有限元方法分析了基于IDT/ZnO/AlN/Diamond不同结构混合SAW/BAW器件的声学特性,包括层状薄膜结构、ZnO薄膜刻蚀结构和填充结构。结果表明,当h_(ZnO)/λ=0.3、h_(AlN)/λ=0.5,且ZnO被完全刻蚀(d/h_(ZnO)=1)时,刻蚀结构混合SAW/BAW(准西沙瓦波)的机电耦合系数(K^(2))取得最大值6.54%,比层状结构(d/h_(ZnO)=0)提升了近一倍。刻蚀结构中,SiO_(2)和Diamond填充物的引入不仅提高了准西沙瓦波的K_(2),而且改善了其压力传感特性。当d/h_(ZnO)=1时,SiO_(2)和Diamond填充结构准西沙瓦波的压力频移分别为81.2 kHz/MPa和207.4 kHz/MPa,比刻蚀结构分别提高了58.7%和300%;同时,Diamond填充物的引入使准西沙瓦波的频率压力系数(PCF)达到最大值297×10^(-6)/MPa,比d/h_(ZnO)=0时提高了约30%。由此可知,通过引入不同的填充物可以开发不同的功能传感器,在压力、温度和气敏等传感领域将具有极大的应用前景。

Surface Acoustic Wave Device with Reduced Insertion Loss by Electrospinning P(VDF–TrFE)/ZnO Nanocomposites

Surface acoustic wave(SAW) devices have been utilized for the sensing of chemical and biological phenomena in microscale for the past few decades. In this study, SAW device was fabricated by electrospinning poly(vinylidenefluoride-co-trifluoroethylene)(P(VDF-TrFE)) incorporated with zinc oxide(ZnO) nanoparticles over the delay line area of the SAW device. The morphology, composition, and crystallinity of P(VDF-TrFE)/ZnO nanocomposites were investigated. After measurement of SAW frequency response, it was found that the insertion loss of the SAW devices incorporated with ZnO nanoparticles was much less than that of the neat polymer-deposited device. The fabricated device was expected to be used in acoustic biosensors to detect and quantify the cell proliferation in cell culture systems.

Effect of Fluid Electrical Property Changes on Surface Transverse Wave Sensors

A fluid sensor based on the surface transverse wave (STW) delay line on ST-cut quartz has been developed and tested in a large number of fluids with different viscosity and permittivity levels.Influence of fluid mechanical and electrical properties on the sensor's response has been determined and the sensor's performance has been compared with a bulk acoustic wave (BAW) viscosity sensor.The result shows that the viscosity sensitivity of the developed STW sensor represented by the signal to noise ratio is lower than that of a 5 MHz BAW sensor.Applications of the sensor in detecting the quality of industrial fluids are discussed.

离子束刻蚀技术在SAW滤波器频率修整上的应用

随着声表面波(SAW)滤波器的应用向高频、窄带方向延伸,在制造过程中准确地控制其中心频率及一致性变得越来越困难,需要对SAW滤波器的频率进行微调。重点介绍了一种在SAW滤波器上可实现目标频率修整的离子束刻蚀修频工艺,通过实验发现刻蚀厚度不同对滤波器表面的影响程度不同,一次离子束刻蚀厚度为50 nm时,铝膜表面出现微结构变化。分析了对晶圆、器件进行离子刻蚀工艺引起热损伤的机理,表征了不同刻蚀厚度对SAW滤波器粘接芯片的剪切力和硅铝丝键合力的影响。根据实验现象及结果提出了分梯度多次刻蚀的优化方案,给出了不同刻蚀厚度的刻蚀精度,对实验结果进行拟合,得到中心频率与刻蚀厚度的关系方程,从频率、插入损耗和通带方面分析了离子束刻蚀工艺对SAW滤波器电学性能的影响。经离子束刻蚀修频后,滤波器中心频率提高2 MHz,中心频率标准差由0.4 MHz减少为0.15 MHz,中心频率的均一性由0.29%改善至0.11%,频率一致性变好。

Propagation Characteristics of Surface Acoustic Waves on LGT and Quartz Substrates

Langatate( LGT) is a novel piezoelectric crystal; its structure is similar to quartz. A numerical analysis of the most important propagation characteristics of surface acoustic waves( SAW) on LGT and quartz is presented in this paper. The results show that the phase velocity on LGT is slower than that on quartz.Similar to quartz,there are zero temperature cuts and pure module orientations on LGT. The electro-mechanical coupling constant( k2)of LGT is larger than that of quartz. The characteristics of SAW on LGT with different material constants are calculated and compared.The results show that there are somewhat deviations with different material constants. Especially, the temperature coefficient of frequency( TCF) shows a relatively high difference.

Application of PRO-ESPRIT algorithm in identification of surface acoustic wave identification-tags

The surface acoustic wave （SAW） identification （ID）-tags have great potential for application in radio frequency identification （RFID） due to their characteristics of wireless sensing and passive operation. In the measurements based on the frequency domain sampling （FDS）, to expand the range of detection and allow the system work in harsh environments, it is necessary to enhance the identification capability at low SNR. In addition, to identify the tags in real time, it is important to reduce identification time. Therefore, estimation of signal parameters based on the Procrustes rotations via the rotational invariance technique （PRO-ESPRIT） is adopted. Experimental results show that good identification capability is achieved with a relatively faster measurement speed.

Influence of the anisotropy on the magneto-acoustic response of magnetic surface acoustic wave resonators

One-port magnetic surface acoustic wave(MSAW) resonators are fabricated by stacking multilayered(FeCoSiB/SiO2)n films directly on top of interdigital electrodes. It is shown that the magneto-acoustic response of the MSAW resonators critically depends the hysteresis of △E effect. For the magnetic multilayer without induced magnetic anisotropy, the resonance frequency( fR) exhibits a butterfly-like dependence on the external field, therefore, enabling bipolar detection of magnetic field smaller than its coercive field. However, for the magnetic multilayers with induced magnetic anisotropy, butterfly-like or loop-like fR–H curves are measured along the interdigtial electrode fingers or the SAW propagation direction, which can be attributed to the competition between the magnetic field-induced anisotropy and the stress-induced or shape anisotropy.

A Novel Wireless PassiveTemperature-Pressure SAW-based Sensor

A novel wireless and passive surface acoustic wave(SAW)sensor is developed for measuring temperature and pressure.The sensor has two single-port resonators on a substrate.One resonator,acting as the temperature sensor,is located at the fixed end without pressure deformation,and the other one,acting as the pressure sensor,is located at the free end to detect pressure changes due to substrate deformation.Pressure at the free end bends the cantilever,causing a relative change in the acoustic propagation characteristics of the SAW traveling along the surface of the substrate and a relative change in the resonant frequency of the resulting signal.The temperature acts on the entire substrate,affecting the propagation speed of the SAW on the substrate and directly affecting the resonant frequency characteristic parameters.The temperature and pressure performance of this new antenna-connected sensor is tested by using a network analyzer,a constant temperature heating station,and a force gauge.A temperature sensitivity of 1.5015 kHz/℃and a pressure sensitivity of 10.6 kHz/gf at the ambient temperature have been observed by wireless measurements.This work should result in practical engineering applications for high-temperature devices.

结构参数对SAW传感器的影响及电极失效分析

文中通过实验制备了一种以LiNbO_(3)为压电基底,Pt为电极,SiO_(2)为保护层的单端口谐振型声表面波传感器,探究了IDT与反射栅之间的距离Lg和电极宽度对SAW传感器的影响,揭示了不同温度下电极的微观变化规律,结果表明:当L_(g)=λ/2时,SAW传感器可以激发1个稳定的谐振峰,寄生峰对其影响较小;当L_(g)=3λ/8时,可以激发2个稳定的谐振峰;随着电极宽度的增加,声表面波传感器的波速和温度敏感性降低;700℃时,电极的部分结构开始变窄,随着温度的升高,电极和保护层凝聚收缩形成微小的孔洞,当温度达到950~1000℃时,电极熔化失效。

Bulk GaN-based SAW resonators with high quality factors for wireless temperature sensor

Surface acoustic wave(SAW)resonator with outstanding quality factors of 4829/6775 at the resonant/anti-resonant frequencies has been demonstrated on C-doped semi-insulating bulk GaN.The impact of device parameters including aspect ratio of length to width of resonators,number of interdigital transducers,and acoustic propagation direction on resonator performance have been studied.For the first time,we demonstrate wireless temperature sensing from 21.6 to 120℃ with a stable temperature coefficient of frequency of–24.3 ppm/℃ on bulk GaN-based SAW resonators.

UV light driven high-performance room temperature surface acoustic wave NH_(3) gas sensor using sulfur-doped g-C_(3)N_(4) quantum dots

Nanomaterials integrated surface acoustic wave(SAW)gas sensing technology has emerged as a promising candidate for realtime toxic gas sensing applications for environmental and human health safety.However,the development of novel chemical interface based on two-dimensional(2D)sensing materials for SAW sensors for the rapid and sensitive detection of NH_(3)gas at room temperature(RT)still remains challenging.Herein,we report a highly selective RT NH_(3)gas sensor based on sulfur-doped graphitic carbon nitride quantum dots(S@g-C_(3)N_(4)QD)coated langasite(LGS)SAW sensor with enhanced sensitivity and recovery rate under ultraviolet(UV)illumination.Fascinatingly,the sensitivity of the S@g-C_(3)N_(4)QD/LGS SAW sensor to NH_(3)(500 ppb)at RT is dramatically enhanced by~4.5-fold with a low detection limit(~85 ppb),high selectivity,excellent reproducibility,fast response/recovery time(70 s/79 s)under UV activation(365 nm)as compared to dark condition.Additionally,the proposed sensor exhibited augmented NH_(3)detection capability across the broad range of relative humidity(20%–80%).Such remarkable gas sensing performances of the as-prepared sensor to NH_(3)are attributed to the high surface area,enhanced functional groups,sulfur defects,UV photogenerated charge carriers,facile charge transfer in the S@g-C_(3)N_(4)QD sensing layer,which further helps to improve the gas molecules adsorption that causes the increase in conductivity,resulting in larger frequency responses.The gas sensing mechanism of S@g-C_(3)N_(4)QD/LGS SAW sensor is ascribed to the enhanced electroacoustic effect,which is supported by the correlation of resistive type and COMSOL Multiphysics simulation studies.We envisage that the present work paves a promising strategy to develop the next generation 2D g-C_(3)N_(4)based high responsive RT SAW gas sensors.

基于SAW的电缆接头内部测温天线研究

由于声表面波(SAW)测温技术因具有无源无线的特点而备受研究人员的广泛关注。该技术可应用在电缆接头内部的温度测量中,但因受电缆接头材料和结构的影响,使SAW测温信号传递受阻,严重影响了温度信号的检测。该文基于DWG-630A型电缆接头的结构和材料,设计了一款可用于电缆接头内部测温的天线。通过其理论分析、仿真及试验验证,证明该设计切实可行。结果表明,穿过电缆接头可传递SAW温度信号,并在工作频段内具有良好的增益和辐射效果。

SAW压力传感器声传播方向特性研究

针对高温恶劣环境下对压力参数的测量需求,结合目前氮化铝(AlN)和蓝宝石(sapphire)等耐高温材料,构建了一种叉指换能器(IDT)/AlN/Sapphire结构的声表面波(SAW)传感器模型,并采用有限元法(FEM)分析SAW在c轴取向AlN薄膜上分别沿a方向(〈11-20〉)和m方向(〈1-100〉)传播时的器件性能,包括AlN和IDT的厚度对声速和机电耦合系数的影响,以及不同方向传播时SAW压力传感器灵敏度的变化。实验结果表明:表面波沿a方向传播的传感器相比于m方向明显具有更高的声速与机电耦合系数,2个方向的传感器灵敏度分别为435.37×10^(-6)/MPa和426.29×10^(-6)/MPa,a方向灵敏度略大于m方向。此研究工作为之后的传感器设计制造提供了一定的参考价值。