Flow softening behavior of a homogenized Mg-7Gd-4Y-1Nd-0.5Zr alloy under compression to a final strain of∼1.8 at elevated temperatures of 450∼550℃ and a constant strain rate of 2s^(−1) has been investigated by opti...Flow softening behavior of a homogenized Mg-7Gd-4Y-1Nd-0.5Zr alloy under compression to a final strain of∼1.8 at elevated temperatures of 450∼550℃ and a constant strain rate of 2s^(−1) has been investigated by optical microscopy,scanning electron microscopy,electron back-scattered diffraction and transmission electron microscopy.The results show that true stress first rises to the peak point and then drops to the bottom value and increases again with further increasing strain at each temperature.Twinning dynamic recrystallization(DRX)and continuous DRX contribute to the formation of new fine grains at temperatures 450∼475℃ when the restoration is caused by both DRX and texture change due to extension twinning,resulting in the larger softening degrees compared with the softening effects owing to continuous DRX and discontinuous DRX at 500∼550℃ when twinning activation is suppressed.500℃ is the transition temperature denoting a significant decline in the contribution of twinning and TDRX to the strain with increasing temperature.The cuboid-shape phase exists in both homogenized and compressed samples,while the compositions are varied.展开更多
The dynamic evolution of microstructure and the characteristics of deformation , as well as the relationshipbetween them have ben studied for TCll alloy with different original conditions, including as-cast, as-rolled...The dynamic evolution of microstructure and the characteristics of deformation , as well as the relationshipbetween them have ben studied for TCll alloy with different original conditions, including as-cast, as-rolled ,as-forged and as-predeformed on casting, during comparison at constant temperature (CCT). The resultsshow that (1) Micrcotructural process during CCT of cast TCll comprises two stages: (i) Founding ofu dynamic equilibrium ”. Original coarse structure breaks up and becomes equiaxed, while the stras decreasesaccordingly. The microstructure gradually trends towards some kind of “dynamic ellullibrium” morphology;(ii) Keeping of “dynamic equilibrium”. Both stress and micrcostructural morphology preserve stable althoughdeformation continues. (2) The final pouilibrium morphology das not depend on its initial microstructure, buton the parameter Z(T, e) .展开更多
To explore the effect of strain rate ε on the high temperature deformation characteristics of ultrafine-grained materials, the deformation and damage features as well as microstructures of ECAP-treated pure Al at dif...To explore the effect of strain rate ε on the high temperature deformation characteristics of ultrafine-grained materials, the deformation and damage features as well as microstructures of ECAP-treated pure Al at different temperatures T and strain ratesε were systematically studied through compression tests and microscopic observations. The increase in ε eliminates strain softening at T≤473 K, and largely enhances the yield strength and flow stress at 473?573 K. The shear deformation dominates the plastic deformation of ECAP-treated Al. Many cracks along shear bands (SBs) are formed at T≥473 K and secondary SBs basically disappear at 1×10?3 s?1; however, at 1×10?2 s?1, cracks are only observed at temperature below 473 K, and secondary SBs become clearer at T≥473 K. The microstructures of ECAP-treated Al mainly consist of sub-grains (SGs). The increase in ε inhibits the SG growth, thus leading to the increases both in yield strength and flow stress at high temperatures.展开更多
Carbon is an important alloying element in improving high temperature mechanical properties of various metallic materials.The effects of carbon on high temperature mechanical properties of aβ-stabilized Ti?45Al?3Fe?2...Carbon is an important alloying element in improving high temperature mechanical properties of various metallic materials.The effects of carbon on high temperature mechanical properties of aβ-stabilized Ti?45Al?3Fe?2Mo(molar fraction,%)alloy were studied through compressive and creep tests.The results show that the carbon addition(0.5%,molar fraction)obviously enhances the high temperature compressive strength and creep resistance of theβ-stabilized Ti?45Al?3Fe?2Mo alloy.A lot of nano-scaled Ti3AlC carbides precipitate in theβ-stabilized alloy and these carbides pin the dislocations,and greatly increase the high temperature properties.At the same time,the carbon addition decreases the amount of?phase,refines the lamellar spacing,and causes solution strengthening,which also contribute to the improvement of the high temperature properties.展开更多
Compression tests A ere conducted in the two phase Ti46Al8.5Nb0.2W alloy with a cast microstructure under the strain rates ranging from 2x10(-5) s(-1) to 10(-2) s(-1) at temperatures ranging front 900degreesC to 1100d...Compression tests A ere conducted in the two phase Ti46Al8.5Nb0.2W alloy with a cast microstructure under the strain rates ranging from 2x10(-5) s(-1) to 10(-2) s(-1) at temperatures ranging front 900degreesC to 1100degreesC. It was found that there exist approximately linear relationships between the flow stress and the logarithm of strain rate at different temperatures. The strain rate dependence was analzed by the thermal activation theory and dislocation climbing is regarded as the controlling mechanism during high temperature compression tests.展开更多
High temperature compressive strength is one of the most important performances of resin sand; its value directly concerns the quality of castings. In order to seek the best testing method of resin sand high temperatu...High temperature compressive strength is one of the most important performances of resin sand; its value directly concerns the quality of castings. In order to seek the best testing method of resin sand high temperature compressive strength, a self-developed instrument was used to carry out experiments, and the sample shape and size were designed and studied. The results show that a hollow cylinder sample can reflect the strength difference of different resin sands better than a solid cylinder sample, and its data is stable. The experiments selected φ20/5×30 mm as the size of the hollow cylinder samples. The high temperature compressive strengths of phenol-formaldehyde resin coated sand, furan resin self-setting sand, and TEA resin sand were each tested. For the resin sand used for cast steel and cast iron, 1,000 ℃ was selected as the test temperature; for the resin sand used for cast non-ferrous alloy, 800 ℃ was selected as the test temperature; and for all the resin sand samples, 1 min was selected as the holding time. This testing method can truthfully reflect the high temperature performance of three kinds of resin sand; it is reproducible, and the variation coefficients of test values are under 10%.展开更多
This paper focuses on the effect of temperature on the out-of-plane compressive properties and failure mechanism of carbon fiber/epoxy composite pyramidal truss cores sandwich panels (CF/CPTSP). CFJCPTSP with novel ...This paper focuses on the effect of temperature on the out-of-plane compressive properties and failure mechanism of carbon fiber/epoxy composite pyramidal truss cores sandwich panels (CF/CPTSP). CFJCPTSP with novel reinforced frames are manufactured by the water jet cutting and interlocking assembly method in this paper. The theoretical analysis is presented to predict the out-of-plane compressive stiffness and strength of CFJCPTSP at different ambient temperatures. The tests of composite sandwich panels are per- formed throughout the temperature range from -90℃ to 180℃. Good agreement is found between theo- retical predictions and experimental measurements. Experimental results indicate that the low tempera- ture increases the compressive stiffness and strength of CF/CPTSP. However, the high temperature causes the degradation of the compressive stiffness and strength. Meanwhile, the effects of temperature on the failure mode of composite sandwich panels are also observed.展开更多
The influence of different lubricants on the deformation behaviour of IN 718 alloy was studied. The results show that, with the improvement of lubrication condition, the deformation of the alloy tends to be homogeneou...The influence of different lubricants on the deformation behaviour of IN 718 alloy was studied. The results show that, with the improvement of lubrication condition, the deformation of the alloy tends to be homogeneous, and the resistance of deformation decreases. Consequently, FR 2 glass lubricant is considered to be an ideal choice when the relationship between stress and strain of IN 718 alloy is measured by means of hot compression experiment.展开更多
Compressed air energy storage is an energy storage technology with strong potential to play a significant role in balancing energy on transmission networks,owing to its use of mature technologies and low cost per unit...Compressed air energy storage is an energy storage technology with strong potential to play a significant role in balancing energy on transmission networks,owing to its use of mature technologies and low cost per unit of storage capacity.Adiabatic compressed air energy storage(A-CAES)systems typically compress air from ambient temperature in the charge phase and expand the air back to ambient temperature in the discharge phase.This papers explores the use of an innovative operating scheme for an A-CAES system aimed at lowering the total cost of the system for a given exergy storage capacity.The configuration proposed considers preheating of the air before compression which increases the fraction of the total exergy that is stored in the fom of high-grade heat in comparison to existing designs in which the main exergy storage medium is the compressed air itself.Storing a high fraction of the total exergy as heat allows reducing the capacity of costly pressure stores in the system and replacing it with cheaper thermal energy stores.Additionally,a configuration that integrates a system based on the aforementioned concept with solar thermal power or low-medium grade waste heat is introduced and thoroughly discussed.展开更多
The true stress-true strain curves of Ti-6Al-2Zr-IMO-IV alloy with hydrogen were obtained by hot compression test. The microstructures of the alloy before and after thermo-compression were observed. The apparent activ...The true stress-true strain curves of Ti-6Al-2Zr-IMO-IV alloy with hydrogen were obtained by hot compression test. The microstructures of the alloy before and after thermo-compression were observed. The apparent activation energies of deformation were calculated for the alloy with and without hydrogen. The behavior and mechanism of deformation for hydrogenated Ti-6A1-2Zr-IMO-IV alloy at high temperature were analyzed. The relationship between hydrogenation time and hydrogen content at 800 ℃ can be expressed as the equation: CH(t)=1.2-1.2exp(-t/120). The true stress-true strain curves of hot compression for Ti-6Al-2Zr-IMO-IV alloy with hydrogen first move down and then move up as hydrogen content increases. Appropriate hydrogen content can reduce the peak of flow stress to minimal value. The apparent activation energies of deformation of the alloy with 0.47% hydrogen content and without hydrogen were calculated as 140 kJ·mol^-1 and 390 kJ-mol^-1, respectively, at 800 ℃ and at strain rate 8.3×10^4 s^-1. The apparent activation energy of deformation increases when the strain rate enhances from 8.3×10^-4 s^-1 to 8.3×10^-2 s^-1.展开更多
The scanning electron microscope,transmission electron microscope,optical microscope,X-ray diffraction and hardness tests were used to investigate the effect of deformation parameters in unrecrystallization range on m...The scanning electron microscope,transmission electron microscope,optical microscope,X-ray diffraction and hardness tests were used to investigate the effect of deformation parameters in unrecrystallization range on microstructural characteristics in Al-bearing hot-rolled transformation-induced plasticity steel.The thermomechanical-controlled processing was carried out with thermomechanical simulation machine,and the samples were compressed to compression strains of 0,0.15,0.25 and 0.35 at compression temperatures of 850,900 and 950°C.The results showed that the volume fraction of polygonal ferrite increased with the increasing compression strain,while the volume fraction of retained austenite reached the maximum value at compression strain of 0.25.The volume fraction of polygonal ferrite decreased with the increasing compression temperature,whereas the volume fraction of retained austenite possessed the maximum value at compression temperature of 850°C.Some granular retained austenite was present in uncompressed samples,and some pearlite appeared at large compression strain,while the hardness of the samples exhibited the similar variation tendency to the volume fraction of retained austenite.展开更多
基金This work was supported by the Changsha University Talent Introduction Project(50800-92808)the Excellent youth project of Hunan Provincial Department of Education(19B055,18B418,19C0156)the Natural Science Foundation of Hunan Province of China(2020JJ4645).
文摘Flow softening behavior of a homogenized Mg-7Gd-4Y-1Nd-0.5Zr alloy under compression to a final strain of∼1.8 at elevated temperatures of 450∼550℃ and a constant strain rate of 2s^(−1) has been investigated by optical microscopy,scanning electron microscopy,electron back-scattered diffraction and transmission electron microscopy.The results show that true stress first rises to the peak point and then drops to the bottom value and increases again with further increasing strain at each temperature.Twinning dynamic recrystallization(DRX)and continuous DRX contribute to the formation of new fine grains at temperatures 450∼475℃ when the restoration is caused by both DRX and texture change due to extension twinning,resulting in the larger softening degrees compared with the softening effects owing to continuous DRX and discontinuous DRX at 500∼550℃ when twinning activation is suppressed.500℃ is the transition temperature denoting a significant decline in the contribution of twinning and TDRX to the strain with increasing temperature.The cuboid-shape phase exists in both homogenized and compressed samples,while the compositions are varied.
文摘The dynamic evolution of microstructure and the characteristics of deformation , as well as the relationshipbetween them have ben studied for TCll alloy with different original conditions, including as-cast, as-rolled ,as-forged and as-predeformed on casting, during comparison at constant temperature (CCT). The resultsshow that (1) Micrcotructural process during CCT of cast TCll comprises two stages: (i) Founding ofu dynamic equilibrium ”. Original coarse structure breaks up and becomes equiaxed, while the stras decreasesaccordingly. The microstructure gradually trends towards some kind of “dynamic ellullibrium” morphology;(ii) Keeping of “dynamic equilibrium”. Both stress and micrcostructural morphology preserve stable althoughdeformation continues. (2) The final pouilibrium morphology das not depend on its initial microstructure, buton the parameter Z(T, e) .
基金Projects(51231002,51271054,51571058,50671023)supported by the National Natural Science Foundation of China
文摘To explore the effect of strain rate ε on the high temperature deformation characteristics of ultrafine-grained materials, the deformation and damage features as well as microstructures of ECAP-treated pure Al at different temperatures T and strain ratesε were systematically studied through compression tests and microscopic observations. The increase in ε eliminates strain softening at T≤473 K, and largely enhances the yield strength and flow stress at 473?573 K. The shear deformation dominates the plastic deformation of ECAP-treated Al. Many cracks along shear bands (SBs) are formed at T≥473 K and secondary SBs basically disappear at 1×10?3 s?1; however, at 1×10?2 s?1, cracks are only observed at temperature below 473 K, and secondary SBs become clearer at T≥473 K. The microstructures of ECAP-treated Al mainly consist of sub-grains (SGs). The increase in ε inhibits the SG growth, thus leading to the increases both in yield strength and flow stress at high temperatures.
基金Project(2014CB6644002)supported by the National Basic Research Program of ChinaProject(2016YFB0700302)supported by the National Major Scientific Research Development Program,ChinaProject(2017JJ2311)supported by the Hunan Natural Science Foundation of China
文摘Carbon is an important alloying element in improving high temperature mechanical properties of various metallic materials.The effects of carbon on high temperature mechanical properties of aβ-stabilized Ti?45Al?3Fe?2Mo(molar fraction,%)alloy were studied through compressive and creep tests.The results show that the carbon addition(0.5%,molar fraction)obviously enhances the high temperature compressive strength and creep resistance of theβ-stabilized Ti?45Al?3Fe?2Mo alloy.A lot of nano-scaled Ti3AlC carbides precipitate in theβ-stabilized alloy and these carbides pin the dislocations,and greatly increase the high temperature properties.At the same time,the carbon addition decreases the amount of?phase,refines the lamellar spacing,and causes solution strengthening,which also contribute to the improvement of the high temperature properties.
文摘Compression tests A ere conducted in the two phase Ti46Al8.5Nb0.2W alloy with a cast microstructure under the strain rates ranging from 2x10(-5) s(-1) to 10(-2) s(-1) at temperatures ranging front 900degreesC to 1100degreesC. It was found that there exist approximately linear relationships between the flow stress and the logarithm of strain rate at different temperatures. The strain rate dependence was analzed by the thermal activation theory and dislocation climbing is regarded as the controlling mechanism during high temperature compression tests.
基金financially supported by the National Natural Science Foundation of China(No.51405002)
文摘High temperature compressive strength is one of the most important performances of resin sand; its value directly concerns the quality of castings. In order to seek the best testing method of resin sand high temperature compressive strength, a self-developed instrument was used to carry out experiments, and the sample shape and size were designed and studied. The results show that a hollow cylinder sample can reflect the strength difference of different resin sands better than a solid cylinder sample, and its data is stable. The experiments selected φ20/5×30 mm as the size of the hollow cylinder samples. The high temperature compressive strengths of phenol-formaldehyde resin coated sand, furan resin self-setting sand, and TEA resin sand were each tested. For the resin sand used for cast steel and cast iron, 1,000 ℃ was selected as the test temperature; for the resin sand used for cast non-ferrous alloy, 800 ℃ was selected as the test temperature; and for all the resin sand samples, 1 min was selected as the holding time. This testing method can truthfully reflect the high temperature performance of three kinds of resin sand; it is reproducible, and the variation coefficients of test values are under 10%.
基金supported by the Major State Basic Research Development Program of China (973 Program) under Grant No. 2011CB610303the National Natural Science Foundation of China under Grant No. 11432004
文摘This paper focuses on the effect of temperature on the out-of-plane compressive properties and failure mechanism of carbon fiber/epoxy composite pyramidal truss cores sandwich panels (CF/CPTSP). CFJCPTSP with novel reinforced frames are manufactured by the water jet cutting and interlocking assembly method in this paper. The theoretical analysis is presented to predict the out-of-plane compressive stiffness and strength of CFJCPTSP at different ambient temperatures. The tests of composite sandwich panels are per- formed throughout the temperature range from -90℃ to 180℃. Good agreement is found between theo- retical predictions and experimental measurements. Experimental results indicate that the low tempera- ture increases the compressive stiffness and strength of CF/CPTSP. However, the high temperature causes the degradation of the compressive stiffness and strength. Meanwhile, the effects of temperature on the failure mode of composite sandwich panels are also observed.
文摘The influence of different lubricants on the deformation behaviour of IN 718 alloy was studied. The results show that, with the improvement of lubrication condition, the deformation of the alloy tends to be homogeneous, and the resistance of deformation decreases. Consequently, FR 2 glass lubricant is considered to be an ideal choice when the relationship between stress and strain of IN 718 alloy is measured by means of hot compression experiment.
基金This work has been supported by the UK Engineering and Physical Sciences Research Council(EPSRC)through the NexGen-TEST(EP/LO14211/1),IMAGES(EP/K002228/1)and RESTLESS(EP/N001893/1)projects.
文摘Compressed air energy storage is an energy storage technology with strong potential to play a significant role in balancing energy on transmission networks,owing to its use of mature technologies and low cost per unit of storage capacity.Adiabatic compressed air energy storage(A-CAES)systems typically compress air from ambient temperature in the charge phase and expand the air back to ambient temperature in the discharge phase.This papers explores the use of an innovative operating scheme for an A-CAES system aimed at lowering the total cost of the system for a given exergy storage capacity.The configuration proposed considers preheating of the air before compression which increases the fraction of the total exergy that is stored in the fom of high-grade heat in comparison to existing designs in which the main exergy storage medium is the compressed air itself.Storing a high fraction of the total exergy as heat allows reducing the capacity of costly pressure stores in the system and replacing it with cheaper thermal energy stores.Additionally,a configuration that integrates a system based on the aforementioned concept with solar thermal power or low-medium grade waste heat is introduced and thoroughly discussed.
基金supported by the National Natural Science Foundation of China(No.50671028)
文摘The true stress-true strain curves of Ti-6Al-2Zr-IMO-IV alloy with hydrogen were obtained by hot compression test. The microstructures of the alloy before and after thermo-compression were observed. The apparent activation energies of deformation were calculated for the alloy with and without hydrogen. The behavior and mechanism of deformation for hydrogenated Ti-6A1-2Zr-IMO-IV alloy at high temperature were analyzed. The relationship between hydrogenation time and hydrogen content at 800 ℃ can be expressed as the equation: CH(t)=1.2-1.2exp(-t/120). The true stress-true strain curves of hot compression for Ti-6Al-2Zr-IMO-IV alloy with hydrogen first move down and then move up as hydrogen content increases. Appropriate hydrogen content can reduce the peak of flow stress to minimal value. The apparent activation energies of deformation of the alloy with 0.47% hydrogen content and without hydrogen were calculated as 140 kJ·mol^-1 and 390 kJ-mol^-1, respectively, at 800 ℃ and at strain rate 8.3×10^4 s^-1. The apparent activation energy of deformation increases when the strain rate enhances from 8.3×10^-4 s^-1 to 8.3×10^-2 s^-1.
基金the support from National Natural Science Foundation of China(No.51504063).R.D.K.Misra,an honorary professor,also acknowledges the continued collaboration with Northeastern University by providing guidance to students in research.
文摘The scanning electron microscope,transmission electron microscope,optical microscope,X-ray diffraction and hardness tests were used to investigate the effect of deformation parameters in unrecrystallization range on microstructural characteristics in Al-bearing hot-rolled transformation-induced plasticity steel.The thermomechanical-controlled processing was carried out with thermomechanical simulation machine,and the samples were compressed to compression strains of 0,0.15,0.25 and 0.35 at compression temperatures of 850,900 and 950°C.The results showed that the volume fraction of polygonal ferrite increased with the increasing compression strain,while the volume fraction of retained austenite reached the maximum value at compression strain of 0.25.The volume fraction of polygonal ferrite decreased with the increasing compression temperature,whereas the volume fraction of retained austenite possessed the maximum value at compression temperature of 850°C.Some granular retained austenite was present in uncompressed samples,and some pearlite appeared at large compression strain,while the hardness of the samples exhibited the similar variation tendency to the volume fraction of retained austenite.