We carry out detailed momentum-dependent and temperature-dependent measurements on Bi_2Sr_2CaCu_2O_(8+δ)(Bi2212) superconductor in the superconducting and pseudogap states by super-high resolution laser-based an...We carry out detailed momentum-dependent and temperature-dependent measurements on Bi_2Sr_2CaCu_2O_(8+δ)(Bi2212) superconductor in the superconducting and pseudogap states by super-high resolution laser-based angleresolved photoemission spectroscopy. The precise determination of the superconducting gap for the nearly optimally doped Bi2212(T_c= 91 K) at low temperature indicates that the momentum-dependence of the superconducting gap deviates from the standard d-wave form(cos(2Φ)). It can be alternatively fitted by including a high-order term(cos(6Φ)) in which the next nearest-neighbor interaction is considered. We find that the band structure near the antinodal region smoothly evolves across the pseudogap temperature without a signature of band reorganization which is distinct from that found in Bi_2Sr_2CuO_(6+δ) superconductors. This indicates that the band reorganization across the pseudogap temperature is not a universal behavior in cuprate superconductors.These results provide new insights in understanding the nature of the superconducting gap and pseudogap in high-temperature cuprate superconductors.展开更多
With the rapid development of infrared imaging technology in last decades, the application range of the nondestructive examination, including fatigue testing,is continuously wider. By reviewing the studies and utiliza...With the rapid development of infrared imaging technology in last decades, the application range of the nondestructive examination, including fatigue testing,is continuously wider. By reviewing the studies and utilizations of temperature evolution during metal undergoing cyclic loading, this paper provides a reference and also guidance for further research. According to the articles on fatigue temperature evolution, the present overview summarized general rule and characteristics of fatigue temperature evolution. The cause of this temperature evolution is specifically analyzed. Some fatigue life prediction methodologies based on the temperature evolution are systematically reviewed. Finally, a prospect of this research direction is given.展开更多
Powder in tube process(PIT) was adopted for the fabrication of single filament Bi-2223 tapes, and a heat treatment process including the first heat treatment(HT1), intermediate rolling(IR), and second heat treat...Powder in tube process(PIT) was adopted for the fabrication of single filament Bi-2223 tapes, and a heat treatment process including the first heat treatment(HT1), intermediate rolling(IR), and second heat treatment(HT2) was performed. The phase evolution mechanism and microstructure changes during these heat treatment processes were systematically discussed. The influences of HT1 parameters on the phase evolution process of Bi-2223 tapes were discussed. With the optimized HT1 process, a proper Bi-2223 content of about 90% was achieved. HT2 process was also optimized by adding a post annealing process. An obvious increase of current capacity was obtained due to the enhancement of intergrain connections. Single filament Bi-2223 tapes with the critical current of Ic-90 A were fabricated with the optimized sintering process.展开更多
To quickly predict the fatigue limit of 6061 aluminum alloy,two assessment methods based on the temperature evolution and the steady ratcheting strain difference under cyclic loading,respectively,were proposed.The tem...To quickly predict the fatigue limit of 6061 aluminum alloy,two assessment methods based on the temperature evolution and the steady ratcheting strain difference under cyclic loading,respectively,were proposed.The temperature evolutions during static and cyclic loadings were both measured by infrared thermography.Fatigue tests show that the temperature evolution was closely related to the cyclic loading,and the cyclic loading range can be divided into three sections according to the regular of temperature evolution in different section.The mechanism of temperature evolution under different cyclic loadings was also analyzed due to the thermoelastic,viscous,and thermoplastic effects.Additionally,ratcheting strain under cyclic loading was also measured,and the results show that the evolution of the ratcheting strain under cyclic loading above the fatigue limit undergone three stages:the first increasing stage,the second steady state,and the final abrupt increase stage.The fatigue limit of the 6061 aluminum alloy was quickly estimated based on transition point of linear fitting of temperature increase and the steady value of ratcheting strain difference.Besides,it is feasible and quick of the two methods by the proof of the traditional S-N curve.展开更多
(Na, K)NbO3 (KNN) powders were successfully prepared by high temperature mixing method (HTMM) under hydrothermal conditions to study the effect of reaction time on the formation of KNN for three K+/(K+ +Na+...(Na, K)NbO3 (KNN) powders were successfully prepared by high temperature mixing method (HTMM) under hydrothermal conditions to study the effect of reaction time on the formation of KNN for three K+/(K+ +Na+) ratios of 0.6, 0.7 and 0.8. The products were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), transmission electron microscopy (TEM) and selected area electron diffraction (SAED), to show the change of phase and morphology of the as-prepared particles with the K+/(K+ + Na+) molar ratio in the solution. Pure Na-rich KNN monoclinic phase and pure K-rich KNN orthorhombic phase could be obtained quickly after mixing the solutions at high temperature when the K+/(K+ +Na+) molar ratio was either 0.6 or 0.8. When the K+/(K+ +Na+) molar ratio was 0.7, however, the K-rich KNN orthorhombic phase grain formed first, followed by the Na-rich KNN monoclinic phase grain, with the two phases coexisting in the final product.展开更多
Temperature rise is a significant factor influencing microstructure during(α+β) deformation of TA15 titanium alloy.An experiment was designed to explore microstructure evolution induced by temperature rise due to...Temperature rise is a significant factor influencing microstructure during(α+β) deformation of TA15 titanium alloy.An experiment was designed to explore microstructure evolution induced by temperature rise due to deformation heat.The experiment was carried out in(α+β) phase field at typical temperature rise rates.The microstructures of the alloy under different temperature rise rates were observed by scanning electron microscopy(SEM).It is found that the dissolution rate of primary equiaxed a phase increases with the increase in both temperature and temperature rise rate.In the same temperature range,the higher the temperature rise rate is,the larger the final content and grain size of primary equiaxed a phase are due to less dissolution time.To quantitatively depict the evolution behavior of primary equiaxed a phase under any temperature rise rates,the dissolution kinetics of primary equiaxed a phase were well described by a diffusion model.The model predictions,including content and grain size of primary equiaxed a phase,are in good agreement with experimental observations.The work provides an important basis for the prediction and control of microstructure during hot working of titanium alloy.展开更多
Through molecular dynamics(MD) simulation, the dependencies of temperature, grain size and strain rate on the mechanical properties were studied. The simulation results demonstrated that the strain rate from 0.05 to...Through molecular dynamics(MD) simulation, the dependencies of temperature, grain size and strain rate on the mechanical properties were studied. The simulation results demonstrated that the strain rate from 0.05 to 2 ns–1 affected the Young's modulus of nickel nanowires slightly, whereas the yield stress increased. The Young's modulus decreased approximately linearly; however, the yield stress firstly increased and subsequently dropped as the temperature increased. The Young's modulus and yield stress increased as the mean grain size increased from 2.66 to 6.72 nm. Moreover, certain efforts have been made in the microstructure evolution with mechanical properties association under uniaxial tension. Certain phenomena such as the formation of twin structures, which were found in nanowires with larger grain size at higher strain rate and lower temperature, as well as the movement of grain boundaries and dislocation, were detected and discussed in detail. The results demonstrated that the plastic deformation was mainly accommodated by the motion of grain boundaries for smaller grain size. However, for larger grain size, the formations of stacking faults and twins were the main mechanisms of plastic deformation in the polycrystalline nickel nanowire.展开更多
In this study, the association between wintertime temperature anomalies over Northwest China and the weather regime transitions in North Atlantic on synoptic scale is analyzed by using observational surface air temper...In this study, the association between wintertime temperature anomalies over Northwest China and the weather regime transitions in North Atlantic on synoptic scale is analyzed by using observational surface air temperature(SAT) data and atmospheric reanalysis data. Daily SAT anomaly and duration time are used in order to define SAT anomaly cases. Differences with regard to the circulation anomalies over the Ural Mountains and the upstream North Atlantic area are evident. It is found that the colder than normal SAT is caused by the enhanced Ural high and associated southward flow over Northwest China. Time-lagged composites reveal possible connections between the SAT anomalies and the different development phases of the North Atlantic Oscillation(NAO). The Ural highs tend to be strengthened during the negative phase of NAO(NAO-) to Atlantic ridge transition, which are closely related to the downstream-propagating Rossby wave activity. The opposite circulation patterns are observed in the warm SAT cases. A cyclonic circulation anomaly is distinctly enhanced over the Urals during the positive phase of NAO(NAO+) to Scandinavian blocking transition, which would cause warmer SAT over Northwest China. Further analyses suggest that the intensified zonal wind over North Atlantic would favor the NAO- to Atlantic ridge transition, while the weakened zonal wind may be responsible for the transition between NAO+ and Scandinavian blocking.展开更多
Dynamic thermo-mechanical coupling behaviors of shape memory TiNi alloy in the strain rate ranging from 300 s^−1 to 2000 s^−1 are investigated by the split Hopkinson pressure bar(SHPB)device with an infrared(IR)detect...Dynamic thermo-mechanical coupling behaviors of shape memory TiNi alloy in the strain rate ranging from 300 s^−1 to 2000 s^−1 are investigated by the split Hopkinson pressure bar(SHPB)device with an infrared(IR)detection system.In stress–strain space,dynamic response shows a strong strain hardening property,however,in stress–temperature space,transformation path is particularly sensitive to the strain rate.The corresponding temperature evolution measured synchronously shows that local temperature increased associated with the forward phase transition,and it would keep the loading maximum value unchanged or decreased for unloading,depending on the strain rate.Besides,local temperature evolution was consistent with the transformation stress and its values at different points are the same.Temperature evolution and transformation deformation mechanism is then analyzed by a simple one-dimensional model.The results show that latent heat and dissipated energy are responsible for temperature variation.Furthermore,the temperature evolution with strain rate reveals that with the increase of strain rate,the phase transformation deformation mechanism undergoes a transformation from phase transition fronts propagation during lower strain rates to combination of local nucleation and front propagation during middle strain rate and to uniform nucleations during higher strain rates.The results are helpful for a passive shape memory alloy(SMA)micro-valve design.展开更多
基金Supported by the National Key Research and Development Program of China under Grant No 2016YFA0300300the National Natural Science Foundation of China under Grant No 11334010+1 种基金the National Basic Research Program of China under Grant No2015CB921300the Strategic Priority Research Program(B)of the Chinese Academy of Sciences under Grant No XDB07020300
文摘We carry out detailed momentum-dependent and temperature-dependent measurements on Bi_2Sr_2CaCu_2O_(8+δ)(Bi2212) superconductor in the superconducting and pseudogap states by super-high resolution laser-based angleresolved photoemission spectroscopy. The precise determination of the superconducting gap for the nearly optimally doped Bi2212(T_c= 91 K) at low temperature indicates that the momentum-dependence of the superconducting gap deviates from the standard d-wave form(cos(2Φ)). It can be alternatively fitted by including a high-order term(cos(6Φ)) in which the next nearest-neighbor interaction is considered. We find that the band structure near the antinodal region smoothly evolves across the pseudogap temperature without a signature of band reorganization which is distinct from that found in Bi_2Sr_2CuO_(6+δ) superconductors. This indicates that the band reorganization across the pseudogap temperature is not a universal behavior in cuprate superconductors.These results provide new insights in understanding the nature of the superconducting gap and pseudogap in high-temperature cuprate superconductors.
基金supported by National Natural Science Foundation of China No.50775182
文摘With the rapid development of infrared imaging technology in last decades, the application range of the nondestructive examination, including fatigue testing,is continuously wider. By reviewing the studies and utilizations of temperature evolution during metal undergoing cyclic loading, this paper provides a reference and also guidance for further research. According to the articles on fatigue temperature evolution, the present overview summarized general rule and characteristics of fatigue temperature evolution. The cause of this temperature evolution is specifically analyzed. Some fatigue life prediction methodologies based on the temperature evolution are systematically reviewed. Finally, a prospect of this research direction is given.
基金Funded by the National Natural Science Foundation of China(No.51472206)the National ITER Program of China(2015GB115001)the Program for Innovative Research Team in Shaanxi Province(No.2013KCT-07)
文摘Powder in tube process(PIT) was adopted for the fabrication of single filament Bi-2223 tapes, and a heat treatment process including the first heat treatment(HT1), intermediate rolling(IR), and second heat treatment(HT2) was performed. The phase evolution mechanism and microstructure changes during these heat treatment processes were systematically discussed. The influences of HT1 parameters on the phase evolution process of Bi-2223 tapes were discussed. With the optimized HT1 process, a proper Bi-2223 content of about 90% was achieved. HT2 process was also optimized by adding a post annealing process. An obvious increase of current capacity was obtained due to the enhancement of intergrain connections. Single filament Bi-2223 tapes with the critical current of Ic-90 A were fabricated with the optimized sintering process.
基金This work was financially supported by the National Natural Science Foundation of China(Nos.51505322 and 51775366)the Natural Science Foundation of Shanxi Province,China(No.201801D221137).
文摘To quickly predict the fatigue limit of 6061 aluminum alloy,two assessment methods based on the temperature evolution and the steady ratcheting strain difference under cyclic loading,respectively,were proposed.The temperature evolutions during static and cyclic loadings were both measured by infrared thermography.Fatigue tests show that the temperature evolution was closely related to the cyclic loading,and the cyclic loading range can be divided into three sections according to the regular of temperature evolution in different section.The mechanism of temperature evolution under different cyclic loadings was also analyzed due to the thermoelastic,viscous,and thermoplastic effects.Additionally,ratcheting strain under cyclic loading was also measured,and the results show that the evolution of the ratcheting strain under cyclic loading above the fatigue limit undergone three stages:the first increasing stage,the second steady state,and the final abrupt increase stage.The fatigue limit of the 6061 aluminum alloy was quickly estimated based on transition point of linear fitting of temperature increase and the steady value of ratcheting strain difference.Besides,it is feasible and quick of the two methods by the proof of the traditional S-N curve.
基金supported by the National Natural Science Foundation of China(Nos.50872053,50830201)Program for New Century Excellent Talents in University(NCET-10-0070)Jiangsu Province Natural Science Foundation(No.BK2008399)
文摘(Na, K)NbO3 (KNN) powders were successfully prepared by high temperature mixing method (HTMM) under hydrothermal conditions to study the effect of reaction time on the formation of KNN for three K+/(K+ +Na+) ratios of 0.6, 0.7 and 0.8. The products were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), transmission electron microscopy (TEM) and selected area electron diffraction (SAED), to show the change of phase and morphology of the as-prepared particles with the K+/(K+ + Na+) molar ratio in the solution. Pure Na-rich KNN monoclinic phase and pure K-rich KNN orthorhombic phase could be obtained quickly after mixing the solutions at high temperature when the K+/(K+ +Na+) molar ratio was either 0.6 or 0.8. When the K+/(K+ +Na+) molar ratio was 0.7, however, the K-rich KNN orthorhombic phase grain formed first, followed by the Na-rich KNN monoclinic phase grain, with the two phases coexisting in the final product.
基金financially supported by the National Natural Science Foundation of China (Nos.51175427 and 51205317)the Open Fund of State Key Laboratory of Materials Processing and Die & Mould Technology of China (No.P2014-005)+1 种基金the Marie Curie International Research Staff Exchange Scheme within the 7th EC Framework Programme (FP7) (No.318968)the Programme of Introducing Talents of Discipline to Universities (No.B08040)
文摘Temperature rise is a significant factor influencing microstructure during(α+β) deformation of TA15 titanium alloy.An experiment was designed to explore microstructure evolution induced by temperature rise due to deformation heat.The experiment was carried out in(α+β) phase field at typical temperature rise rates.The microstructures of the alloy under different temperature rise rates were observed by scanning electron microscopy(SEM).It is found that the dissolution rate of primary equiaxed a phase increases with the increase in both temperature and temperature rise rate.In the same temperature range,the higher the temperature rise rate is,the larger the final content and grain size of primary equiaxed a phase are due to less dissolution time.To quantitatively depict the evolution behavior of primary equiaxed a phase under any temperature rise rates,the dissolution kinetics of primary equiaxed a phase were well described by a diffusion model.The model predictions,including content and grain size of primary equiaxed a phase,are in good agreement with experimental observations.The work provides an important basis for the prediction and control of microstructure during hot working of titanium alloy.
基金Supported by the National Natural Science Foundation of China(11102139,11472195)the Natural Science Foundation of Hubei Province of China(2014CFB713)
文摘Through molecular dynamics(MD) simulation, the dependencies of temperature, grain size and strain rate on the mechanical properties were studied. The simulation results demonstrated that the strain rate from 0.05 to 2 ns–1 affected the Young's modulus of nickel nanowires slightly, whereas the yield stress increased. The Young's modulus decreased approximately linearly; however, the yield stress firstly increased and subsequently dropped as the temperature increased. The Young's modulus and yield stress increased as the mean grain size increased from 2.66 to 6.72 nm. Moreover, certain efforts have been made in the microstructure evolution with mechanical properties association under uniaxial tension. Certain phenomena such as the formation of twin structures, which were found in nanowires with larger grain size at higher strain rate and lower temperature, as well as the movement of grain boundaries and dislocation, were detected and discussed in detail. The results demonstrated that the plastic deformation was mainly accommodated by the motion of grain boundaries for smaller grain size. However, for larger grain size, the formations of stacking faults and twins were the main mechanisms of plastic deformation in the polycrystalline nickel nanowire.
基金Supported by the National Natural Science Foundation of China(41405047)China Meteorological Administration Special Public Welfare Research Fund(GYHY201106015)+1 种基金National(Key)Basic Research and Development(973)Program of China(2012CB957804)National Science and Technology Support Program of China(2014CB954301 and 2014CB954300)
文摘In this study, the association between wintertime temperature anomalies over Northwest China and the weather regime transitions in North Atlantic on synoptic scale is analyzed by using observational surface air temperature(SAT) data and atmospheric reanalysis data. Daily SAT anomaly and duration time are used in order to define SAT anomaly cases. Differences with regard to the circulation anomalies over the Ural Mountains and the upstream North Atlantic area are evident. It is found that the colder than normal SAT is caused by the enhanced Ural high and associated southward flow over Northwest China. Time-lagged composites reveal possible connections between the SAT anomalies and the different development phases of the North Atlantic Oscillation(NAO). The Ural highs tend to be strengthened during the negative phase of NAO(NAO-) to Atlantic ridge transition, which are closely related to the downstream-propagating Rossby wave activity. The opposite circulation patterns are observed in the warm SAT cases. A cyclonic circulation anomaly is distinctly enhanced over the Urals during the positive phase of NAO(NAO+) to Scandinavian blocking transition, which would cause warmer SAT over Northwest China. Further analyses suggest that the intensified zonal wind over North Atlantic would favor the NAO- to Atlantic ridge transition, while the weakened zonal wind may be responsible for the transition between NAO+ and Scandinavian blocking.
基金This work was supported by the National Natural Science Foundation of China(Grant 11702086)Henan Provincial Natural Science Foundation(Grant NSFRF180422).
文摘Dynamic thermo-mechanical coupling behaviors of shape memory TiNi alloy in the strain rate ranging from 300 s^−1 to 2000 s^−1 are investigated by the split Hopkinson pressure bar(SHPB)device with an infrared(IR)detection system.In stress–strain space,dynamic response shows a strong strain hardening property,however,in stress–temperature space,transformation path is particularly sensitive to the strain rate.The corresponding temperature evolution measured synchronously shows that local temperature increased associated with the forward phase transition,and it would keep the loading maximum value unchanged or decreased for unloading,depending on the strain rate.Besides,local temperature evolution was consistent with the transformation stress and its values at different points are the same.Temperature evolution and transformation deformation mechanism is then analyzed by a simple one-dimensional model.The results show that latent heat and dissipated energy are responsible for temperature variation.Furthermore,the temperature evolution with strain rate reveals that with the increase of strain rate,the phase transformation deformation mechanism undergoes a transformation from phase transition fronts propagation during lower strain rates to combination of local nucleation and front propagation during middle strain rate and to uniform nucleations during higher strain rates.The results are helpful for a passive shape memory alloy(SMA)micro-valve design.