Evolution and Application of Sealing Ability of Gypsum Caprocks under Temperature-Pressure Coupling:An Example of the ZS5 Well in the Tazhong Area of the Tarim Basin

Gypsum caprocks'sealing ability is affected by temperature-pressure coupling.Due to the limitations of experimental conditions,there is still a lack of triaxial stress-strain experiments that simultaneously consider changes in temperature and pressure conditions,which limits the accuracy of the comprehensive evaluation of the brittle plastic evolution and sealing ability of gypsum rocks using temperature pressure coupling.Triaxial stress-strain tests were utilized to investigate the differences in the evolution of the confinement capacity of gypsum rocks under coupled temperaturepressure action and isothermal-variable pressure action on the basis of sample feasibility analysis.According to research,the gypsum rock's peak and residual strengths decrease under simultaneous increases in temperature and pressure over isothermal pressurization experimental conditions,and it becomes more ductile.This reduces the amount of time it takes for the rock to transition from brittle to plastic.When temperature is taken into account,both the brittle–plastic transformation's depth limit and the lithological transformation of gypsum rocks become shallower,and the evolution of gypsum rocks under variable temperature and pressure conditions is more complicated than that under isothermal pressurization.The sealing ability under the temperature-pressure coupling is more in line with the actual geological context when the application results of the Well#ZS5 are compared.This provides a theoretical basis for precisely determining the process of hydrocarbon accumulation and explains why the early hydrocarbon were not well preserved.

A Novel Wireless PassiveTemperature-Pressure SAW-based Sensor

A novel wireless and passive surface acoustic wave(SAW)sensor is developed for measuring temperature and pressure.The sensor has two single-port resonators on a substrate.One resonator,acting as the temperature sensor,is located at the fixed end without pressure deformation,and the other one,acting as the pressure sensor,is located at the free end to detect pressure changes due to substrate deformation.Pressure at the free end bends the cantilever,causing a relative change in the acoustic propagation characteristics of the SAW traveling along the surface of the substrate and a relative change in the resonant frequency of the resulting signal.The temperature acts on the entire substrate,affecting the propagation speed of the SAW on the substrate and directly affecting the resonant frequency characteristic parameters.The temperature and pressure performance of this new antenna-connected sensor is tested by using a network analyzer,a constant temperature heating station,and a force gauge.A temperature sensitivity of 1.5015 kHz/℃and a pressure sensitivity of 10.6 kHz/gf at the ambient temperature have been observed by wireless measurements.This work should result in practical engineering applications for high-temperature devices.

Pressure control method and device innovative design for deep oil in-situ exploration and coring

Deep oil exploration coring technology cannot accurately maintain the in-situ pressure and temperature of samples, which leads to a distortion of deep oil and gas resource reserve evaluations based on conventional cores and cannot guide the development of deep oil and gas resources on Earth. The fundamental reason is the lack of temperature and pressure control in in-situ coring environments. In this paper, a pressure control method of a coring device is studied. The theory and method of deep intelligent temperature-pressure coupling control are innovatively proposed, and a multifield coupling dynamic sealing model is established. The optimal cardinality three term PID (Proportional-Integral-Differential) intelligent control algorithm of pressure system is developed. The temperature-pressure characteristic of the gas-liquid two-phase cavity is analyzed, and the pressure intelligent control is carried out based on three term PID control algorithms. An in-situ condition-preserved coring (ICP-Coring) device is developed, and an intelligent control system for the temperature and pressure of the coring device is designed and verified by experiments. The results show that the temperature-pressure coupling control system can effectively realize stable sealing under temperature-pressure fields of 140 MPa and 150 °C. The temperature-pressure coupling control method can accurately realize a constant pressure inside the coring device. The maximum working pressure is 140 MPa, and the effective pressure compensation range is 20 MPa. The numerical simulation experiment of pressure system control algorithm is carried out, and the optimal cardinality and three term coefficients are obtained. The pressure steady-state error is less than 0.01%. The method of temperature-pressure coupling control has guiding significance for coring device research, and is also the basis for temperature-pressure decoupling control in ICP-Coring.

Experimental Study on Anchoring Physical Properties of Different Anchoring Lengths Coupled with Temperature and Pressure

Aiming at deep roadway anchorage solids, laboratory similar model tests were used to reveal the mechanical properties of anchorage solids with different anchorage lengths under the coupling effect of temperature and pressure, and SPSS statistical analysis software was used to conduct linear regression analysis of the ultimate anchorage force obtained from the tests. The results show that: through multiple linear regression analysis, the influence degree of temperature and pressure coupling on the ultimate anchorage force is arranged in order of anchoring length > surrounding rock strength > temperature > side pressure coefficient, and the linear regression equation of the model is obtained. Compared with the linear regression equation of simulation results, the model has a high explanatory ability.

Cubic anvil cell apparatus for high-pressure and low-temperature physical property measurements

We will build a cubic anvil cell （CAC） apparatus for high-pressure and low-temperature physical property measurements in the synergic extreme condition user facility （SECUF）. In this article, we first introduce the operating principle, the development history, and the current status of the CAC apparatus, and subsequently describe the design plan and technical targets for the CAC in SECUF. We will demonstrate the unique advantages of CAC, i.e., excellent pressure homogeneity and large hydrostatic pressure capacity, by summarizing our recent research progresses using CAC. Finally, we conclude by providing some perspectives on the applications of CAC in the related research fields.

Transformation from Neoproterozoic Sinistral to Early Paleozoic Dextral Shearing for the Jingdezhen Ductile Shear Zone in the Jiangnan Orogen, South China

The Jingdezhen ductile shear zone is evolved from the Neoproterozoic Zhangyuan ophiolite melange belt in the eastern Jiangnan Orogen, South China. Comprehensive study of geometry, kinematics, quartz c-axis fabric, temperature-pressure conditions and geochronology were conducted in this study. The Jingdezhen shear zone extends -180 km along the NE orientation with two groups of subvertical fo- liation and subhorizontal lineation. One group of foliation strikes NEN orientation whereas another one NEE orientation. Field investigation, microscopic observation and quartz c-axis fabric show that sinistral shearing along NEN-striking foliation occurred earlier than dextral shearing along NEE-striking foliation. Syn-tectonic staurolite porphyroblasts and deformation manner of feldspar imply that sinistral shearing occurred at 530-420 ℃ and 6-2 kbar. Deformation manner and c-axis fabric of quartz and pre-tectonic staurolite porphyroblasts indicate that dextral shearing took place at 420-300 ℃. LA-ICP-MS zircon U-Pb and mica ^40Ar/^39Ar dating indicate that the sinistral shearing occurred during Neoproterozoic oro- geny （830-800 Ma） whereas the dextral shearing at 447＋12 Ma. The sinistral shearing resulted from the Neoproterozoic final assembly between the Yangtze and Cathaysia blocks. The dextral shearing was caused by Early Paleozoic orogen parallel extension and clockwise rotation.

Key process study in nanoimprint lithography

Nanoimprint lithography（NIL） is widely used in the fabrication of nano-scale semiconductor devices for its advantages of high resolution,low cost,and high throughput.However,traditional hard stamp imprinting has some drawbacks such as short stamp lifetime,bad uniformity in big areas,and large particle influence.In this paper, a flexible intermediate polymer stamp（IPS） is proposed to solve the drawbacks mentioned above.Meanwhile, we use a method of temperature-pressure variation imprinting to improve the resist liquidity in the process of imprinting,and eventually we achieve high quality patterns.This method combined with IPS has been used to fabricate a high quality grating whose half pitch is 50 nm.