The textured shape memory alloys exhibits anisotropic because the property of single crystal is strongly orientation dependent. The effect of texture on phase transformation strain in CuZnAl shape memory sheets was in...The textured shape memory alloys exhibits anisotropic because the property of single crystal is strongly orientation dependent. The effect of texture on phase transformation strain in CuZnAl shape memory sheets was investigated. The texture of parent austenite was measured by X ray goniometer and analyzed by the orientation distribution function. Subsequently, using the texture parameters and single crystal properties, the phase transformation strains at the different directions of rolling plane by the statistically averaging method were calculated. It was showed that the experimental results are agreeable with the calculated ones. It is well explained that this anisotropy of phase transformation strain is mainly caused by the crystallographic texture of the rolled sheets.展开更多
This thesis presents a new approach to classify 3D surface textures by using lifting transform with quincunx subsampling. Feature vectors are generated from eight different lifting prediction directions. We classify 3...This thesis presents a new approach to classify 3D surface textures by using lifting transform with quincunx subsampling. Feature vectors are generated from eight different lifting prediction directions. We classify 3D surface texture images based on minimum Euclidean distance between the test images and the training sets. The feasibility and effectiveness of our proposed approach can be validated by the experimental results.展开更多
A novel and efficient approach for detecting wood texture orientation by computer was presented. Four Matlab functions were tried to describe the relative position and orientation of wood texture pixels, to detect tex...A novel and efficient approach for detecting wood texture orientation by computer was presented. Four Matlab functions were tried to describe the relative position and orientation of wood texture pixels, to detect texture shape and to create skeletal lines image of wood texture, and BWMORPH function was found the best one. Then by Radon transform, it generated a signature composed of 180 values, each value summing up the size of texture lines that are shaped along that angle, and a two dimensional curve plot was drawn to represent the texture orientation of wood. Furthermore, it analyzed texture orientations of forty species as well as their general statistic laws, classified by softwood, hardwood, radial section and tangential section, and the results showed that texture orientation laws described by Radon trans- form plot and their extracting datum were in accord with the impression of wood texture that people possessed in daily life, which con- firmed the validity of this new approach and their appealing utilization potentials.展开更多
Empirical mode decomposition (EMD) is an adaptive and approximately orthogonal filtering process that reflects human’s visual mechanism of differentiating textures. In this paper, we present a modified 2D EMD algorit...Empirical mode decomposition (EMD) is an adaptive and approximately orthogonal filtering process that reflects human’s visual mechanism of differentiating textures. In this paper, we present a modified 2D EMD algorithm using the FastRBF and an appropriate number of iterations in the shifting process (SP), then apply it to texture classification. Rotation-invariant texture feature vectors are extracted using auto-registration and circular regions of magnitude spectra of 2D fast Fourier transform (FFT). In the experiments, we employ a Bayesion classifier to classify a set of 15 distinct natural textures selected from the Brodatz album. The experimental results, based on different testing datasets for images with different orientations, show the effectiveness of the proposed classification scheme.展开更多
Ground textures seriously interfere with the exact identification of grinding damage. The common nondestructive testing techniques for engineering ceramics are limited by their difficulty and cost. Therefore, this pap...Ground textures seriously interfere with the exact identification of grinding damage. The common nondestructive testing techniques for engineering ceramics are limited by their difficulty and cost. Therefore, this paper proposes a global image reconstruction scheme in ground texture surface using Fourier transform (FT). The lines associated with high-energy frequency components in the spectrum that represent ground texture information can be detected by Hough transform (HT), and the corresponding high-energy frequency components are set to zero. Then the spectrum image is back-transformed into the spatial domain image with inverse Fourier transform (IFT). In the reconstructed image, the main ground texture information has been removed, whereas the surface defects information is preserved. Finally, Canny edge detection is used to extract damage image in the reconstructed image. The experimental results of damage detection for the ground texture surfaces of engineering ceramics have shown that the proposed method is effective.展开更多
A new approach based on multiwavelets transformation and singular value decomposition (SVD) is proposed for the classification of image textures. Lower singular values are truncated based on its energy distribution to...A new approach based on multiwavelets transformation and singular value decomposition (SVD) is proposed for the classification of image textures. Lower singular values are truncated based on its energy distribution to classify the textures in the presence of additive white Gaussian noise (AWGN). The proposed approach extracts features such as energy, entropy, local homogeneity and max-min ratio from the selected singular values of multiwavelets transformation coefficients of image textures. The classification was carried out using probabilistic neural network (PNN). Performance of the proposed approach was compared with conventional wavelet domain gray level co-occurrence matrix (GLCM) based features, discrete multiwavelets transformation energy based approach, and HMM based approach. Experimental results showed the superiority of the proposed algorithms when compared with existing algorithms.展开更多
Mean shift is a widely used clustering algorithm in image segmentation. However, the segmenting results are not so good as expected when dealing with the texture surface due to the influence of the textures. Therefore...Mean shift is a widely used clustering algorithm in image segmentation. However, the segmenting results are not so good as expected when dealing with the texture surface due to the influence of the textures. Therefore, an approach based on wavelet transform (WT), co-occurrence matrix (COM) and mean shift is proposed in this paper. First, WT and COM are employed to extract the optimal resolution approximation of the original image as feature image. Then, mean shift is successfully used to obtain better detection results. Finally, experiments are done to show this approach is effective.展开更多
Texture analysis is a fundamental field in computer vision. However,it is also a particularly difficult problem for no universal mathematical model of real world textures. By extending a new application of the fractio...Texture analysis is a fundamental field in computer vision. However,it is also a particularly difficult problem for no universal mathematical model of real world textures. By extending a new application of the fractional Fourier transform( Fr FT) in the field of texture analysis,this paper proposes an Fr FT-based method for describing textures. Firstly,based on the Radon-Wigner transform,1-D directional Fr FT filters are designed to two types of texture features,i. e.,the coarseness and directionality. Then,the frequencies with maximum and median amplitudes of the Fr FT of the input signal are regarded as the output of the 1-D directional Fr FT filter. Finally,the mean and the standard deviation are used to compose of the feature vector. Compared to the WD-based method,three benefits can be achieved with the proposed Fr FT-based method,i. e.,less memory size,lower computational load,and less disturbed by the cross-terms. The proposed method has been tested on16 standard texture images. The experimental results show that the proposed method is superior to the popular Gabor filtering-based method.展开更多
In order to overcome the shortcoming of poor accuracy and non-serious intuitivism of traditional wavelength calculation method in serious noise, a revised Radon transform algorithm is proposed by using a straight-line...In order to overcome the shortcoming of poor accuracy and non-serious intuitivism of traditional wavelength calculation method in serious noise, a revised Radon transform algorithm is proposed by using a straight-line instead of using the wave's texture approximately applied to wavelength estimation. Firstly, Radon transform of the radar image is analyzed. Then, to obtain its fitting straight line combined with wave texture, the distance is calculated between straight lines to get the wavelength. Finally, the algorithm is programmed with Matlab on PC. The experimental results show that the proposed algorithm can improve the estimation accuracy of the wavelength with good visibility.展开更多
In this paper, we proposed a metric to measure the shift invariance of the three different contourlet transforms. And then, using the same structure texture image retrieval system which use subband coefficients energy...In this paper, we proposed a metric to measure the shift invariance of the three different contourlet transforms. And then, using the same structure texture image retrieval system which use subband coefficients energy, standard deviation and kurtosis features with Canberra distance, we gave a comparison of their texture description abilities. Experimental results show that contourlet-2.3 texture image retrieval system has almost retrieval rates with non-sub sampled contourlet system;the two systems have better retrieval results than the original contourlet retrieval system. On the other hand, for the relatively lower redundancy, we recommend using contourlet- 2.3 as texture description transform.展开更多
The hot deformation behavior of Ni48Mn31Ga21 alloy was studied by thermal simulation rolling technology. Microstructure evolution of the alloys under different rolling processes was studied by optical microscopy(OM) a...The hot deformation behavior of Ni48Mn31Ga21 alloy was studied by thermal simulation rolling technology. Microstructure evolution of the alloys under different rolling processes was studied by optical microscopy(OM) and X-ray diffractometry(XRD).The results show that, by thermal simulation pack rolling technology, textures appear in polycrystalline Ni48Mn31Ga21 alloy, and big cracks can be avoided under large deformation ratio. The rolling process with few passes and strong deformation makes Ni48Mn31Ga21 alloy obtain (202), (400) and (323) textures of martensitic variants more easily, especially (400) texture. Besides the interface between package materials and the Ni48Mn31Ga21 alloy is clear, which is beneficial for Ni48Mn31Ga21 alloy to separate from pack.展开更多
The effect of cooling rate on the microstructure and transformation textures of high strength hot-rolled steels was investigated.Heat treated samples subjected to different cooling conditions were characterized by opt...The effect of cooling rate on the microstructure and transformation textures of high strength hot-rolled steels was investigated.Heat treated samples subjected to different cooling conditions were characterized by optical and scanning electron microscopes using orientation imaging microscopy(OIM).The experimental results demonstrate that there is a significant effect of cooling rate on microstructures and textures resulting from phase transformation.Slow cooling rates lead to the appearance of the cube(001)[010],rotated cube(001)[110]/(001)[110],Goss(110)[001]and rotated Goss(110)[110]components.In contrast,textures developed at rapid cooling rates are preferably of Cu(112)[111],Br(110)[112],transformed Cu(113)[110]and transformed Br(332)[113]/(112)[131].These texture changes are attributed to the selective character of the phase transformation.The OIM technique was used to have a better understanding of the formation of phases and their relationship between microstructure and processing conditions.The volume fraction of micro-constituents resulting from phase transformation such as bainite,martensite and different types of ferrite,can be measured satisfactorily by this technique correlating image quality of EBSD patterns to specific phases.展开更多
The control of the post-forging cooling rate has been a key issue in the industrial production process of titanium alloys. We investigated texture evolution and variant selection(VS) during β → α transformation thr...The control of the post-forging cooling rate has been a key issue in the industrial production process of titanium alloys. We investigated texture evolution and variant selection(VS) during β → α transformation through high-temperature compression experiments followed by quantitative control of varying cooling rates. Results show that post-forging cooling rates affect β grains, α variants, and α/β textures. The αprecipitation inhibits motions of β static recrystallization(β_(SRX)) grain boundaries and thus leads to grain refining from 0.1 ℃/s to 0.05 ℃/s. Further analysis reveals that lamellae grain boundary widmanstattenα(α_(WGB)) keeps growing rapidly within β-grain in an interface instability manner at 0.1–0.05 ℃/s. Most of α-phase with 50°–60°/<-12–10> is preferentially precipitated at β-medium angle GBs between 30°and 45° and strictly follows BOR with the side of of adjacent β-grain with the same or similar {110} or{111}. Moreover, the texture type transforms gradually from RGoss {110} <1–10> to Brass {110} <1–12>from 25 ℃/s to 1 ℃/s. βgrains exhibit(102) [-201] texture, while the corresponding α has textures of<0001>//Z and <11–20>//Y from 1 ℃/s to 0.05 ℃/s. Our findings lay a profound theoretical foundation in microstructure evolution of near-β titanium alloy for industrial production.展开更多
The undesired {111} texture component for the magnetic properties mainly exists in the sheets of electrical steels by the conventional process, whereas the sheets with the non-{111} texture can be obtained by α→γ→...The undesired {111} texture component for the magnetic properties mainly exists in the sheets of electrical steels by the conventional process, whereas the sheets with the non-{111} texture can be obtained by α→γ→α transformation. In this paper, we mainly investigate the opposite relationship between orientation selection and texture memory in the deformed ultra-low carbon steel sheet during →→ transformation annealing. A 0.5 mm thick hot-rolled sheet is directly subjected to transformation. The result shows that the specific transformation textures are not possible to generate in the sheets without deformation. Besides, transformation annealing is conducted on the recrystallized sheets in hydrogen and vacuum, respectively. The near {100} and {110} grains have the growth advantage at the atmosphere/metal interface, and the initial ferrite textures are retained in vacuum. Cold-rolled sheets with different thicknesses are annealed for transformation in vacuum, hydrogen and nitrogen, respectively.The near {100} and {110} textures are still the preferential orientations at the atmosphere/metal interface. When the surface grains have sufficiently large growth advantage, the {111} grains developed by texture memory effect will be annexed. Otherwise, the {111} grains at the center layer of the sheets are hard to be replaced, and they are retained after α→γ→α transformation cycle. The results of deformed sheets annealed with different heating rates in hydrogen show that the growth of initial recrystallization grains has a great effect on variant selection.展开更多
Taking Fe-C binary alloy as an example,based on the multi-phase field model,the nucleation and growth ofδphase,peritectic reaction,peritectic transformation,and the growth of subsequent austenite are simulated.Effect...Taking Fe-C binary alloy as an example,based on the multi-phase field model,the nucleation and growth ofδphase,peritectic reaction,peritectic transformation,and the growth of subsequent austenite are simulated.Effects of the nucleation site of austenite on the peritectic reaction rate and the starting time of the peritectic transformation were studied.The simulation results show that theγphase,as a shell,surrounds theδphase and grows rapidly when the peritectic reaction occurs between the dendriticδgrains,and a layer ofγphase shell is formed aroundδphase after the peritectic reaction.After theδphase is surrounded byγphase completely,the membrane shell separates the L phase from theδphase,so that the phase transfers from peritectic reaction to peritectic transformation.During the peritectic transformation,since the solute diffusion coefficient of the liquid phase is much greater than that of the solid phase,the average growth rate of austenite in the liquid phase is visibly higher than that of theδphase.The peritectic reaction rate is related to the curvature of the nucleation site of theγphase on theδphase grains.The peritectic reaction rate at the large curvatures is faster than that at small curvatures.展开更多
The hexagonal to orthorhombic(HO)transformation fromβ-Ni_(3)Sn_(2)(hexagonal)phase toα'-Ni_(3)Sn_(2)(orthorhombic)phase was confirmed in directionally solidified Sn−Ni peritectic alloys.It is shown that the reme...The hexagonal to orthorhombic(HO)transformation fromβ-Ni_(3)Sn_(2)(hexagonal)phase toα'-Ni_(3)Sn_(2)(orthorhombic)phase was confirmed in directionally solidified Sn−Ni peritectic alloys.It is shown that the remelting/resolidification process which is caused by both the temperature gradient zone melting(TGZM)and Gibbs−Thomson(G−T)effects can take place on secondary dendrites.Besides,the intersection angle between the primary dendrite stem and secondary branch(θ)is found to increase fromπ/3 toπ/2 as the solidification proceeds.This is the morphological feature of the HO transformation,which can change the diffusion distance of the remelting/resolidification process.Thus,a diffusion-based analytical model is established to describe this process through the specific surface area(S_(V))of dendrites.The theoretical prediction demonstrates that the remelting/resolidification process is restricted when the HO transformation occurs during peritectic solidification.In addition,the slope of the prediction curves is changed,indicating the variation of the local remelting/resolidification rates.展开更多
TA2 pure titanium was chosen to research the interaction among deformation, recrystallization and phase transformation during hot compression. The samples were hot compressed by thermal simulation method with differen...TA2 pure titanium was chosen to research the interaction among deformation, recrystallization and phase transformation during hot compression. The samples were hot compressed by thermal simulation method with different processing parameters. Variant selection induced by stress during cooling after compression was found. The prismatical texture component which featured that the [0001] direction perpendicular to the compressing direction produced preferentially under the compressing stress. As a result, the transformedα phase possesses strong prismatical texture which is different with the basal texture of compressed αphase. The minimum elastic strain energy is demonstrated to be the main reason that causes the variant selection. Dynamic recrystallization behavior and microstructure evolution during hot compression were also studied.展开更多
Microstructure evolution during deformation of undercooled austenite at 760℃ was investigated in Nb-microalloyed steel by using SEM (scanning electron microscope), TEM (transmission electron microscope), and EBSD...Microstructure evolution during deformation of undercooled austenite at 760℃ was investigated in Nb-microalloyed steel by using SEM (scanning electron microscope), TEM (transmission electron microscope), and EBSD (electron backscattered diffraction). It is indicated that during deformation-enhanced ferrite transformation (DEFT) in Nb-microalloyed steel, the incubation period is prolonged, and the higher strain is needed to accomplish ferrite transformation. Therefore, the transformation kinetics curves move to high strain parallelly; and the transformation kinetics curves of Nb-microalloyed steel can be divided into three stages. At the fast stage, the solute drag effect of Nb and the consumption of strain energy for the dynamic precipitation of Nb(CN) led to a long incubation period, and at the second stage, ferrite transformation was accelerated significantly and fine Nb(CN) precipitates restrict the grain growth of ferrite effectively. The results also showed that DEFT in Nb-microalloyed steel is still a nucleation dominated process, and during the microstructure evolution the interchange of 〈001〉 and 〈111〉 texture was obtained.展开更多
Fe66Mn15Si5Cr9Ni5(wt.%)shape memory alloy(SMA)withγaustenite andεmartensite was subjected to mechanical vibrating polishing and consequently its surface suffered from plastic deformation in the case of compressive s...Fe66Mn15Si5Cr9Ni5(wt.%)shape memory alloy(SMA)withγaustenite andεmartensite was subjected to mechanical vibrating polishing and consequently its surface suffered from plastic deformation in the case of compressive stress.Almost completeεmartensite transformation is found to occur in FeMnSiCrNi sample subjected to mechanical vibrating polishing,where stress-induced martensite transformation plays a predominant role.Stressinduced martensite transformation of FeMnSiCrNi SMA is closely related to the orientation of external stress.The complicated compressive stress which results from the mechanical vibrating polishing contributes toεmartensite transformation fromγaustenite of FeMnSiCrNi SMA.Mechanical vibrating polishing has a certain influence on the surface texture ofεmartensite of FeMnSiCrNi SMA,where■<0001>texture appears in the polished FeMnSiCrNi SMA.展开更多
文摘The textured shape memory alloys exhibits anisotropic because the property of single crystal is strongly orientation dependent. The effect of texture on phase transformation strain in CuZnAl shape memory sheets was investigated. The texture of parent austenite was measured by X ray goniometer and analyzed by the orientation distribution function. Subsequently, using the texture parameters and single crystal properties, the phase transformation strains at the different directions of rolling plane by the statistically averaging method were calculated. It was showed that the experimental results are agreeable with the calculated ones. It is well explained that this anisotropy of phase transformation strain is mainly caused by the crystallographic texture of the rolled sheets.
文摘This thesis presents a new approach to classify 3D surface textures by using lifting transform with quincunx subsampling. Feature vectors are generated from eight different lifting prediction directions. We classify 3D surface texture images based on minimum Euclidean distance between the test images and the training sets. The feasibility and effectiveness of our proposed approach can be validated by the experimental results.
文摘A novel and efficient approach for detecting wood texture orientation by computer was presented. Four Matlab functions were tried to describe the relative position and orientation of wood texture pixels, to detect texture shape and to create skeletal lines image of wood texture, and BWMORPH function was found the best one. Then by Radon transform, it generated a signature composed of 180 values, each value summing up the size of texture lines that are shaped along that angle, and a two dimensional curve plot was drawn to represent the texture orientation of wood. Furthermore, it analyzed texture orientations of forty species as well as their general statistic laws, classified by softwood, hardwood, radial section and tangential section, and the results showed that texture orientation laws described by Radon trans- form plot and their extracting datum were in accord with the impression of wood texture that people possessed in daily life, which con- firmed the validity of this new approach and their appealing utilization potentials.
基金Project supported by the National Basic Research Program (973) of China (Nos. 2004CB318000 and 2002CB312104), the National Natural Science Foundation of China (Nos. 60133020 and 60325208) and the Natural Science Foundation of Beijing (No. 1062006), China
文摘Empirical mode decomposition (EMD) is an adaptive and approximately orthogonal filtering process that reflects human’s visual mechanism of differentiating textures. In this paper, we present a modified 2D EMD algorithm using the FastRBF and an appropriate number of iterations in the shifting process (SP), then apply it to texture classification. Rotation-invariant texture feature vectors are extracted using auto-registration and circular regions of magnitude spectra of 2D fast Fourier transform (FFT). In the experiments, we employ a Bayesion classifier to classify a set of 15 distinct natural textures selected from the Brodatz album. The experimental results, based on different testing datasets for images with different orientations, show the effectiveness of the proposed classification scheme.
基金Supported by National Natural Science Foundation of China (No. 51075296)
文摘Ground textures seriously interfere with the exact identification of grinding damage. The common nondestructive testing techniques for engineering ceramics are limited by their difficulty and cost. Therefore, this paper proposes a global image reconstruction scheme in ground texture surface using Fourier transform (FT). The lines associated with high-energy frequency components in the spectrum that represent ground texture information can be detected by Hough transform (HT), and the corresponding high-energy frequency components are set to zero. Then the spectrum image is back-transformed into the spatial domain image with inverse Fourier transform (IFT). In the reconstructed image, the main ground texture information has been removed, whereas the surface defects information is preserved. Finally, Canny edge detection is used to extract damage image in the reconstructed image. The experimental results of damage detection for the ground texture surfaces of engineering ceramics have shown that the proposed method is effective.
文摘A new approach based on multiwavelets transformation and singular value decomposition (SVD) is proposed for the classification of image textures. Lower singular values are truncated based on its energy distribution to classify the textures in the presence of additive white Gaussian noise (AWGN). The proposed approach extracts features such as energy, entropy, local homogeneity and max-min ratio from the selected singular values of multiwavelets transformation coefficients of image textures. The classification was carried out using probabilistic neural network (PNN). Performance of the proposed approach was compared with conventional wavelet domain gray level co-occurrence matrix (GLCM) based features, discrete multiwavelets transformation energy based approach, and HMM based approach. Experimental results showed the superiority of the proposed algorithms when compared with existing algorithms.
基金Project (No. 035115039) supported by the Scientific Committee of Shanghai, China
文摘Mean shift is a widely used clustering algorithm in image segmentation. However, the segmenting results are not so good as expected when dealing with the texture surface due to the influence of the textures. Therefore, an approach based on wavelet transform (WT), co-occurrence matrix (COM) and mean shift is proposed in this paper. First, WT and COM are employed to extract the optimal resolution approximation of the original image as feature image. Then, mean shift is successfully used to obtain better detection results. Finally, experiments are done to show this approach is effective.
基金Sponsored by the National Natural Science Foundation of China(Grant No.61003128)
文摘Texture analysis is a fundamental field in computer vision. However,it is also a particularly difficult problem for no universal mathematical model of real world textures. By extending a new application of the fractional Fourier transform( Fr FT) in the field of texture analysis,this paper proposes an Fr FT-based method for describing textures. Firstly,based on the Radon-Wigner transform,1-D directional Fr FT filters are designed to two types of texture features,i. e.,the coarseness and directionality. Then,the frequencies with maximum and median amplitudes of the Fr FT of the input signal are regarded as the output of the 1-D directional Fr FT filter. Finally,the mean and the standard deviation are used to compose of the feature vector. Compared to the WD-based method,three benefits can be achieved with the proposed Fr FT-based method,i. e.,less memory size,lower computational load,and less disturbed by the cross-terms. The proposed method has been tested on16 standard texture images. The experimental results show that the proposed method is superior to the popular Gabor filtering-based method.
文摘In order to overcome the shortcoming of poor accuracy and non-serious intuitivism of traditional wavelength calculation method in serious noise, a revised Radon transform algorithm is proposed by using a straight-line instead of using the wave's texture approximately applied to wavelength estimation. Firstly, Radon transform of the radar image is analyzed. Then, to obtain its fitting straight line combined with wave texture, the distance is calculated between straight lines to get the wavelength. Finally, the algorithm is programmed with Matlab on PC. The experimental results show that the proposed algorithm can improve the estimation accuracy of the wavelength with good visibility.
文摘In this paper, we proposed a metric to measure the shift invariance of the three different contourlet transforms. And then, using the same structure texture image retrieval system which use subband coefficients energy, standard deviation and kurtosis features with Canberra distance, we gave a comparison of their texture description abilities. Experimental results show that contourlet-2.3 texture image retrieval system has almost retrieval rates with non-sub sampled contourlet system;the two systems have better retrieval results than the original contourlet retrieval system. On the other hand, for the relatively lower redundancy, we recommend using contourlet- 2.3 as texture description transform.
基金Project(50501008) supported by the National Natural Science Foundation of China
文摘The hot deformation behavior of Ni48Mn31Ga21 alloy was studied by thermal simulation rolling technology. Microstructure evolution of the alloys under different rolling processes was studied by optical microscopy(OM) and X-ray diffractometry(XRD).The results show that, by thermal simulation pack rolling technology, textures appear in polycrystalline Ni48Mn31Ga21 alloy, and big cracks can be avoided under large deformation ratio. The rolling process with few passes and strong deformation makes Ni48Mn31Ga21 alloy obtain (202), (400) and (323) textures of martensitic variants more easily, especially (400) texture. Besides the interface between package materials and the Ni48Mn31Ga21 alloy is clear, which is beneficial for Ni48Mn31Ga21 alloy to separate from pack.
文摘The effect of cooling rate on the microstructure and transformation textures of high strength hot-rolled steels was investigated.Heat treated samples subjected to different cooling conditions were characterized by optical and scanning electron microscopes using orientation imaging microscopy(OIM).The experimental results demonstrate that there is a significant effect of cooling rate on microstructures and textures resulting from phase transformation.Slow cooling rates lead to the appearance of the cube(001)[010],rotated cube(001)[110]/(001)[110],Goss(110)[001]and rotated Goss(110)[110]components.In contrast,textures developed at rapid cooling rates are preferably of Cu(112)[111],Br(110)[112],transformed Cu(113)[110]and transformed Br(332)[113]/(112)[131].These texture changes are attributed to the selective character of the phase transformation.The OIM technique was used to have a better understanding of the formation of phases and their relationship between microstructure and processing conditions.The volume fraction of micro-constituents resulting from phase transformation such as bainite,martensite and different types of ferrite,can be measured satisfactorily by this technique correlating image quality of EBSD patterns to specific phases.
文摘The control of the post-forging cooling rate has been a key issue in the industrial production process of titanium alloys. We investigated texture evolution and variant selection(VS) during β → α transformation through high-temperature compression experiments followed by quantitative control of varying cooling rates. Results show that post-forging cooling rates affect β grains, α variants, and α/β textures. The αprecipitation inhibits motions of β static recrystallization(β_(SRX)) grain boundaries and thus leads to grain refining from 0.1 ℃/s to 0.05 ℃/s. Further analysis reveals that lamellae grain boundary widmanstattenα(α_(WGB)) keeps growing rapidly within β-grain in an interface instability manner at 0.1–0.05 ℃/s. Most of α-phase with 50°–60°/<-12–10> is preferentially precipitated at β-medium angle GBs between 30°and 45° and strictly follows BOR with the side of of adjacent β-grain with the same or similar {110} or{111}. Moreover, the texture type transforms gradually from RGoss {110} <1–10> to Brass {110} <1–12>from 25 ℃/s to 1 ℃/s. βgrains exhibit(102) [-201] texture, while the corresponding α has textures of<0001>//Z and <11–20>//Y from 1 ℃/s to 0.05 ℃/s. Our findings lay a profound theoretical foundation in microstructure evolution of near-β titanium alloy for industrial production.
基金supported by the National Natural Science Foundation of China(Grant No.51271028)
文摘The undesired {111} texture component for the magnetic properties mainly exists in the sheets of electrical steels by the conventional process, whereas the sheets with the non-{111} texture can be obtained by α→γ→α transformation. In this paper, we mainly investigate the opposite relationship between orientation selection and texture memory in the deformed ultra-low carbon steel sheet during →→ transformation annealing. A 0.5 mm thick hot-rolled sheet is directly subjected to transformation. The result shows that the specific transformation textures are not possible to generate in the sheets without deformation. Besides, transformation annealing is conducted on the recrystallized sheets in hydrogen and vacuum, respectively. The near {100} and {110} grains have the growth advantage at the atmosphere/metal interface, and the initial ferrite textures are retained in vacuum. Cold-rolled sheets with different thicknesses are annealed for transformation in vacuum, hydrogen and nitrogen, respectively.The near {100} and {110} textures are still the preferential orientations at the atmosphere/metal interface. When the surface grains have sufficiently large growth advantage, the {111} grains developed by texture memory effect will be annexed. Otherwise, the {111} grains at the center layer of the sheets are hard to be replaced, and they are retained after α→γ→α transformation cycle. The results of deformed sheets annealed with different heating rates in hydrogen show that the growth of initial recrystallization grains has a great effect on variant selection.
基金the National Natural Science Foundation of China(Grant Nos.:11504149,51661020)Natural Science Foundation of Gansu Province of China(Grant No.:18JR3RA147).
文摘Taking Fe-C binary alloy as an example,based on the multi-phase field model,the nucleation and growth ofδphase,peritectic reaction,peritectic transformation,and the growth of subsequent austenite are simulated.Effects of the nucleation site of austenite on the peritectic reaction rate and the starting time of the peritectic transformation were studied.The simulation results show that theγphase,as a shell,surrounds theδphase and grows rapidly when the peritectic reaction occurs between the dendriticδgrains,and a layer ofγphase shell is formed aroundδphase after the peritectic reaction.After theδphase is surrounded byγphase completely,the membrane shell separates the L phase from theδphase,so that the phase transfers from peritectic reaction to peritectic transformation.During the peritectic transformation,since the solute diffusion coefficient of the liquid phase is much greater than that of the solid phase,the average growth rate of austenite in the liquid phase is visibly higher than that of theδphase.The peritectic reaction rate is related to the curvature of the nucleation site of theγphase on theδphase grains.The peritectic reaction rate at the large curvatures is faster than that at small curvatures.
基金the support from the Natural Science Foundation of China(No.51871118)Open Project of Key Laboratory for Magnetism and Magnetic Materials of the Ministry of Education,Lanzhou University,China(No.LZUMMM2021005)+1 种基金the Science and Technology Project of Lanzhou City,China(No.2019-1-30)State Key Laboratory of Special Rare Metal Materials,China(No.SKL2020K003)。
文摘The hexagonal to orthorhombic(HO)transformation fromβ-Ni_(3)Sn_(2)(hexagonal)phase toα'-Ni_(3)Sn_(2)(orthorhombic)phase was confirmed in directionally solidified Sn−Ni peritectic alloys.It is shown that the remelting/resolidification process which is caused by both the temperature gradient zone melting(TGZM)and Gibbs−Thomson(G−T)effects can take place on secondary dendrites.Besides,the intersection angle between the primary dendrite stem and secondary branch(θ)is found to increase fromπ/3 toπ/2 as the solidification proceeds.This is the morphological feature of the HO transformation,which can change the diffusion distance of the remelting/resolidification process.Thus,a diffusion-based analytical model is established to describe this process through the specific surface area(S_(V))of dendrites.The theoretical prediction demonstrates that the remelting/resolidification process is restricted when the HO transformation occurs during peritectic solidification.In addition,the slope of the prediction curves is changed,indicating the variation of the local remelting/resolidification rates.
文摘TA2 pure titanium was chosen to research the interaction among deformation, recrystallization and phase transformation during hot compression. The samples were hot compressed by thermal simulation method with different processing parameters. Variant selection induced by stress during cooling after compression was found. The prismatical texture component which featured that the [0001] direction perpendicular to the compressing direction produced preferentially under the compressing stress. As a result, the transformedα phase possesses strong prismatical texture which is different with the basal texture of compressed αphase. The minimum elastic strain energy is demonstrated to be the main reason that causes the variant selection. Dynamic recrystallization behavior and microstructure evolution during hot compression were also studied.
基金This work was financially supported by the National High-Tech Research and Development Program of China ("863" Program)(No.2001AA332020).
文摘Microstructure evolution during deformation of undercooled austenite at 760℃ was investigated in Nb-microalloyed steel by using SEM (scanning electron microscope), TEM (transmission electron microscope), and EBSD (electron backscattered diffraction). It is indicated that during deformation-enhanced ferrite transformation (DEFT) in Nb-microalloyed steel, the incubation period is prolonged, and the higher strain is needed to accomplish ferrite transformation. Therefore, the transformation kinetics curves move to high strain parallelly; and the transformation kinetics curves of Nb-microalloyed steel can be divided into three stages. At the fast stage, the solute drag effect of Nb and the consumption of strain energy for the dynamic precipitation of Nb(CN) led to a long incubation period, and at the second stage, ferrite transformation was accelerated significantly and fine Nb(CN) precipitates restrict the grain growth of ferrite effectively. The results also showed that DEFT in Nb-microalloyed steel is still a nucleation dominated process, and during the microstructure evolution the interchange of 〈001〉 and 〈111〉 texture was obtained.
基金Projects (51475101, 51871070) supported by the National Natural Science Foundation of China。
文摘Fe66Mn15Si5Cr9Ni5(wt.%)shape memory alloy(SMA)withγaustenite andεmartensite was subjected to mechanical vibrating polishing and consequently its surface suffered from plastic deformation in the case of compressive stress.Almost completeεmartensite transformation is found to occur in FeMnSiCrNi sample subjected to mechanical vibrating polishing,where stress-induced martensite transformation plays a predominant role.Stressinduced martensite transformation of FeMnSiCrNi SMA is closely related to the orientation of external stress.The complicated compressive stress which results from the mechanical vibrating polishing contributes toεmartensite transformation fromγaustenite of FeMnSiCrNi SMA.Mechanical vibrating polishing has a certain influence on the surface texture ofεmartensite of FeMnSiCrNi SMA,where■<0001>texture appears in the polished FeMnSiCrNi SMA.