Synthesis and luminescent properties of Ce^(3+) doped LuAG nano-sized powders by mixed solvo-thermal method

Polycrystalline LuAG:Ce3+(cerium3+-doped lutetium aluminum garnet) powders were prepared by mixed solvo-thermal method.Fourier-transform IR spectroscopy(FTIR) and X-ray diffraction(XRD) measurements showed that the precursors were ethanol derivatives AlO(OH) crystal with hydroxyl and carbonate group.XRD results showed that phase of Lu2O3 disappeared with the precursors were annealed at 400 °C,cubic phase LuAG:Ce3+ appeared but only one diffraction peaks of LuAP(LuAlO3) at calcination temperature to 700 °C,a...

Design and analysis of an advanced thermal management system for the solar close observations and proximity experiments spacecraft

In this paper,the mission and the thermal environment of the Solar Close Observations and Proximity Experiments(SCOPE)spacecraft are analyzed,and an advanced thermal management system(ATMS)is designed for it.The relationship and functions of the integrated database,the intelligent thermal control system and the efficient liquid cooling system in the ATMS are elaborated upon.For the complex thermal field regulation system and extreme space thermal environment,a modular simulation and thermal field planning method are proposed,and the feasibility of the planning algorithm is verified by numerical simulation.A solar array liquid cooling system is developed,and the system simulation results indicate that the temperatures of the solar arrays meet the requirements as the spacecraft flies by perihelion and aphelion.The advanced thermal management study supports the development of the SCOPE program and provides a reference for the thermal management in other deep-space exploration programs.

Modal and Thermal Analysis of a Modified Connecting Rod of an Internal Combustion Engine Using Finite Element Method

The connecting rod is one of the most important moving components in an internal combustion engine. The present work determined the possibility of using aluminium alloy 7075 material to design and manufacture a connecting rod for weight optimisation without losing the strength of the connecting rod. It considered modal and thermal analyses to investigate the suitability of the material for connecting rod design. The parameters that were considered under the modal analysis were: total deformation, and natural frequency, while the thermal analysis looked at the temperature distribution, total heat flux and directional heat flux of the four connecting rods made with titanium alloy, grey cast iron, structural steel and aluminium 7075 alloy respectively. The connecting rod was modelled using Autodesk inventor2017 software using the calculated parameters. The steady-state thermal analysis was used to determine the induced heat flux and directional heat flux. The study found that Aluminium 7075 alloy deformed more than the remaining three other materials but has superior qualities in terms of vibrational natural frequency, total heat flux and lightweight compared to structural steel, grey cast iron and titanium alloy.

Synthesis and electrochemical properties of Li FePO_(4) cathode material by ionic thermal method using eutectic mixture of tetramethyl ammonium chloride-urea

In this study, the LiFePO_(4) cathode was synthesized by the ionic thermal method using the deep eutectic mixture of tetramethyl ammonium chloride and urea. The synthetic conditions were systematically investigated by orthogonal experiments, which indicate that the optimal reaction time, reaction temperature, molar ratio of Li to DES and rotate speed are 96 h, 220 ℃, 1:14 and20 r·min^(-1), respectively. X-ray diffraction(XRD), scanning electron microscope(SEM) and transmission electron microscope(TEM) were characterized to investigate the crystalline structure and morphology of the obtained materials, indicating well-crystallized LiFePO_(4) with olivine structure. And the physical properties of LiFePO_(4) were explored through Fourier transform infrared spectroscopy(FTIR),57 Fe Mo¨ ssbauer absorption spectra and Raman spectra. An initial discharge capacity can reach 151 m Ah·g^(-1) at 0.1 C rate for LiFePO_(4) following by calcining at 600 ℃ under the optimal conditions, and it retains 125.1 m Ah·g^(-1) after 100 cycles. These results demonstrated that the addition of ionic liquids can improve the rate performance, cycle performance and ion diffusion rate of LiFePO_(4).

Thermal Stresses and Cracks During the Growth of Large-sized Sapphire with SAPMAC Method

The finite-element method has been used to study the thermal stress distribution in large-sized sapphire crystals grown with the sapphire growth technique with micro-pulling and shoulder-expanding at cooled center （SAPMAC） method. A critical defect model has been established to explain the growth and propagation of cracks during the sapphire growing process. It is demonstrated that the stress field depends on the growth rate, the ambient temperature and the crystallizing direction. High stresses always exist near the growth interfaces, at the shoulder-expanding locations, the tailing locations and the sites where the diameters undergo sharp changes. The maximum stresses always occur at the interface of seeds and crystals. Cracks often form in the critical defect region and spread in the m-planes and a-planes under applied tensile stresses during crystal growth. The experimental results have verified that with the improved system of crystal growth and well-controlled techniques, the large-sized sapphire crystals of high quality can be grown due to absence of cracks.

Numerical Investigation of Thermal Behavior of CNC Machine Tool and Its Effects on Dimensional Accuracy of Machined Parts

The dimensional accuracy of machined parts is strongly influenced by the thermal behavior of machine tools (MT). Minimizing this influence represents a key objective for any modern manufacturing industry. Thermally induced positioning error compensation remains the most effective and practical method in this context. However, the efficiency of the compensation process depends on the quality of the model used to predict the thermal errors. The model should consistently reflect the relationships between temperature distribution in the MT structure and thermally induced positioning errors. A judicious choice of the number and location of temperature sensitive points to represent heat distribution is a key factor for robust thermal error modeling. Therefore, in this paper, the temperature sensitive points are selected following a structured thermomechanical analysis carried out to evaluate the effects of various temperature gradients on MT structure deformation intensity. The MT thermal behavior is first modeled using finite element method and validated by various experimentally measured temperature fields using temperature sensors and thermal imaging. MT Thermal behavior validation shows a maximum error of less than 10% when comparing the numerical estimations with the experimental results even under changing operation conditions. The numerical model is used through several series of simulations carried out using varied working condition to explore possible relationships between temperature distribution and thermal deformation characteristics to select the most appropriate temperature sensitive points that will be considered for building an empirical prediction model for thermal errors as function of MT thermal state. Validation tests achieved using an artificial neural network based simplified model confirmed the efficiency of the proposed temperature sensitive points allowing the prediction of the thermally induced errors with an accuracy greater than 90%.

Investigation on the test method of rupture forces of thermal bonding seams in nonwovens shopping bags

超声波热黏合的非织造布接缝不同于普通机织物和针织物等的车缝接缝。运用正交试验设计方法，对纺粘法PP非织造布购物袋热黏合接缝断裂强力测试中的试样宽度、拉伸速率和隔距三个因素进行优化。试验结果表明，试样宽度对纺粘法PP非织造布热黏合接缝断裂强力的测试结果影响最大，并且接缝的断裂强力随着试样宽度的增加而增加。选用试样宽度为200mm、拉伸速率为50mm／min、隔距为100mm的组合所得出的测试结果能比较真实地反映实际的接缝断裂强力。

Analysis of the Temperature Characteristics of High-speed Train Bearings Based on a Dynamics Model and Thermal Network Method

High-speed trains often use temperature sensors to monitor the motion state of bearings.However,the temperature of bearings can be affected by factors such as weather and faults.Therefore,it is necessary to analyze in detail the relationship between the bearing temperature and influencing factors.In this study,a dynamics model of the axle box bearing of high-speed trains is established.The model can obtain the contact force between the rollers and raceway and its change law when the bearing contains outer-ring,inner-ring,and rolling-element faults.Based on the model,a thermal network method is introduced to study the temperature field distribution of the axle box bearings of high-speed trains.In this model,the heat generation,conduction,and dispersion of the isothermal nodes can be solved.The results show that the temperature of the contact point between the outer-ring raceway and rolling-elements is the highest.The relationships between the node temperature and the speed,fault type,and fault size are analyzed,finding that the higher the speed,the higher the node temperature.Under different fault types,the node temperature first increases and then decreases as the fault size increases.The effectiveness of the model is demonstrated using the actual temperature data of a high-speed train.This study proposes a thermal network model that can predict the temperature of each component of the bearings on a high-speed train under various speed and fault conditions.

Study on the condensation and crosslinking reactions of furfuryl alcohol and tris(2-hy-droxyethyl)isocyanurate by thermal methods

Condensation and crosslinking reactions of furfuryl alcohol(FA)and FA with tris(2-hydro- xyethyl)isocyanurate(THEIC)are studied by means of DSC,TG,TBA,NMR and elemental analysis. Four exothermic peaks are observed on the DSC curves of thermal condensation of FA and FA with THEIC in the presence of sulfuric acid.The peaks Ⅰ,Ⅱ(50—80℃),Ⅲ(110—130℃)and Ⅳ(150— 190℃)correspond to linear polycondensation of FA through head-to-tail condensation,head-to-head etherification,crosslinking dehydration reaction between methylene group and terminal hydroxy group of FA polymeric chain and to further crosslinking reaction at higher temperature,respectively.The reactivity of FA and THEIC increases sharply at 130—150℃ and THEIC is reacted completely at 150℃.Addition of THEIC raises the initial decomposition temperature of FA polymer by 60℃.

Synthesis and growth mechanism of SiC/SiO2 nanochains by catalyst-free thermal evaporation method in Ar/CO atmosphere

SiC/SiO2 nanochains were synthesized on a carbon fiber substrate by a catalyst-free thermal evaporation method in the Ar/CO atmosphere.X-ray diffraction(XRD),Fourier-transform infrared spectroscopy(FT-IR),scanning electron microscopy(SEM)and transmission electron microscopy(TEM)revealed that the as-synthesized SiC/SiO2 nanochains are composed of single-crystalline SiC nanowires and amorphous SiO2 beads.The introduction of CO can promote the formation of SiO2,so that the SiC/SiO2 nanochains are subsequently formed during cooling.In addition,the photoluminescence spectrum of SiC/SiO2 nanochains showed a broad emission peak at around 350 nm,which is ascribed to the oxygen discrepancy in the SiO2 beads as well as the SiC/SiO2 interfacial effect.These findings can provide guidance for further study of the vapor growth of 1D SiC-based materials.

SILICON NITRIDE POWDER SYNTHESIZED BY THERMAL PLASMA METHOD

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Analysis of temperature field for a surface-mounted and interior permanent magnet synchronous motor adopting magnetic-thermal coupling method

Aiming at obtaining high power density of surface-mounted and interior permanent magnet synchronous motor(SIPMSM),it is important to accurately calculate the temperature field distribution of SIPMSM,and a magnetic-thermal coupling method is proposed.The magnetic-thermal coupling mechanism is analyzed.The thermal network model and finite element model are built by this method,respectively.The effects of power frequency on iron losses and temperature fields are analyzed by the magnetic-thermal coupling finite element model under the condition of rated load,and the relationship between the load and temperature field is researched under the condition of the synchronous speed.In addition,the equivalent thermal network model is used to verify the magnetic-thermal coupling method.Then the temperatures of various nodes are obtained.The results show that there are advantages in both computational efficiency and accuracy for the proposed coupling method,which can be applied to other permanent magnet motors with complex structures.

A FINITE VOLUME ELEMENT METHOD FOR THERMAL CONVECTION PROBLEMS

Consider the finite volume element method for the thermal convection problem with the infinite Prandtl number. The author uses a conforming piecewise linear function on a fine triangulation for velocity and temperature, and a piecewise constant function on a coarse triangulation for pressure. For general triangulation the optimal order H1 norm error estimates are given.

Simulation of natural convection under high magnetic field by means of the thermal lattice Boltzmann method

The thermal lattice Boltzmann method （TLBM）, which was proposed by J. G. M. Eggels and J. A. Somers previously, has been improved in this paper. The improved method has introduced a new equilibrium solution for the temperature distribution function on the assumption that flow is incompressible, and it can correct the effect of compressibility on the macroscopic temperature computed. Compared to the previous method, where the half- way bounce back boundary condition was used for non-slip velocity and temperature, a non-equilibrium extrapolation scheme has been adopted for both velocity and temperature boundary conditions in this paper. Its second-order accuracy coincides with the ensemble accuracy of lattice Boltzmann method. In order to validate the improved thermal scheme, the natural convection of air in a square cavity is simulated by using this method. The results obtained in the simulation agree very well with the data of other numerical methods and benchmark data. It is indicated that the improved TLBM is also successful for the simulations of non-isothermal flows. Moreover, this thermal scheme can be applied to simulate the natural convection in a non-uniform high magnetic field. The simulation has been completed in a square cavity filled with the aqueous solutions of KC1 （llwt%）, which is considered as a diamagnetic fluid with electrically low-conducting, with Grashof number Gr=4.64~104 and Prandtl number Pr----7.0. And three cases, with different cavity locations in the magnetic field, have been studied. In the presence of a high magnetic field, the natural convection is quenched by the body forces exerted on the electrically low-conducting fluids, such as the magnetization force and the Lorentz force. From the results obtained, it can be seen that the quenching efficiencies decrease with the variation of location from left, symmetrical line, to the right. These phenomena originate from the different distributions of the magnetic field strengths in the zones of the symmetrical central line of the magnetic fields. The results are also compared with those without a magnetic field. Finally, we can conclude that the improved TLBM will enable effective simulation of the natural convection under a high magnetic field.

Thermal conductivity measurements on xonotlite-type calcium silicate by the transient hot-strip method

The experimental results of the thermal conductivities of xonotlite-type calcium silicate insulation materials were presented at different temperatures and pressures. Two appropriative surroundings, i.e. an elevated temperature surrounding from ambient temperature to 1450 K and a vacuum surrounding from atmosphere pressure to 10-3 Pa, were designed for the transient hot-strip （THS） method. The thermal conductivities of xonotlite-type calcium silicate with four densities from ambient temperature to 1000 K and 0.045 Pa to atmospheric pressure were measured. The results show that the thermal conductivity of xonotlite-type calcium silicate decreases apparently with the fall of density, and decreases apparently with the drop of pressure, and reaches the least value at about 100 Pa. The thermal conductivity of xonotlite-type calcium silicate increases almost linearly with T0, and increases more abundantly with low density than with high density. The thermal conductivity measurement uncertainty is estimated to be approximately 3% at ambient temperature, and 6% at 800 K.

Analysis of Temperature Rise in High-Speed Permanent Magnet Synchronous Traction Motors by Coupling the Equivalent Thermal Circuit Method and Computational Fluid Dynamics

To solve the problem of temperature rise caused by the high power density of high-speed permanent magnet synchronous traction motors,the temperature rise of various components in the motor is analyzed by coupling the equivalent thermal circuit method and computational fluid dynamics.Also,a cooling strategy is proposed to solve the problem of temperature rise,which is expected to prolong the service life of these devices.First,the theoretical bases of the approaches used to study heat transfer and fluid mechanics are discussed,then the fluid flow for the considered motor is analyzed,and the equivalent thermal circuit method is introduced for the calculation of the temperature rise.Finally,the stator,rotor loss,motor temperature rise,and the proposed cooling method are also explored through experiments.According to the results,the stator temperature at 50,000 r/min and 60,000 r/min at no-load operation is 68℃ and 76℃,respectively.By monitoring the temperature of the air outlets inside and outside the motor at different speeds,it is also found that the motor reaches a stable temperature rise after 65 min of operation.Coupling of the thermal circuit method and computational fluid dynamics is a strategy that can provide the average temperature rise of each component and can also comprehensively calculate the temperature of each local point.We conclude that a hybrid cooling strategy based on axial air cooling of the inner air duct of the motor and water cooling of the stator can meet the design requirements for the ventilation and cooling of this type of motors.

Refractory Material—Determination of Thermal Expansion-Push Rod Method

1 Scope This standard specifies thermal expansion test method of refractories by push rod method.

Differential transformation method for studying flow and heat transfer due to stretching sheet embedded in porous medium with variable thickness, variable thermal conductivity,and thermal radiation

This article presents a numerical solution for the flow of a Newtonian fluid over an impermeable stretching sheet embedded in a porous medium with the power law surface velocity and variable thickness in the presence of thermal radiation. The flow is caused by non-linear stretching of a sheet. Thermal conductivity of the fluid is assumed to vary linearly with temperature. The governing partial differential equations （PDEs） are transformed into a system of coupled non-linear ordinary differential equations （ODEs） with appropriate boundary conditions for various physical parameters. The remaining system of ODEs is solved numerically using a differential transformation method （DTM）. The effects of the porous parameter, the wall thickness parameter, the radiation parameter, the thermal conductivity parameter, and the Prandtl number on the flow and temperature profiles are presented. Moreover, the local skin-friction and the Nusselt numbers are presented. Comparison of the obtained numerical results is made with previously published results in some special cases, with good agreement. The results obtained in this paper confirm the idea that DTM is a powerful mathematical tool and can be applied to a large class of linear and non-linear problems in different fields of science and engineering.

An Effective Thermal Splicing Method to Join Fluoride and Silica Fibers for a High Power Regime

A repeatable and simple thermal splicing method for low loss splice between fluoride and silica fibers is presented. The minimum splicing loss of 0.58 dB is achieved experimentally with this approach, Meanwhile, the power capacity of this splicing joint is also tested with a high power fiber laser. The maximum input power is up to 15 W, only limited by the available power of the laser source. To the best of our knowledge, this is the first report on thermal splicing between fluoride and silica fibers operating in a high power regime without any complicated ion-assisted deposition process.

A MIXED METHOD OF DETERMINING THETHERMAL STRESS FOR COLD ROLLER

A mixed method which combines the recent developed finite analytical method and the boundary fitting coordinate transformation method was used first to calculate the temperature field and thermal stress field of the cold roller in this paper. The following results are obtained by the calculation: thermal stresses σr=0, σθ=σz are maximum tension stress on the inner surface of the cold roller and σr=0, |σθ|=|σz| are maximum compression stress on the outer surface of the cold roller in the steady and unsteady case. Effectiveness and validity of the mixed method are checked with steady coil roller problems having theoretical solutions. The results show that good agreement is achived between the calculated value and theoretical solution,and the mixed method used in the paper is very workable. The mixed method is also useful in solving the steady and unsteady thermal stress field proplems of the hot -rolled for the reversing rolling mill and the continous rolling mill.