The title compound 2-(4-methylbenzoly)-3-(4-chlrolphenyl)-4-(1,2,4-triazole)-5- anilino-thiopene has been prepared and characterized by IR, EA, 1H NMR, UV, MS and X-ray analysis. It crystallizes in the triclinic syste...The title compound 2-(4-methylbenzoly)-3-(4-chlrolphenyl)-4-(1,2,4-triazole)-5- anilino-thiopene has been prepared and characterized by IR, EA, 1H NMR, UV, MS and X-ray analysis. It crystallizes in the triclinic system, space group P1 with a = 8.061(2), b = 9.981(2), c = 15.462(3) ? a = 90.96(3), b = 103.11(3), g = 106.26(3)? Mr = 470.96 (C26H19ClN4OS), V = 1158.8(4) 3, Z = 2, Dc = 1.350 g/cm3, F(000) = 488, = 0.282 mm-1, R = 0.0482 and wR = 0.1043. In the crystal lattice, there exist some intermolecular hydrogen bonds, - stacking interactions and CH贩?supramolecular interactions. In the solid state, all of the above intermolecular interactions in the title compound can stabilize the crystal structure.展开更多
基金This work was supported by the Natural Science Foundation of Shandong Province (No. Y2002B06)
文摘The title compound 2-(4-methylbenzoly)-3-(4-chlrolphenyl)-4-(1,2,4-triazole)-5- anilino-thiopene has been prepared and characterized by IR, EA, 1H NMR, UV, MS and X-ray analysis. It crystallizes in the triclinic system, space group P1 with a = 8.061(2), b = 9.981(2), c = 15.462(3) ? a = 90.96(3), b = 103.11(3), g = 106.26(3)? Mr = 470.96 (C26H19ClN4OS), V = 1158.8(4) 3, Z = 2, Dc = 1.350 g/cm3, F(000) = 488, = 0.282 mm-1, R = 0.0482 and wR = 0.1043. In the crystal lattice, there exist some intermolecular hydrogen bonds, - stacking interactions and CH贩?supramolecular interactions. In the solid state, all of the above intermolecular interactions in the title compound can stabilize the crystal structure.
