Bonding enhancement of cold rolling TA1 P-Ti/AA6061 composite plates via surface oxidation treatment

TA1 P-Ti/AA6061 composite plate was produced by oxidizing the surface of the titanium plate and adopting a cold roll bonding process.The results revealed that the oxide film(Ti6O)prepared on the surface of TA1 pure titanium was easy to crack during the cold roll bonding,thereby promoting the formation of an effective mechanical interlock at the interface,which can effectively reduce the minimum reduction rate of the composite plates produced by cold rolling of titanium and aluminium plates.Moreover,the composite plate subjected to oxidation treatment exhibited high shear strength,particularly at a 43%reduction rate,achieving a commendable value of 117 MPa.Based on oxidation treatment and different reduction rates,the annealed composite plates at temperatures of 400,450,and 500°C displayed favorable resistance to interface delamination,highlighting their remarkable strength-plasticity compatibility as evidenced by a maximum elongation of 31.845%.

Relationship between Hardness and Deformation during Cold Rolling Process of Complex Profles

The hardening on surface of complex profles such as thread and spline manufactured by cold rolling can efectively improve the mechanical properties and surface quality of rolled parts. The distribution of hardness in superfcial layer is closely related to the deformation by rolling. To establish the suitable correlation model for describing the relationship between strain and hardness during cold rolling forming process of complex profles is helpful to the optimization of rolling parameters and improvement of rolling process. In this study, a physical analog experiment refecting the uneven deformation during complex-profle rolling process has been extracted and designed, and then the large date set (more than 400 data points) of training samples refecting the local deformation characteristics of complexprofle rolling have been obtained. Several types of polynomials and power functions were adopted in regression analysis, and the regression correlation models of 45# steel were evaluated by the single-pass and multi-pass physical analog experiments and the complex-profle rolling experiment. The results indicated that the predicting accuracy of polynomial regression model is better in the strain range (i.e., ε < 1.2) of training samples, and the correlation relationship between strain and hardness out strain range (i.e., ε > 1.2) of training samples can be well described by power regression model;so the correlation relationship between strain and hardness during complex-profle rolling process of 45# steel can be characterized by a segmented function such as third-order polynomial in the range ε < 1.2 and power function with a ftting constant in the range ε > 1.2;and the predicting error of the regression model by segmented function is less than 10%.

Effects of cold rolling and heat treatment on microstructure and mechanical properties of AA 5052 aluminum alloy

The microstructures and mechanical properties of homogenized-rolled AA5052 aluminum alloys with different rolling reductions and following annealing treatments were investigated by optical microscope, scanning electron microscope, X-ray diffractometer, micro-hardness and tensile tests. The results show that with increasing rolling reduction, the equiaxed grains are elongated along the rolling direction obviously, and accumulation of rolling reduction increases the work hardening effect, which results in the enhanced strength and degraded plasticity. When rolling reduction is 87%, the ultimate tensile strength reaches 325 MPa but elongation is only 2.5%. There are much more secondary phase precipitates after annealing treatment. With an increase of annealing temperature, the amount of precipitates increases and work hardening diminishes continuously. The elongation is improved to ~23% but the tensile strength is decreased to 212 MPa after annealing at 300 °C for 4 h, which are comparable to those of as-homogenized alloy.

Multilayered Ti-Al intermetallic sheets fabricated by cold rolling and annealing of titanium and aluminum foils

Multilayered Ti-Al based intermetallic sheets were fabricated by sintering alternately layered titanium and aluminum foils.The microstructure and phase formation of the obtained sheets under different sintering conditions were evaluated by various techniques.The results reveal that when the sintering temperature is above the melting point of aluminum,the self-propagating high-temperature synthesis reaction occurs between Ti and Al,and forms various phases of Ti-based solid solutions including α-Ti Ti3Al,TiAl,TiAl2 and α-Ti including TiAl3,etc.When the sintering time increased,Ti-based solid solution,TiAl2 and TiAl3 disappeared gradually,and the sheet containing Ti3Al and TiAl phases in a multilayered structure formed finally.A lot of voids were also observed in the sintered structures,which were caused by the melting Al,Kirkendall effect and the difference of molar volumes between reactants and products.The voids were eliminated and a dense sample was obtained by the following hot press.

Strength enhancement of Mg-3Gd-1Zn alloy by cold rolling

The severe cold rolling was employed to enhance strength of Mg-3Gd-lZn （mass fraction, %） alloy sheet. The 0.2% yield stress of the Mg-3Gd-1Zn hot-rolled sheet can be increased by 150% through the single-pass cold rolling with the reduction of 23%, due to the high intensity of dislocation and basal texture established during cold rolling. Compared with the Mg-3Gd-lZn hot-rolled sheet, the cold-rolled sheet annealed at 350 for 30 min may get an enhancement in strength without a great loss of ductility. The sheet processed by multi-pass cold rolling does not show a higher strength as expected, due to the softening effect of shear bands. However, the thin slab with the thickness less than 1 mm can be produced by the multi-pass cold rolling with the annealing treatment as few as possible.

Deformation mechanism of cold ring rolling in view of texture evolution predicted by a newly proposed polycrystal plasticity model

An explicit polycrystal plasticity model was proposed to investigate the deformation mechanism of cold ring rolling in view of texture evolution. The model was created by deducing a set of linear incremental controlling equations within the framework of crystal plasticity theory. It was directly solved by a linear algorithm within a two-level procedure so that its efficiency and stability were guaranteed. A subroutine VUMAT for ABAQUS/Explicit was developed to combine this model with the 3D FE model of cold ring rolling. Results indicate that the model is reliable in predictions of stress-strain response and texture evolution in the dynamic complicated forming process; the shear strain in RD of the ring is the critical deformation mode according to the sharp Goss component （{110}？100？） of deformed ring; texture and crystallographic structure of the ring blank do not affect texture type of the deformed ring;texture evolves rapidly at the later stage of rolling, which results in a dramatically increasing deformation of the ring.

MECHANICS ANALYSIS ON PRECISE FORMING PROCESS OF EXTERNAL SPLINE COLD ROLLING

According to the suitable assumption, the deformation process of external spline cold rolling is analyzed. By the graphing method, the slip-line field of plastically deforming area in process of external spline cold rolling is set up. Different friction-conditions are used in different contact areas in order to realistically reflect the actual situation. The unit average pressure on contact surface of the rolling process is solved according to the stress filed theory of slip-line. And the formulae of the rolling-force and rolling-moment are established. The theoretical result is well consistent with the finite element analysis. A theoretical basis is provided for the precise forming process of spline cold rolling and the production of external splined shafts.

Research and Development Trend of Shape Control for Cold Rolling Strip

Shape is an important quality index of cold rolling strip. Up to now, many problems in the shape control domain have not been solved satisfactorily, and a review on the research progress in the shape control domain can help to seek new breakthrough directions. In the past 10 years, researches and applications of shape control models, shape control means, shape detection technology, and shape con- trol system have achieved significant progress. In the aspect of shape control models, the researches in the past improve the accuracy, speed and robustness of the models. The intelligentization of shape control models should be strengthened in the future. In the aspect of the shape control means, the researches in the past focus on the roll opti- mization, mill type selection, process optimization, local strip shape control, edge drop control, and so on. In the future, more attention should be paid to the coordination control of both strip shape and other quality indexes, and the refinement of control objective should be strengthened. In the aspects of shape detection technology and shape control system, some new types of shape detection meters and shape control systems are developed and have successfully indus- trial applications. In the future, the standardization of shape detection technology and shape control system should be promoted to solve the problem of compatibility. In general,the four expected development trends of shape control for cold roiling strip in the future are intelligentization, coordi- nation, refinement, and standardization. The proposed research provides new breakthrough directions for improv- ing shape quality.

Rolling Force and Rolling Moment in Spline Cold Rolling Using Slip-line Field Method

Rolling force and rolling moment are prime process parameter of external spline cold rolling. However, the precise theoretical formulae of rolling force and rolling moment are still very fewer, and the determination of them depends on experience. In the present study, the mathematical models of rolling force and rolling moment are established based on stress field theory of slip-line. And the isotropic hardening is used to improve the yield criterion. Based on MATLAB program language environment, calculation program is developed according to mathematical models established. The rolling force and rolling moment could be predicted quickly via the calculation program, and then the reliability of the models is validated by FEM. Within the range of module of spline m=0.5-1.5 mm, pressure angle of reference circle α=30.0°-45.0°, and number of spline teeth Z=19-54, the rolling force and rolling moment in rolling process （finishing rolling is excluded） are researched by means of virtualizing orthogonal experiment design. The results of the present study indicate that： the influences of module and number of spline teeth on the maximum rolling force and rolling moment in the process are remarkable; in the case of pressure angle of reference circle is little, module of spline is great, and number of spline teeth is little, the peak value of rolling force in rolling process may appear in the midst of the process; the peak value of rolling moment in rolling process appears in the midst of the process, and then oscillator weaken to a stable value. The results of the present study may provide guidelines for the determination of power of the motor and the design of hydraulic system of special machine, and provide basis for the farther researches on the precise forming process of external spline cold rolling.

Texture evolution of commercial pure Ti during cold rolling and recrystallization annealing

X-ray diffraction （XRD） was employed to analyze the texture evolution of commercial pure （CP） Ti during cold rolling and re- crystallization annealing. The texture components were measured by electron backscattered diffraction （EBSD） after recrystallization an- nealing. The CP Ti tends to form a texture with the basal pole tilted 30°-40° away from the normal direction toward the transverse direction. The texture of the initial hot-rolled plate can be classified into three kinds, i.e., the pyramid texture （1013）[5230] and （2021）[1015], the basal plane texture （0001）[2110], and the stronger_prism_texture （1120）[0001]. After cold rolling and annealing （700℃,60 min）,_the main texture components are the cold-rolled texture （1125）[1123] and the recrystallized texture （1013）[5230]. The texture （2021）[1015] is in- herited from the texture of the initial hot-rolled plate with the decrease of orientation density gradually. The volume contents of the cold-rolled texture {2115}（0110） and the recrystallized texture {1013}（1210） are calculated by EBSD. After recrystallization annealing, the specimen is rich in the recrystallized texture and inherits some of texture components from the cold-rolled texture. When the annealing time is prolonged, the anisotropic value decreases.

Microstructural Evolution of Pearlite in Eutectoid Fe-C Alloys during Severe Cold Rolling

The microstructural evolution of pearlite during severe cold rolling in Fe-0.8C binary alloy and Fe-1Mn-0.8C ternary alloys was investigated by using SEM, TEM and XRD etc. The results show that the deformed pearlite consists of irregularly bent lamella, coarse lamella with shear-band and fine lamella. As the rolling reduction increases, the proportion of fine lamella increases. The strong plastic deformation, amorphization and dissolution of cementite take place during the severe cold rolling. The maximum carbon content in ferrite reaches 0.15 mass% after 90% cold rolling.

Control of Surface Thermal Scratch of Strip in Tandem Cold Rolling

The thermal scratch seriously affects the surface quality of the cold rolled stainless steel strip. Some researchers have carried out qualitative and theoretical studies in this field. However, there is currently a lack of research on effective forecast and control of thermal scratch defects in practical production, especially in tandem cold rolling. In order to establish precise mathematical model of oil film thickness in deformation zone, the lubrication in cold rolling process of SUS410L stainless steel strip is studied, and major factors affecting oil film thickness are also analyzed. According to the principle of statistics, mathematical model of critical oil film thickness in deformation zone for thermal scratch is built, with fitting and regression analytical method, and then based on temperature comparison method, the criterion for deciding thermal scratch defects is put forward. Storing and calling data through SQL Server 2010, a software on thermal scratch defects control is developed through Microsoft Visual Studio 2008 by MFC technique for stainless steel in tandem cold rolling, and then it is put into practical production. Statistics indicate that the hit rate of thermal scratch is as high as 92.38%, and the occurrence rate of thermal scratch is decreased by 89.13%. Owing to the application of the software, the rolling speed is increased by approximately 9.3%. The software developed provides an effective solution to the problem of thermal scratch defects in tandem cold rolling, and helps to promote products surface quality of stainless steel strips in practical production.

TOOTH CURVES AND ENTIRE CONTACT AREA IN PROCESS OF SPLINE COLD ROLLING

In spline rolling process, the contact area between roller and workpiece plays an important role in calculating rolling-force and rolling-moment. For the purpose of studying the contact area, contact state between roller and workpiece in process of spline cold rolling based upon cross rolling is analyzed. According to the suitable hypothesis, the mathematic model of roller-tooth-curve in optional position of rolling process is established. Combing the theory of conjugate curves with the theory of envelope curve, the corresponding mathematic model of workpiece-tooth-curve is established. By utilizing establishing mathematic models, the algorithm of entire contact area in rolling process is created. On the basis of the algorithm, calculation-program is compiled under MATLAB program language environment. The calculation-program actualizes quantitative analysis and quantitative calculation of contact areas. Utilizing the calculation-program, the influence of parameters on contact area is analyzed, and the tendency is consistent with the manufacturing experience. In consideration of rolling-force optimization, the primary process parameters may be selected according to results of calculation. The result of the present study may provide basis for research on rolling-force and rolling-moment.

EVALUATION OF LUBRICANTS FOR COLD ROLLING ALUMINUM STRIPS

Various kinds of base oils were applied to cold rolling aluminum strips on a test mill for evaluationof the influences of these base oils,aromatics contents and viscosity of base oils on their lubricating performances and surface reflectivity of rolled strips at annealing. Results showed that low friction coefficient androlling force were obtained by using the normal paraffins,whereas their contaminations on the annealed stripsurface were the same as those of other saturated hydrocarbons. Aromatics in base oil affected the stir face reflectivity of annealed strips, but the decrease of aromatics in base oil was ineffective to improve rolled stripssurface quality when it is less than 1 %. Base oil viscosity has the great influences on the lubricating performances and surface reflectivity of annealed strips just in this condition.

Microstructure and textural evolution during cold rolling and annealing of commercially pure titanium sheet

The effects of cold rolling and annealing on the microstructure and textural evolution of a commercially pure titanium（CP-Ti） sheet were investigated. Electron backscatter diffractometry demonstrates that the deformation during rolling is accommodated by twinning and slip. Additionally, twinning is the dominant deformation mechanism when the cold rolling reduction is less than 40%. During rolling, {11ˉ22}11ˉ2ˉ3contraction twinning（CT） and {10ˉ12}10ˉ11 extension twinning（ET） are activated. And, the intensity of the（0002） pole along the ND gradually increases with increasing deformation. During annealing, the fraction of low angle grain boundaries（LAGBs） and the intensity of the（0002） pole along the ND gradually decrease slightly with increasing annealing time, while twinning lamellae disappear rapidly. When the annealing time reaches 60 min, 20% cold-rolled sheet recrystallizes almost completely.

FEM Analysis of Rolling Pressure Along Strip Width in Cold Rolling Process

Using 3-D elastic-plastic FEM, the cold strip rolling process in a 4-high mill was simulated. The elastic deformation of rolls, the plastic deformation of the strip, and the pressure between the work roll and the backup roll were taken into account. The distribution of rolling pressure along the strip width was obtained. Based on the simulation results, the peak value of rolling pressure and the location of the peak were analyzed under different rolling conditions. The effects of the roll bending force and the strip width on the distribution of rolling pressure along the width direction were determined.

Effect of cold rolling on the microstructural, magnetic, mechanical, and corrosion properties of AISI 316L austenitic stainless steel

This study has evaluated the effect of different levels of cold rolling（from 0 to 50%）on the microstructural,magnetic,and mechanical properties and the corrosion behavior of 316L austenitic stainless steel in Na Cl（1 mol/L）＋H_2SO_4（0.5 mol/L）solution.Microstructural examinations using optical microscopy revealed the development of a morphological texture from coaxial to elongated grains during the cold-rolling process.Phase analysis carried out on the basis of X-ray diffraction confirmed the formation of the ferromagneticα′-martensite phase under the stresses applied during cold rolling.This finding is in agreement with magnetic measurements using a vibrating sample magnetometer.Mechanical properties determined by tensile and Vickers microhardness tests demonstrated an upward trend in the hardness-to-yield strength ratio with increasing cold-rolling percentage,representing a reduction in the material’s work-hardening ability.Uniform and localized corrosion parameters were estimated via potentiodynamic polarization corrosion tests and electrochemical impedance spectroscopy.In contrast to the uniform corrosion,wherein the corrosion current density increased with increasing cold-working degree because of the high density of microstructural defects,the passive potential range and breakdown potential increased by cold working,showing greater resistance to pit nucleation.Although pits were formed,the cold-rolled material repassivation tendency decreased because of the broader hysteresis anodic loop,as confirmed experimentally by observation of the microscopic features after electrochemical cyclic polarization evaluations.

Numerical simulation of involutes spline shaft in cold rolling forming

Design of forming dies and whole process of simulation of cold rolling involutes spline can be realized by using of CAD software of PRO-E and CAE software of DEFORM-3D. Software DEFORM-3D provides an automatic and optimized remeshing function, especially for the large deformation. In order to use this function sufficiently, simulation of cold rolling involutes spline can be implemented indirectly. The relationship between die and workpiece, forming force and characteristic of deformation in the forming process of cold rolling involutes spline are analyzed and researched. Meanwhile, reliable proofs for the design of dies and deforming equipment are provided.

Recycle of valuable products from oily cold rolling mill sludge

Oily cold rolling mill （CRM） sludge contains lots of iron and alloying elements along with plenty of hazardous organic components, which makes it as an attractive secondary source and an environmental contaminant at the same time. The compound methods of ＂vacuum distillation ＋ oxidizing roasting＂ and ＂vacuum distillation ＋ hydrogen reduction＂ were employed for the recycle of oily cold rolling mill sludge. First, the sludge was dynamically vacuum distilled in a rotating furnace at 50 r/rain and 600℃ for 3 h, which removed almost hazardous organic components, obtaining 89.2wt% ferrous resultant. Then, high purity ferric oxide powders （99.2wt%） and reduced iron powders （98.9wt%） were obtained when the distillation residues were oxidized and reduced, respectively. The distillation oil can be used for fuel or chemical feedstock, and the distillation gases can be collected and reused as a fuel.

Research and Application of Non-symmetrical Roll Bending Control of Cold Rolling Mill

The existing research of the flatness control for strip cold rolling mainly focuses on the calculation of the optimum adjustment of individual flatness actuator in accordance with the flatness deviation, which can be used for general flatness control. However, it does not work for some special rolling processes, such as the elimination of ultra single side edge-waves and the prevention of strip break due to tilting roll control overshooting. For the purpose of solving these problems, the influences of non-symmetrical work roll bending and intermediate roll bending on flatness control were analyzed by studying efficiencies of them. Moreover, impacts of two kinds of non-symmetrical roll bending control on the pressure distribution between rolls were studied theoretically. A non-symmetrical work roll bending model was developed by theoretical analysis in accordance with practical conditions. The model was applied to the revamp of a 1250 6-H reversible universal crown mill (UCM) cold mill. Theoretical study and practical applications show that the coordination utilization of the non-symmetrical work roll bending control and tilting roll control was effective in flatness control when there appeared bad strip single side edge waves, especially when the incoming strip was with a wedge shape. In addition, the risk of strip break due to tilting control overshooting could be reduced. Furthermore, the non-symmetrical roll bending control can reduce the extent of uneven distribution of pressure between rolls caused by intermediate roll shifting in flatness control and slow down roll wear. The non-symmetrical roll bending control technology has important theoretical and practical significance to better flatness control.