The title compound 4-(3,4-methylenedioxylphenyl)-6-methyl-5-ethoxycaronyl-3,4- dihydropyrimidin-2(H)-one (C15H16N2O5) has been synthesized and determined by single-crystal X-ray diffraction. The crystal is of triclini...The title compound 4-(3,4-methylenedioxylphenyl)-6-methyl-5-ethoxycaronyl-3,4- dihydropyrimidin-2(H)-one (C15H16N2O5) has been synthesized and determined by single-crystal X-ray diffraction. The crystal is of triclinic, space group P with a = 7.580(1), b = 7.920(2), c = 13.168(4) ? a = 96.44(2), b = 96.71(2), g = 109.81(2), V = 728.8(3) 3, Z = 2, Mr = 304.30, Dc = 1.387 g/cm3, F(000) = 320, m(MoKa) = 0.105 mm-1 (l = 0.71073 ?, R = 0.0446 and wR = 0.1205. In the molecule the pyrimidine ring adopts a boat conformation.展开更多
基金Supported by the National Natural Science Foundation of China (No. 20372057) Natural Science Foundation of Jiangsu Province (No. BK2001142) and the Natural Science Foundation of Jiangsu Education Department (No. 01KJB150008) and Jiangsu Provincial
文摘The title compound 4-(3,4-methylenedioxylphenyl)-6-methyl-5-ethoxycaronyl-3,4- dihydropyrimidin-2(H)-one (C15H16N2O5) has been synthesized and determined by single-crystal X-ray diffraction. The crystal is of triclinic, space group P with a = 7.580(1), b = 7.920(2), c = 13.168(4) ? a = 96.44(2), b = 96.71(2), g = 109.81(2), V = 728.8(3) 3, Z = 2, Mr = 304.30, Dc = 1.387 g/cm3, F(000) = 320, m(MoKa) = 0.105 mm-1 (l = 0.71073 ?, R = 0.0446 and wR = 0.1205. In the molecule the pyrimidine ring adopts a boat conformation.
