Reagents are optimized for the simultaneous determination of trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in zinc sulfate solution, which contains an extremely large excess of Zn^(2+). First, the reagents and their d...Reagents are optimized for the simultaneous determination of trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in zinc sulfate solution, which contains an extremely large excess of Zn^(2+). First, the reagents and their doses for the experiment are selected according to the characteristics of the zinc sulfate solution. Then, the reagent doses are optimized by analyzing the influence of reagent dose on the polarographic parameters(i.e. half-wave potential E_(1/2) and limiting diffusion current I_p). Finally, the optimization results are verified by simultaneously determining trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in the presence of an extremely large excess of Zn^(2+). The determination results indicate that the optimized reagents exhibit wide linearity, low detection limits, high accuracy and good precision for the simultaneous determination of trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in the presence of an extremely large excess of Zn^(2+).展开更多
Assessment of the current status of Lake Baikal proved to be based on changes in natural (“preindustrial”) chemical content in basic abiotic and biological compartments of the Lake geosystem. This approach was used ...Assessment of the current status of Lake Baikal proved to be based on changes in natural (“preindustrial”) chemical content in basic abiotic and biological compartments of the Lake geosystem. This approach was used to evaluate background “base-line levels” of 6 major and about 50 minor and trace ele-ments in the Lake Baikal water body using a number of most reliable data re-ported within 1992-2012. In terms of environment geochemistry Baikal is one of the purest water reservoirs on the Earth. A simple mass balance model was proposed for assessing possible anthropogenic impact on Baikal water geo-chemistry. Estimations of change trends showed that only for Na+, SO42-, Cl- and Mo growth rate of their average concentrations in the Lake occurred to be 1%, 3%, 7% and 2% in every 10 years. Space-time monitoring schedules for all water body compartments of the Lake are proposed as well as similar moni-toring programs for tributaries, precipitations, bottom sediments, aquatic biota.展开更多
Trace is the important composition structure of printed circuit board,w hich connects the devices,it is also the module that taking up the highest proportion,thus,it is the major testing target of quality assurance. T...Trace is the important composition structure of printed circuit board,w hich connects the devices,it is also the module that taking up the highest proportion,thus,it is the major testing target of quality assurance. The sunken defects proposed in this paper is a w idth abnormity defect on the FPC trace,w hich w ould cause the latent open circuit defect and affect the electrical function of circuit. The problem of flexible deformation and w idth difference make the FPC trace detection harder. Therefore,this paper proposed a detection scheme combined w ith linear masks and circle distribution characteristic. Firstly,this scheme preprocessed the acquired FPC image,divided the trace into several sub-regions and obtained the line w idth values of each trace transverse section. Then the line w idth sequences w ere searched w ith the linear difference template of gray scale. Thus,the sunken defects alternative positions w ere located. Lastly,the circle distribution characteristic is defined to identify the real defect areas from the alternative regions acquired from the previous step. Thus,the detection of sunken defects on the FPC trace w as accomplished.The algorithm w as tested in the self-built image database,w hich show s the better detection performance than the other typical algorithms.展开更多
基金Projects(61533021,61321003,61273185)supported by the National Natural Science Foundation of ChinaProject(2015CX007)supported by the Innovation-driven Plan in Central South University,ChinaProject(13JJ8003)supported by the Joint Fund of Hunan Provincial Natural Science Foundation of China
文摘Reagents are optimized for the simultaneous determination of trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in zinc sulfate solution, which contains an extremely large excess of Zn^(2+). First, the reagents and their doses for the experiment are selected according to the characteristics of the zinc sulfate solution. Then, the reagent doses are optimized by analyzing the influence of reagent dose on the polarographic parameters(i.e. half-wave potential E_(1/2) and limiting diffusion current I_p). Finally, the optimization results are verified by simultaneously determining trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in the presence of an extremely large excess of Zn^(2+). The determination results indicate that the optimized reagents exhibit wide linearity, low detection limits, high accuracy and good precision for the simultaneous determination of trace amounts of Cu^(2+), Cd^(2+) and Co^(2+) in the presence of an extremely large excess of Zn^(2+).
文摘Assessment of the current status of Lake Baikal proved to be based on changes in natural (“preindustrial”) chemical content in basic abiotic and biological compartments of the Lake geosystem. This approach was used to evaluate background “base-line levels” of 6 major and about 50 minor and trace ele-ments in the Lake Baikal water body using a number of most reliable data re-ported within 1992-2012. In terms of environment geochemistry Baikal is one of the purest water reservoirs on the Earth. A simple mass balance model was proposed for assessing possible anthropogenic impact on Baikal water geo-chemistry. Estimations of change trends showed that only for Na+, SO42-, Cl- and Mo growth rate of their average concentrations in the Lake occurred to be 1%, 3%, 7% and 2% in every 10 years. Space-time monitoring schedules for all water body compartments of the Lake are proposed as well as similar moni-toring programs for tributaries, precipitations, bottom sediments, aquatic biota.
文摘Trace is the important composition structure of printed circuit board,w hich connects the devices,it is also the module that taking up the highest proportion,thus,it is the major testing target of quality assurance. The sunken defects proposed in this paper is a w idth abnormity defect on the FPC trace,w hich w ould cause the latent open circuit defect and affect the electrical function of circuit. The problem of flexible deformation and w idth difference make the FPC trace detection harder. Therefore,this paper proposed a detection scheme combined w ith linear masks and circle distribution characteristic. Firstly,this scheme preprocessed the acquired FPC image,divided the trace into several sub-regions and obtained the line w idth values of each trace transverse section. Then the line w idth sequences w ere searched w ith the linear difference template of gray scale. Thus,the sunken defects alternative positions w ere located. Lastly,the circle distribution characteristic is defined to identify the real defect areas from the alternative regions acquired from the previous step. Thus,the detection of sunken defects on the FPC trace w as accomplished.The algorithm w as tested in the self-built image database,w hich show s the better detection performance than the other typical algorithms.
