The effect of deep cryogenic treatment on the microstructure, hardness, and wear behavior of D2 tool steel was studied by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffracti...The effect of deep cryogenic treatment on the microstructure, hardness, and wear behavior of D2 tool steel was studied by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), hardness test, pin-on-disk wear test, and the reciprocating pin-on-fiat wear test. The results show that deep cryogenic treatment eliminates retained austenite, makes a better carbide distribution, and increases the carbide content. Furthermore, some new nano-sized carbides form during the deep cryogenic treatment, thereby increasing the hardness and improving the wear behavior of the samples.展开更多
The effect of deep cryogenic treatment on the mechanical properties of 80CrMo 12 5 tool steel was investigated. Moreover, the effects of stabilization (holding at room temperature for some periods before deep cryogen...The effect of deep cryogenic treatment on the mechanical properties of 80CrMo 12 5 tool steel was investigated. Moreover, the effects of stabilization (holding at room temperature for some periods before deep cryogenic treatment) and tempering before deep cryogenic treatment were studied. The results show that deep cryogenic treatment can eliminate the retained austenite, making a better carbide distribu- tion and a higher carbide amount. As a result, a remarkable improvement in wear resistance of cryogenically treated specimens is observed. Moreover, the ultimate tensile strength increases, and the toughness of the sample decreases. It is also found that both stabilization and tem- pering before deep cryogenic treatment decrease the wear resistance, hardness, and carbides homogeneity compared to the deep cryogeni- cally treated samples. It is concluded that deep cryogenic treatment should be performed without any delay on samples after quenching to reach the highest wear resistance and hardness.展开更多
Deep cryogenic treatment (DCT) is one of the most recent processes being used to treat tool steels. It is a supplementary treatment where components are treated below subzero temperatures for several cryo-soaking hour...Deep cryogenic treatment (DCT) is one of the most recent processes being used to treat tool steels. It is a supplementary treatment where components are treated below subzero temperatures for several cryo-soaking hours. This paper focuses on to study the effect of deep cryogenic treatment on Thermo mechanical properties of AISI H-13 tool steel. Deep cryogenic treatment at 32 hours of cryo-soaking time is applied and thermo mechanical performance of tool steel was analyzed by using pin on disk high temperature wear testing and stress rupture testings. The microstructural evolutions during DCT were evaluated by using scanning electron microscope (SEM). It was observed that microstructural modifications like increase in carbide density, fine and uniform martensitic structure during DCT had significantly improved properties.展开更多
A surface engineering approach for a novel pre-treatment of hard metal tool substrate for optimum adhesion of diamond coatings is presented. Firsfly, an alkaline solution was used to etch the WC grains to generate a r...A surface engineering approach for a novel pre-treatment of hard metal tool substrate for optimum adhesion of diamond coatings is presented. Firsfly, an alkaline solution was used to etch the WC grains to generate a rough surface for better mechanical interlocking. Subsequently, surface Co was removed by etching in acid solution. Then the hard metal substrate was boronized to form a compound interlayer which acted as an efficient diffusion barrier to prevent the outward diffusion of Co. Novel nano-microcrystalline composite diamond film coatings with a very smooth surface was deposited on the surface engineering pre-treated hard metal surface. Promising results of measurement in adhesion strength as well as field cutting tests have been obtained.展开更多
The main objective of the die heat treatment is to enhance the surface hardness and wear properties to extend the die service life. In this paper, a series of heat treatment experiments were conducted under different ...The main objective of the die heat treatment is to enhance the surface hardness and wear properties to extend the die service life. In this paper, a series of heat treatment experiments were conducted under different atmospheric conditions and length of treatment. Four austenitization atmospheric conditions were studied and although each heat treatment condition resulted in a different hardness profile, it did not affect the results for gas nitriding. All samples subjected to the nitriding process produced similar thicknesses of hardened case layer with average hardness of 70 - 72 HRC if the initial carbon content is not too low. It was shown that heat treatment without atmospheric control results in a lower hardness on the surface since the material was subjected to decarburization effect. The stainless steel foil wrapping around the sample and heat treatment in a vacuum furnace could restrict the decarburization process, while pack carburization heat treatment resulted in a carburization effect on the material.展开更多
目的了解肿瘤多学科协作诊疗(multidisciplinary diagnosis and treatment,MDT)的有效性评价研究,分析国内外有效性评价工具的发展现状以及差异,为后续肿瘤MDT的总结评价和持续改进、强化MDT监管提供借鉴与参考。方法检索国内外4个文献...目的了解肿瘤多学科协作诊疗(multidisciplinary diagnosis and treatment,MDT)的有效性评价研究,分析国内外有效性评价工具的发展现状以及差异,为后续肿瘤MDT的总结评价和持续改进、强化MDT监管提供借鉴与参考。方法检索国内外4个文献数据库以获取相关研究文献,并进行文献筛选和系统综述。结果最终纳入文献87篇,中文和英文文献分别为26篇和61篇,发表数量最多的年份是2020年,第一作者所属国家主要为英国。国外评价工具侧重于结构和过程的关键要素,国内评价体系侧重于结果层面的指标内容。结论在国内研究中,MDT评价指标选择的科学性和全面性有待提升,对MDT结构、过程层面的影响因素分析尚需加强,现有评价体系的外推性仍待验证。建议强化评价指标选择的证据支持,重视过程环节的评价,促进对肿瘤MDT影响因素的深入研究,进一步鼓励现有评价体系的实证应用。展开更多
背景失眠障碍是一种常见的精神疾病,给患者的生活和健康带来严重的负面影响。传统的认知行为疗法(CBT-I)是一种有效的非药物治疗方法,但其操作复杂、耗时长、依从性低等缺点限制了其在真实世界的应用。简版行为疗法(BBT-I)是一种基于CB...背景失眠障碍是一种常见的精神疾病,给患者的生活和健康带来严重的负面影响。传统的认知行为疗法(CBT-I)是一种有效的非药物治疗方法,但其操作复杂、耗时长、依从性低等缺点限制了其在真实世界的应用。简版行为疗法(BBT-I)是一种基于CBT-I的简化治疗方法,其疗效与CBT-I相当,更适合在真实世界中推广。然而,BBT-I是否适用于中国失眠障碍人群暂不明确,而通过线上方式进行BBT-I的研究更是缺乏。目的本研究旨在探讨通过微信小程序进行的在线BBT-I(eBBT-I)对中国失眠障碍患者失眠改善的疗效,以及其对患者睡眠信念和态度的影响。方法本研究采用前瞻性非随机对照研究的设计,将2023年2—11月来自暨南大学附属第一医院精神医学科睡眠门诊的失眠障碍患者设为干预组,将线上和线下招募的失眠障碍志愿者设为对照组,干预组接受为期2周的eBBT-I治疗,对照组接受精神卫生教育的伪干预。在干预前后分别测量患者的失眠严重程度指数量表(ISI)和简版睡眠信念与态度问卷(DBAS-16)得分,以评估干预效果。结果研究最终共纳入35例干预组患者和30例对照组患者。主要结局指标:组别与时间对ISI得分存在交互作用(P<0.05);组别与时间分别对ISI得分主效应显著(P<0.05)。干预前3d(基线)两组ISI得分比较,差异无统计学意义(P>0.05);干预后14d干预组ISI得分低于对照组(P<0.05);干预组干预后14 d ISI得分低于组内干预前(P<0.05)。次要结局指标:组别与时间对DBAS-16得分不存在交互作用(P>0.05);时间对DBAS-16得分主效应显著(P<0.05);组别对DBAS-16得分主效应不显著(P>0.05)。干预前3 d(基线)、干预后14 d两组DBAS-16得分比较,差异无统计学意义(P>0.05);干预组干预后14 d DBAS-16得分高于组内干预前(P<0.05)。结论eBBT-I有效地改善了失眠障碍患者的失眠症状和负面影响,但对睡眠信念与态度的改善效果仍有待提升。本研究支持了eBBT-I在中国失眠障碍患者失眠治疗中的可行性和有效性。展开更多
The present work is to characterize both processes of thermochemical treatments: plasma nitriding and gas. The tests were carried out in collaboration with the Franco-Tunisian heat treatment (F3T) applied to a widely ...The present work is to characterize both processes of thermochemical treatments: plasma nitriding and gas. The tests were carried out in collaboration with the Franco-Tunisian heat treatment (F3T) applied to a widely used steel in industrial production as a tool for hot work on X38CrMoV5 (AISI H13). The material underwent a first cycle of hardening heat treatment at 1030℃ followed by two successive incomes at 550℃ and 590℃. After nitriding (ion and gas), the quantification of wear was performed in the laboratory of tribology at SUPMECA (St. Ouen). After defining the test conditions on the alternative tribometer ensuring on one hand a quantitatively sufficient wear and avoiding on the other hand, the phenomenon of jamming. The conditions chosen are: 58.8 N load, frequency 0.5 Hz, friction coefficient μ = 0.5. The wear tracks were scanned using the profilometer Talysurf 5 M type, which allowed us to assess the volume used and the wear rate. Moreover, these tracks were characterized by metallography. What emerges from this work is that the control parameters of ion nitriding ensures a better depth of treatment for the same holding time with a total absence of the white layer known for chipping and fragility.展开更多
文摘The effect of deep cryogenic treatment on the microstructure, hardness, and wear behavior of D2 tool steel was studied by scanning electron microscopy (SEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), hardness test, pin-on-disk wear test, and the reciprocating pin-on-fiat wear test. The results show that deep cryogenic treatment eliminates retained austenite, makes a better carbide distribution, and increases the carbide content. Furthermore, some new nano-sized carbides form during the deep cryogenic treatment, thereby increasing the hardness and improving the wear behavior of the samples.
文摘The effect of deep cryogenic treatment on the mechanical properties of 80CrMo 12 5 tool steel was investigated. Moreover, the effects of stabilization (holding at room temperature for some periods before deep cryogenic treatment) and tempering before deep cryogenic treatment were studied. The results show that deep cryogenic treatment can eliminate the retained austenite, making a better carbide distribu- tion and a higher carbide amount. As a result, a remarkable improvement in wear resistance of cryogenically treated specimens is observed. Moreover, the ultimate tensile strength increases, and the toughness of the sample decreases. It is also found that both stabilization and tem- pering before deep cryogenic treatment decrease the wear resistance, hardness, and carbides homogeneity compared to the deep cryogeni- cally treated samples. It is concluded that deep cryogenic treatment should be performed without any delay on samples after quenching to reach the highest wear resistance and hardness.
文摘Deep cryogenic treatment (DCT) is one of the most recent processes being used to treat tool steels. It is a supplementary treatment where components are treated below subzero temperatures for several cryo-soaking hours. This paper focuses on to study the effect of deep cryogenic treatment on Thermo mechanical properties of AISI H-13 tool steel. Deep cryogenic treatment at 32 hours of cryo-soaking time is applied and thermo mechanical performance of tool steel was analyzed by using pin on disk high temperature wear testing and stress rupture testings. The microstructural evolutions during DCT were evaluated by using scanning electron microscope (SEM). It was observed that microstructural modifications like increase in carbide density, fine and uniform martensitic structure during DCT had significantly improved properties.
文摘A surface engineering approach for a novel pre-treatment of hard metal tool substrate for optimum adhesion of diamond coatings is presented. Firsfly, an alkaline solution was used to etch the WC grains to generate a rough surface for better mechanical interlocking. Subsequently, surface Co was removed by etching in acid solution. Then the hard metal substrate was boronized to form a compound interlayer which acted as an efficient diffusion barrier to prevent the outward diffusion of Co. Novel nano-microcrystalline composite diamond film coatings with a very smooth surface was deposited on the surface engineering pre-treated hard metal surface. Promising results of measurement in adhesion strength as well as field cutting tests have been obtained.
文摘The main objective of the die heat treatment is to enhance the surface hardness and wear properties to extend the die service life. In this paper, a series of heat treatment experiments were conducted under different atmospheric conditions and length of treatment. Four austenitization atmospheric conditions were studied and although each heat treatment condition resulted in a different hardness profile, it did not affect the results for gas nitriding. All samples subjected to the nitriding process produced similar thicknesses of hardened case layer with average hardness of 70 - 72 HRC if the initial carbon content is not too low. It was shown that heat treatment without atmospheric control results in a lower hardness on the surface since the material was subjected to decarburization effect. The stainless steel foil wrapping around the sample and heat treatment in a vacuum furnace could restrict the decarburization process, while pack carburization heat treatment resulted in a carburization effect on the material.
文摘目的了解肿瘤多学科协作诊疗(multidisciplinary diagnosis and treatment,MDT)的有效性评价研究,分析国内外有效性评价工具的发展现状以及差异,为后续肿瘤MDT的总结评价和持续改进、强化MDT监管提供借鉴与参考。方法检索国内外4个文献数据库以获取相关研究文献,并进行文献筛选和系统综述。结果最终纳入文献87篇,中文和英文文献分别为26篇和61篇,发表数量最多的年份是2020年,第一作者所属国家主要为英国。国外评价工具侧重于结构和过程的关键要素,国内评价体系侧重于结果层面的指标内容。结论在国内研究中,MDT评价指标选择的科学性和全面性有待提升,对MDT结构、过程层面的影响因素分析尚需加强,现有评价体系的外推性仍待验证。建议强化评价指标选择的证据支持,重视过程环节的评价,促进对肿瘤MDT影响因素的深入研究,进一步鼓励现有评价体系的实证应用。
文摘背景失眠障碍是一种常见的精神疾病,给患者的生活和健康带来严重的负面影响。传统的认知行为疗法(CBT-I)是一种有效的非药物治疗方法,但其操作复杂、耗时长、依从性低等缺点限制了其在真实世界的应用。简版行为疗法(BBT-I)是一种基于CBT-I的简化治疗方法,其疗效与CBT-I相当,更适合在真实世界中推广。然而,BBT-I是否适用于中国失眠障碍人群暂不明确,而通过线上方式进行BBT-I的研究更是缺乏。目的本研究旨在探讨通过微信小程序进行的在线BBT-I(eBBT-I)对中国失眠障碍患者失眠改善的疗效,以及其对患者睡眠信念和态度的影响。方法本研究采用前瞻性非随机对照研究的设计,将2023年2—11月来自暨南大学附属第一医院精神医学科睡眠门诊的失眠障碍患者设为干预组,将线上和线下招募的失眠障碍志愿者设为对照组,干预组接受为期2周的eBBT-I治疗,对照组接受精神卫生教育的伪干预。在干预前后分别测量患者的失眠严重程度指数量表(ISI)和简版睡眠信念与态度问卷(DBAS-16)得分,以评估干预效果。结果研究最终共纳入35例干预组患者和30例对照组患者。主要结局指标:组别与时间对ISI得分存在交互作用(P<0.05);组别与时间分别对ISI得分主效应显著(P<0.05)。干预前3d(基线)两组ISI得分比较,差异无统计学意义(P>0.05);干预后14d干预组ISI得分低于对照组(P<0.05);干预组干预后14 d ISI得分低于组内干预前(P<0.05)。次要结局指标:组别与时间对DBAS-16得分不存在交互作用(P>0.05);时间对DBAS-16得分主效应显著(P<0.05);组别对DBAS-16得分主效应不显著(P>0.05)。干预前3 d(基线)、干预后14 d两组DBAS-16得分比较,差异无统计学意义(P>0.05);干预组干预后14 d DBAS-16得分高于组内干预前(P<0.05)。结论eBBT-I有效地改善了失眠障碍患者的失眠症状和负面影响,但对睡眠信念与态度的改善效果仍有待提升。本研究支持了eBBT-I在中国失眠障碍患者失眠治疗中的可行性和有效性。
文摘The present work is to characterize both processes of thermochemical treatments: plasma nitriding and gas. The tests were carried out in collaboration with the Franco-Tunisian heat treatment (F3T) applied to a widely used steel in industrial production as a tool for hot work on X38CrMoV5 (AISI H13). The material underwent a first cycle of hardening heat treatment at 1030℃ followed by two successive incomes at 550℃ and 590℃. After nitriding (ion and gas), the quantification of wear was performed in the laboratory of tribology at SUPMECA (St. Ouen). After defining the test conditions on the alternative tribometer ensuring on one hand a quantitatively sufficient wear and avoiding on the other hand, the phenomenon of jamming. The conditions chosen are: 58.8 N load, frequency 0.5 Hz, friction coefficient μ = 0.5. The wear tracks were scanned using the profilometer Talysurf 5 M type, which allowed us to assess the volume used and the wear rate. Moreover, these tracks were characterized by metallography. What emerges from this work is that the control parameters of ion nitriding ensures a better depth of treatment for the same holding time with a total absence of the white layer known for chipping and fragility.