The crystal structure of the title compound, C_34H_29GeN_3S, has been determined by single-crystal X-ray diffraction at 299 (±1)K. The crystal is trichlnic with space group P1, a=9. 772(3), b= 11. 643(3), c= 13. ...The crystal structure of the title compound, C_34H_29GeN_3S, has been determined by single-crystal X-ray diffraction at 299 (±1)K. The crystal is trichlnic with space group P1, a=9. 772(3), b= 11. 643(3), c= 13. 960(3) A . α=66. 55(2),β=83. 49(2),γ=88. 49(2)°, Z=2, V= 1440. 0(8) A￣3, M_r=584. 28, F(000) =604, μ(MoKα) = 11. 44 cm￣-1. D_c= l. 349 g/cm￣-3. The final R factor is 0. 058, and R_w is 0. 068. The result of X-ray analysis indicates that the heterocycle of the title compound appears as a triazoline instead of a triazole.展开更多
文摘The crystal structure of the title compound, C_34H_29GeN_3S, has been determined by single-crystal X-ray diffraction at 299 (±1)K. The crystal is trichlnic with space group P1, a=9. 772(3), b= 11. 643(3), c= 13. 960(3) A . α=66. 55(2),β=83. 49(2),γ=88. 49(2)°, Z=2, V= 1440. 0(8) A￣3, M_r=584. 28, F(000) =604, μ(MoKα) = 11. 44 cm￣-1. D_c= l. 349 g/cm￣-3. The final R factor is 0. 058, and R_w is 0. 068. The result of X-ray analysis indicates that the heterocycle of the title compound appears as a triazoline instead of a triazole.
