The microstructure and properties of the 93W-4Ni-2Co-1Fe(mass fraction,%) tungsten heavy alloys prepared by mechanical alloying and electric current activated sintering from mixed elemental powders were investigated.A...The microstructure and properties of the 93W-4Ni-2Co-1Fe(mass fraction,%) tungsten heavy alloys prepared by mechanical alloying and electric current activated sintering from mixed elemental powders were investigated.After 15 h milling,the average W grain size in the powders is decreased to 120 nm.For the powders milled for 15 h,the density,hardness and transverse rupture strength of the alloys sintered only by an intensive pulse electric current are the maximum.When the total sintering time keeps constant,the properties of the sintered alloys can be obviously improved by optimizing the sintering time of pulse-and constant-currents.A bulk ultrafine alloy with an average W grain size of about 340 nm can be obtained by sintering 15 h-milled powders in a total sintering time of 6 min.The corresponding sintered density,hardness and transverse rupture strength reach 16.78 g /cm3,HRA84.3 and 968 MPa,respectively.展开更多
基金Project(51074187)supported by National Natural Science Foundation of ChinaProject(50925416)supported by National Natural Science Funds for Distinguished Young ScholarsProject(51021063)supported by Creative Research Group of National Nature Science Foundation of China
基金Project(2007CB616905) supported by the National Basic Research Program of ChinaProject(2007AA03Z112) supported by the National High-tech Research and Development Program of China+1 种基金Project(x2jqB6080210) supported by the Natural Science Foundation of Guangdong Province,ChinaProject(9140A18040709JW1601) supported by the Advanced Research Fund of Department of Defense,China
文摘The microstructure and properties of the 93W-4Ni-2Co-1Fe(mass fraction,%) tungsten heavy alloys prepared by mechanical alloying and electric current activated sintering from mixed elemental powders were investigated.After 15 h milling,the average W grain size in the powders is decreased to 120 nm.For the powders milled for 15 h,the density,hardness and transverse rupture strength of the alloys sintered only by an intensive pulse electric current are the maximum.When the total sintering time keeps constant,the properties of the sintered alloys can be obviously improved by optimizing the sintering time of pulse-and constant-currents.A bulk ultrafine alloy with an average W grain size of about 340 nm can be obtained by sintering 15 h-milled powders in a total sintering time of 6 min.The corresponding sintered density,hardness and transverse rupture strength reach 16.78 g /cm3,HRA84.3 and 968 MPa,respectively.
