Two multi-step (two-step and three-step) slow shot speeds were used in the vacuum die casting process of AZ91D magnesium alloy. The vacuum pressure variation in the die cavity before mold filling was monitored by us...Two multi-step (two-step and three-step) slow shot speeds were used in the vacuum die casting process of AZ91D magnesium alloy. The vacuum pressure variation in the die cavity before mold filling was monitored by using a pressure sensor. The microstructures of the produced castings were analyzed with optical microscope and image analysis software. The experimental results demonstrate that, the vacuum pressure in the die cavity at the beginning of mold filling is significantly reduced by using three-step slow shot speed, resulting in a low gas porosity level in the produced castings. At an appropriate multi-step slow shot speed, the dwell time of the liquid metal in the shot sleeve before mold filling can be reduced and the flow of the liquid metal in the shot sleeve at the later stage of the slow shot process can be restrained, which cause a low externally solidified crystal content in the produced castings.展开更多
Vacuum die casting is the optimal method to produce high quality aluminum alloy components.At present,there are still very few systematic studies on vacuum die casting theory and equipment design.On the basis of the e...Vacuum die casting is the optimal method to produce high quality aluminum alloy components.At present,there are still very few systematic studies on vacuum die casting theory and equipment design.On the basis of the existing theories of the vacuum die casting pumping and venting systems,a simplified model is established in this research.The model has an aggregate unit consisted of "vacuum pump + buffer tank" and a cylindrical container(including the shot sleeve,cavity and exhaust channel).The theoretical analysis is carried out between the cavity pressure and the pumping time under different volume models.An auxiliary system for high vacuum die casting is designed based on the above analysis.This system is composed of a vacuum control machine and a new vacuum stop valve.The machine has a human-computer control mode with "programmable logic controller(PLC) + touch screen" and a real-time monitoring function of vacuum degree for buffer tank and die cavity.The vacuum stop valve with the "compressed gas + piston rod + labyrinth groove" structure can realize the function of whole-process vacuum venting.The new system shows great advantages on vacuuming the cavity with a much faster speed by making tests on an existing die casting mold and a 250 t die casting machine.A die cavity pressure less than 10 kPa can be reached within 0.8 s in the experiment and the porosity of castings can be greatly decreased.The systematic studies on vacuum die casting theory and equipment have a great guiding significance for high vacuum die casting,and can also be applied to other high vacuum forming in related theoretical and practical research.展开更多
High pressure die casting copper is used to produce rotors for induction motors to improve efficiency.Experiments were carried out for a special"step-shape"casting with different step thicknesses.Based on th...High pressure die casting copper is used to produce rotors for induction motors to improve efficiency.Experiments were carried out for a special"step-shape"casting with different step thicknesses.Based on the measured temperature inside the die,the interfacial heat transfer coefficient(IHTC)at the metal/die interface during vacuum die casting was evaluated by solving the inverse problem.The IHTC peak value was 4.5×10^3-11×10^3 W·m^-2·K^-1 under the basic operation condition.The influences of casting pressure,fast shot speed,pouring temperature and initial die surface temperature on the IHTC peak values were investigated.Results show that a greater casting pressure and faster shot speed could only increase the IHTC peak values at the location close to the ingate.An increase of pouring temperature and/or initial die surface temperature significantly increases the IHTC peak values.展开更多
The purpose of this study was to prepare high-quality Al-Si-Mg-Mn alloy with a good combination of strength and ductility employing the vacuum-assisted high-pressure die cast process. An orthogonal study of heat treat...The purpose of this study was to prepare high-quality Al-Si-Mg-Mn alloy with a good combination of strength and ductility employing the vacuum-assisted high-pressure die cast process. An orthogonal study of heat treatments was conducted to design an optimized T6 heat treatment process for both Al-10%Si-0.3%Mg-Mn and Al-11%Si-0.6%Mg-Mn alloys. The results demonstrate that no obvious blisters and warpage were observed in these two alloys with solid solution treatment. After the optimal T6 heat treatment of 530°C×3 h + 165°C×6 h, Al-11%Si-0.6%Mg-Mn alloy has better mechanical properties, of which tensile strength, yield strength and elongation reached 377.3 MPa, 307.8 MPa and 9%, respectively. The improvement of mechanical properties can be attributed to the high density of needle-like β″(Mg_5Si_6) precipitation after aging treatment and the fine and spherical eutectic Si particles uniformly distributed in the α-Al matrix.展开更多
The effects of vacuum assistance on the microstructure and mechanical properties of high-pressure die cast AZ91 D alloy at different slow shot speeds were evaluated. Plate-shaped castings of AZ91 D alloy were carried ...The effects of vacuum assistance on the microstructure and mechanical properties of high-pressure die cast AZ91 D alloy at different slow shot speeds were evaluated. Plate-shaped castings of AZ91 D alloy were carried out on a TOYO BD-350V5 cold chamber die casting machine incorporated with a self-improved TOYO vacuum system. It was found that the vacuum pressure in the die cavity at the beginning of mold filling increases with the increase of slow shot speed, following a cubic polynomial curve, resulting in a decline in the porosity-reduction ability of vacuum assistance with the increase of slow shot speed. The externally solidified crystal(ESC) contents in conventional and vacuum die castings behave similar against the slow shot speed. The tensile properties of vacuum die castings were strongly influenced by the ESC content at relative low slow shot speeds. With the increase of slow shot speed, the influence of the gas porosity level in vacuum die castings would get prominent.展开更多
The effects of vacuum assistance on the microstructure and mechanical properties of high pressure die cast A390alloy at different slow shot speeds were evaluated.Plate-shaped specimens of hypereutectic A390aluminum al...The effects of vacuum assistance on the microstructure and mechanical properties of high pressure die cast A390alloy at different slow shot speeds were evaluated.Plate-shaped specimens of hypereutectic A390aluminum alloy were produced on a TOYO BD?350V5cold chamber die casting machine incorporated with a self-improved TOYO vacuum system.According to the results,the vacuum pressure inside the die cavity increased linearly with the increasing slow shot speed at the beginning of mold filling.Meanwhile,tensile properties of vacuum die castings were deteriorated by the porosity content.In addition,the average primary silicon size decreased from23to14μm when the slow shot speed increased from0.05to0.2m/s,which has a binary functional relationship with the slow shot speed.After heat treatment,microstructural morphologies revealed that needle-shaped and thin-flaked eutectic silicon particles became rounded while Al2Cu dissolved intoα(Al)matrix.Furthermore,the fractography revealed that the fracture mechanism has evolved from brittle transgranular fracture to a fracture mode with many dimples after heat treatment.展开更多
Pure copper tensile bars were produced by conventional die casting(HPDC) and vacuum-assist die casting(VADC) processes. Porosity and mechanical properties were investigated by using optical microscopy(OM), scanning el...Pure copper tensile bars were produced by conventional die casting(HPDC) and vacuum-assist die casting(VADC) processes. Porosity and mechanical properties were investigated by using optical microscopy(OM), scanning electron microscopy(SEM), energy dispersive spectroscopy(EDS), X-ray computed tomography(XCT) and tensile tester. Results show that porosities including gas porosity and shrinkage porosity could be observed in copper castings. Since the application of vacuum could reduce filling related gas entrapment and facilitate solidification due to the increased heat transfer between metal and die, both number and size of the entrapped gases, as well as shrinkage porosities were significantly reduced in vacuum-assist die castings of pure copper. The porosity fraction decreased from 2.243% to 0.875% compared with that of the conventional die casting. Besides, mechanical properties were improved significantly, i.e., by 15% for ultimate tensile strength and three times for elongation.展开更多
When diecasting large and thin Mg alloy parts,material defects occur,which include porosity,nonuniform mechanical properties,irregular surfaces,and incomplete filling.To resolve these problems,it is necessary to have ...When diecasting large and thin Mg alloy parts,material defects occur,which include porosity,nonuniform mechanical properties,irregular surfaces,and incomplete filling.To resolve these problems,it is necessary to have uniform injection velocities and temperatures as well as control the melt.This study investigated the feasibility of producing large and thin components using a die caster by attaching a high vacuum system.In particular,the effects of injection velocity on surface quality and the mechanical properties of the products were investigated.Hence,an injection velocity scheme and a die structure capable of casting in a vacuum were proposed.As a result,it was found that the critical low injection velocity was 0.2 m/s to produce large thin Mg alloy structures having good mechanical properties.展开更多
Vacuum die casting can reduce the'air entrapment'phenomenon during casting process.Based on the temperature measurements at metal-die interface with different processing parameters,such as slow shot speed(VL),...Vacuum die casting can reduce the'air entrapment'phenomenon during casting process.Based on the temperature measurements at metal-die interface with different processing parameters,such as slow shot speed(VL),high shot speed(VH),pouring temperature(Tp)and initial die temperature(Tm),inverse method was developed to determine the interfacial heat transfer coefficient(IHTC).The results indicate that a closer contact between the casting and die could be achieved when the vacuum system is used.It is found that the vacuum could strongly increase the values of IHTC and decrease the grain size in castings.The IHTC could have a higher peak value with increasing the Tp from680to720℃or the VL from0.1to0.4m/s.In addition,the influence of the VH and Tm on IHTC could be negligible.展开更多
The glass-forming ability and mechanical properties of metallic glasses and their composites are well known to be sensitive to the preparation conditions and are highly deteriorated by industrial preparing conditions ...The glass-forming ability and mechanical properties of metallic glasses and their composites are well known to be sensitive to the preparation conditions and are highly deteriorated by industrial preparing conditions such as low-purity raw materials and low vacuum.Here,we showed that a series of in-situ bulk metallic glass composites(BMGCs)which exhibit excellent ductility and segmental work hardening were successfully developed utilizing a high vacuum high-pressure die casting(HV-HPDC)technology along with industrial-grade raw materials.The tensile properties of these BMGCs are systematically investigated and correlated with the alloy microstructure.As compared with the copper mold suction casting method,the volume fraction difference of the dendrite phase for the BMGCs with the same composition is not significant when fabricated by the HV-HPDC,whereas the size of theβ-phase is generally larger.Insitu BMGCs with the composition of Ti_(48)Zr_(20)(V_(12/17)Cu_(5/17))19 Be 13 obtained by the HV-HPDC process show ductility up to 11.3%under tension at room temperature and exhibit a certain amount of work hardening.Two conditions need to be met to enable the BMGCs,which are prepared by vacuum die-casting to retain favorable ductility:(1)The volume fraction ofβphase stays below 62%±2%;(2)The equiaxed crystals with a more uniform size in the range of 5-10μm.Meanwhile,the results of the present study provided guidance for developing BMGCs with good ductile properties under industrial conditions.展开更多
基金Project(51275269)supported by the National Natural Science Foundation of ChinaProject(20121087918)supported by the Independent Research Program,China+1 种基金Project(2012ZX04012011)supported by the National Science and Technology Major Project of the Ministry of Science and Technology of ChinaProject(2013M540936)supported by Postdoctoral Science Foundation of China
文摘Two multi-step (two-step and three-step) slow shot speeds were used in the vacuum die casting process of AZ91D magnesium alloy. The vacuum pressure variation in the die cavity before mold filling was monitored by using a pressure sensor. The microstructures of the produced castings were analyzed with optical microscope and image analysis software. The experimental results demonstrate that, the vacuum pressure in the die cavity at the beginning of mold filling is significantly reduced by using three-step slow shot speed, resulting in a low gas porosity level in the produced castings. At an appropriate multi-step slow shot speed, the dwell time of the liquid metal in the shot sleeve before mold filling can be reduced and the flow of the liquid metal in the shot sleeve at the later stage of the slow shot process can be restrained, which cause a low externally solidified crystal content in the produced castings.
基金supported by Fujian Provincial Natural Science Foundation of China (Grant No.2007J0170)Xiamen Municipal Natural Science Foundation of China (Grant No.3502Z20093034)
文摘Vacuum die casting is the optimal method to produce high quality aluminum alloy components.At present,there are still very few systematic studies on vacuum die casting theory and equipment design.On the basis of the existing theories of the vacuum die casting pumping and venting systems,a simplified model is established in this research.The model has an aggregate unit consisted of "vacuum pump + buffer tank" and a cylindrical container(including the shot sleeve,cavity and exhaust channel).The theoretical analysis is carried out between the cavity pressure and the pumping time under different volume models.An auxiliary system for high vacuum die casting is designed based on the above analysis.This system is composed of a vacuum control machine and a new vacuum stop valve.The machine has a human-computer control mode with "programmable logic controller(PLC) + touch screen" and a real-time monitoring function of vacuum degree for buffer tank and die cavity.The vacuum stop valve with the "compressed gas + piston rod + labyrinth groove" structure can realize the function of whole-process vacuum venting.The new system shows great advantages on vacuuming the cavity with a much faster speed by making tests on an existing die casting mold and a 250 t die casting machine.A die cavity pressure less than 10 kPa can be reached within 0.8 s in the experiment and the porosity of castings can be greatly decreased.The systematic studies on vacuum die casting theory and equipment have a great guiding significance for high vacuum die casting,and can also be applied to other high vacuum forming in related theoretical and practical research.
文摘High pressure die casting copper is used to produce rotors for induction motors to improve efficiency.Experiments were carried out for a special"step-shape"casting with different step thicknesses.Based on the measured temperature inside the die,the interfacial heat transfer coefficient(IHTC)at the metal/die interface during vacuum die casting was evaluated by solving the inverse problem.The IHTC peak value was 4.5×10^3-11×10^3 W·m^-2·K^-1 under the basic operation condition.The influences of casting pressure,fast shot speed,pouring temperature and initial die surface temperature on the IHTC peak values were investigated.Results show that a greater casting pressure and faster shot speed could only increase the IHTC peak values at the location close to the ingate.An increase of pouring temperature and/or initial die surface temperature significantly increases the IHTC peak values.
基金financially supported by the Jiangsu province transformation of scientific and technological achievements program(BA2015041)the Jiangsu key laboratory for advanced metallic materials(BM2007204)
文摘The purpose of this study was to prepare high-quality Al-Si-Mg-Mn alloy with a good combination of strength and ductility employing the vacuum-assisted high-pressure die cast process. An orthogonal study of heat treatments was conducted to design an optimized T6 heat treatment process for both Al-10%Si-0.3%Mg-Mn and Al-11%Si-0.6%Mg-Mn alloys. The results demonstrate that no obvious blisters and warpage were observed in these two alloys with solid solution treatment. After the optimal T6 heat treatment of 530°C×3 h + 165°C×6 h, Al-11%Si-0.6%Mg-Mn alloy has better mechanical properties, of which tensile strength, yield strength and elongation reached 377.3 MPa, 307.8 MPa and 9%, respectively. The improvement of mechanical properties can be attributed to the high density of needle-like β″(Mg_5Si_6) precipitation after aging treatment and the fine and spherical eutectic Si particles uniformly distributed in the α-Al matrix.
基金Project(2012ZX04012011)supported by the National Science and Technology Major Project of the Ministry of Science and Technology of ChinaProject(2011BAE22B02)supported by the National Key Technologies R&D Program of ChinaProject(51275269)supported by the National Natural Science Foundation of China
文摘The effects of vacuum assistance on the microstructure and mechanical properties of high-pressure die cast AZ91 D alloy at different slow shot speeds were evaluated. Plate-shaped castings of AZ91 D alloy were carried out on a TOYO BD-350V5 cold chamber die casting machine incorporated with a self-improved TOYO vacuum system. It was found that the vacuum pressure in the die cavity at the beginning of mold filling increases with the increase of slow shot speed, following a cubic polynomial curve, resulting in a decline in the porosity-reduction ability of vacuum assistance with the increase of slow shot speed. The externally solidified crystal(ESC) contents in conventional and vacuum die castings behave similar against the slow shot speed. The tensile properties of vacuum die castings were strongly influenced by the ESC content at relative low slow shot speeds. With the increase of slow shot speed, the influence of the gas porosity level in vacuum die castings would get prominent.
基金Project(51775297)supported by the National Natural Science Foundation of ChinaProject(2015M580093)supported by the China Postdoctoral Science Foundation
文摘The effects of vacuum assistance on the microstructure and mechanical properties of high pressure die cast A390alloy at different slow shot speeds were evaluated.Plate-shaped specimens of hypereutectic A390aluminum alloy were produced on a TOYO BD?350V5cold chamber die casting machine incorporated with a self-improved TOYO vacuum system.According to the results,the vacuum pressure inside the die cavity increased linearly with the increasing slow shot speed at the beginning of mold filling.Meanwhile,tensile properties of vacuum die castings were deteriorated by the porosity content.In addition,the average primary silicon size decreased from23to14μm when the slow shot speed increased from0.05to0.2m/s,which has a binary functional relationship with the slow shot speed.After heat treatment,microstructural morphologies revealed that needle-shaped and thin-flaked eutectic silicon particles became rounded while Al2Cu dissolved intoα(Al)matrix.Furthermore,the fractography revealed that the fracture mechanism has evolved from brittle transgranular fracture to a fracture mode with many dimples after heat treatment.
文摘Pure copper tensile bars were produced by conventional die casting(HPDC) and vacuum-assist die casting(VADC) processes. Porosity and mechanical properties were investigated by using optical microscopy(OM), scanning electron microscopy(SEM), energy dispersive spectroscopy(EDS), X-ray computed tomography(XCT) and tensile tester. Results show that porosities including gas porosity and shrinkage porosity could be observed in copper castings. Since the application of vacuum could reduce filling related gas entrapment and facilitate solidification due to the increased heat transfer between metal and die, both number and size of the entrapped gases, as well as shrinkage porosities were significantly reduced in vacuum-assist die castings of pure copper. The porosity fraction decreased from 2.243% to 0.875% compared with that of the conventional die casting. Besides, mechanical properties were improved significantly, i.e., by 15% for ultimate tensile strength and three times for elongation.
基金Acknowledgement This work was supported by the National Core Research Center Program from MOST/KOSEF (No. R15- 2006-022-02001-0).
文摘When diecasting large and thin Mg alloy parts,material defects occur,which include porosity,nonuniform mechanical properties,irregular surfaces,and incomplete filling.To resolve these problems,it is necessary to have uniform injection velocities and temperatures as well as control the melt.This study investigated the feasibility of producing large and thin components using a die caster by attaching a high vacuum system.In particular,the effects of injection velocity on surface quality and the mechanical properties of the products were investigated.Hence,an injection velocity scheme and a die structure capable of casting in a vacuum were proposed.As a result,it was found that the critical low injection velocity was 0.2 m/s to produce large thin Mg alloy structures having good mechanical properties.
基金Project (2016YFB0301001) supported by the National Key Research and Development Program of ChinaProject (2015M580093) supported by the General Financial Grant from the China Postdoctoral Science Foundation of China
文摘Vacuum die casting can reduce the'air entrapment'phenomenon during casting process.Based on the temperature measurements at metal-die interface with different processing parameters,such as slow shot speed(VL),high shot speed(VH),pouring temperature(Tp)and initial die temperature(Tm),inverse method was developed to determine the interfacial heat transfer coefficient(IHTC).The results indicate that a closer contact between the casting and die could be achieved when the vacuum system is used.It is found that the vacuum could strongly increase the values of IHTC and decrease the grain size in castings.The IHTC could have a higher peak value with increasing the Tp from680to720℃or the VL from0.1to0.4m/s.In addition,the influence of the VH and Tm on IHTC could be negligible.
基金supported by the National Key Research and Development Plan(Grant Nos.2018YFA0703603,2021YFA0716302)Guangdong Major Project of Basic and Applied Basic Research,China(Grant Nos.2019B030302010,2020B1515120092)+2 种基金Guangdong Basic and Applied Basic Research Foundation,China(Grant Nos.2020B1515120092,2019B030302010)the National Natural Science Foundation of China(Grant Nos.52192602,52192603,51971092,11790291,and 61888102)the Strategic Priority Research Program of Chinese Academy of Sciences(Grant No.XDB30000000).
文摘The glass-forming ability and mechanical properties of metallic glasses and their composites are well known to be sensitive to the preparation conditions and are highly deteriorated by industrial preparing conditions such as low-purity raw materials and low vacuum.Here,we showed that a series of in-situ bulk metallic glass composites(BMGCs)which exhibit excellent ductility and segmental work hardening were successfully developed utilizing a high vacuum high-pressure die casting(HV-HPDC)technology along with industrial-grade raw materials.The tensile properties of these BMGCs are systematically investigated and correlated with the alloy microstructure.As compared with the copper mold suction casting method,the volume fraction difference of the dendrite phase for the BMGCs with the same composition is not significant when fabricated by the HV-HPDC,whereas the size of theβ-phase is generally larger.Insitu BMGCs with the composition of Ti_(48)Zr_(20)(V_(12/17)Cu_(5/17))19 Be 13 obtained by the HV-HPDC process show ductility up to 11.3%under tension at room temperature and exhibit a certain amount of work hardening.Two conditions need to be met to enable the BMGCs,which are prepared by vacuum die-casting to retain favorable ductility:(1)The volume fraction ofβphase stays below 62%±2%;(2)The equiaxed crystals with a more uniform size in the range of 5-10μm.Meanwhile,the results of the present study provided guidance for developing BMGCs with good ductile properties under industrial conditions.
基金financially supported by the National Key Research and Development Program of China (No. 2020YFA0405903)the National Natural Science Foundation of China (Nos. 52001159, 52101141)+1 种基金the Natural Science Foundation of Jiangsu ProvinceChina (No. BK20202010)。