Effects of diamond particle size on microstructure and properties of diamond/Al-12Si composites prepared by vacuum-assisted pressure infiltration

Diamond/aluminium composites have attracted attention in the field of thermal management of electronic packaging for their excellent properties.In order to solve the interfacial problem between diamond and aluminium,a novel process combining pressure infiltration with vacuum-assisted technology was proposed to prepare diamond/aluminum composites.The effect of diamond particle size on the microstructure and properties of the diamond/Al-12Si composites was investigated.The results show that the diamond/Al-12Si composites exhibit high relative density and a uniform microstructure.Both thermal conductivity and coefficient of thermal expansion increase with increasing particle size,while the bending strength exhibits the opposite trend.When the average diamond particle size increases from 45μm to 425μm,the thermal conductivity of the composites increases from 455 W·m^(-1)·K^(-1)to 713 W·m^(-1)·K^(-1)and the coefficient of thermal expansion increases from 4.97×10^(-6)K^(-1)to 6.72×10^(-6)K^(-1),while the bending strength decreases from 353 MPa to 246 MPa.This research demonstrates that high-quality composites can be prepared by the vacuum-assisted pressure infiltration process and the thermal conductivity of the composites can be effectively improved by increasing the diamond particle size.

MXene-based flexible pressure sensor with piezoresistive properties significantly enhanced by atomic layer infiltration

The flexible pressure sensor has been credited for leading performance including higher sensitivity,faster response/recovery,wider detection range and higher mechanical durability,thus driving the development of novel sensing materials enabled by new processing technologies.Using atomic layer infiltration,Pt nanocrystals with dimensions on the order of a few nanometers can be infiltrated into the compressible lamellar structure of Ti3C2Tx MXene,allowing a modulation of its interlayer spacing,electrical conductivity and piezoresistive property.The flexible piezoresistive sensor is further developed from the Pt-infiltrated MXene on a paper substrate.It is demonstrated that Pt infiltration leads to a significant enhancement of the pressure-sensing performance of the sensor,including increase of sensitivity from 0.08 kPa^(-1)to 0.5 kPa^(-1),extension of detection limit from 5 kPa to 9 kPa,decrease of response time from 200 ms to 20 ms,and reduction of recovery time from 230 ms to 50 ms.The mechanical durability of the flexible sensor is also improved,with the piezoresistive performance stable over 1000 cycles of flexure fatigue.The atomic layer infiltration process offers new possibilities for the structure modification of MXene for advanced sensor applications.

Effect of specific pressure on fabrication of 2D-C_f/Al composite by vacuum and pressure infiltration

Carbon fiber reinforced aluminum matrix （Cf/Al） composite has many excellent properties, and it has received more and more attention. Two-dimensional （2D） Cf/Al composites were fabricated by vacuum and pressure infiltration, which was an integrated technique and could provide high vacuum and high infiltration pressure. The effect of specific pressure on the infiltration quality of the obtained composites was comparatively evaluated through microstructure observation. The experimental results show that satisfied Cf/Al composites could be fabricated at the specific pressure of 75 MPa. In this case, the preform was infiltrated much more completely by aluminum alloy liquid, and the residual porosity was seldom found. It is found that the ultimate tensile strength of the obtained Cf/Al composite reached maximum at the specific pressure of 75 MPa, which was improved by 138.9% compared with that of matrix alloy.

Threshold pressure and infiltration behavior of liquid metal into fibrous preform

A dynamic measuring apparatus was developed to investigate the infiltration process of liquid metal into the fibrous preform. 10% （volume fraction） chopped carbon fiber preforms were infiltrated with magnesium alloy under different infiltration pressures. The threshold pressure and flow behavior of liquid metal infiltrating into the preforms were calculated and measured. The microstructure of obtained Ct4Mg composites was observed. The results indicate that the measured threshold pressure for infiltration was 0.048 MPa, which was larger than the calculated value. The infiltration rate increased with the increase of infiltration pressure, but the increase amplitude decreased gradually. The tiny pores in the composites could be eliminated by increasing the infiltration pressure. When the infiltration pressure rose to 0.6 MPa, high quality C1/Mg composite was obtained.

Effects of boron on the microstructure and thermal properties of Cu/diamond composites prepared by pressure infiltration

Diamond reinforced copper（Cu/diamond） composites were prepared by pressure infiltration for their application in thermal management where both high thermal conductivity and low coefficient of thermal expansion（CTE） are important.They were characterized by the microstructure and thermal properties as a function of boron content,which is used for matrix-alloying to increase the interfacial bonding between the diamond and copper.The obtained composites show high thermal conductivity（660 W/（m·K）） and low CET（7.4×10-6 K-1） due to the formation of the B13C2 layer at the diamond-copper interface,which greatly strengthens the interfacial bonding.Thermal property measurements indicate that in the Cu-B/diamond composites,the thermal conductivity and the CTE show a different variation trend as a function of boron content,which is attributed to the thickness and distribution of the interfacial carbide layer.The CTE behavior of the present composites can be well described by Kerner＇s model,especially for the composites with 0.5wt% B.

Thermal conductivity of diamond/copper composites with a bimodal distribution of diamond particle sizes prepared by pressure infiltration method

The thermal conductivity of diamond/copper composites with bimodal particle sizes was studied. The composites were prepared through pressure infiltration of liquid copper into diamond preforms with a mixture of 40 and 100 pm-size diamonds. The permeability of the preforms with different coarse-to-fine volume ratios of diamonds was investigated. The thermal conductivity of the diamond/copper composites with bimodal size distribution was compared to the theoretical value derived from an analytical model developed by Chu. It is predicted that the diamond/copper composites could reach a higher thermal conductivity and their surface roughness could be improved by applying bimodal diamond particle sizes.

Effect of graphite powder as a forming filler on the mechanical properties of SiCp/Al composites by pressure infiltration

（38vo1% SiCp ＋ 2vo1% A1203f）/2024 A1 composites were fabricated by pressure infiltration. Graphite powder was introduced as a forming filler in preform preparation, and the effects of the powder size on the microstructures and mechanical properties of the final com- posites were investigated. The results showed that the composite with 15 μm graphite powder as a forming filler had the maximum tensile strength of 506 MPa, maximum yield strength of 489 MPa, and maximum elongation of 1.2%, which decreased to 490 MPa, 430 MPa, and 0.4%, respectively, on increasing the graphite powder size from 15 to 60 μm. The composite with 60 μm graphite powder showed the highest elastic modulus, and the value decreased from 129 to 113 GPa on decreasing the graphite powder size from 60 to 15 μm. The differences between these properties are related to the different microstructures of the corresponding composites, which determine their failure modes.

Microstructure,mechanical properties and wear resistance of SiC_(p)/AZ91 composite prepared by vacuum pressure infiltration

SiC_(p)/AZ91 composites were prepared by vacuum pressure infiltration.The microstructure,mechanical properties and wear resistance of composite were studied.Results indicated that SiC particles were uniformly distributed in the metal matrix and had a good interface bonding with the metal matrix.Mg_(17)Al_(12) preferably precipitated near the SiC particles,and high-density dislocations were induced by the mismatch of the coefficient of thermal expansion(CTE)between the SiC particle and the AZ91 matrix,thereby accelerating the aging precipitation of the matrix.Compared with AZ91 alloy,the addition of SiC particles improves the hardness and compressive strength of the composite,which is mainly due to the load transfer strengthening and grain refinement strengthening mechanisms.Furthermore,a stable support surface-protecting matrix formed during the wear process because of the excellent wear resistance of SiC.

THE PRODUCTION OF FOAM ALUMINIUM ALLOY BY LOW-PRESSURE INFILTRATION METHOD

The influence of technical parameters on the infiltrating height of the moltenmetal in the process of Producing aluminium alloy foam by low-pressure infiltration method were investigated.Experiments indicated that the height increases with the preheating temperature of granules,theexternal pressureand the pouring temperature of molten alloy,among which the action of pre heating temperature of granules is more effective.There exists a critical pre heating temperature for different size of granules.

Low-temperature heat conduction characteristics of diamond/Cu composite by pressure infiltration method

In this paper,diamond/CuCr and diamond/CuB composites were prepared using the pressure infiltration method.The physical property measurement system(PPMS)was adopted to evaluate the thermal conductivity of diamond/Cu and MoCu composites within the range of100–350 K,and a scanning electron microscope(SEM)was utilized to analyze the microstructure and fracture appearance of the materials.The research indicates that the thermal conductivity of diamond/Cu composite within the range of100–350 K is 2.5–3.0 times that of the existing MoCu material,and the low-temperature thermal conductivity of diamond/Cu composite presents an exponential relationship with the temperature.If B element was added to a Cu matrix and a low-temperature binder was used for prefabricated elements,favorable interfacial adhesion,relatively high interfacial thermal conductivity,and favorable low-temperature heat conduction characteristics would be apparent.

DETERMINATION OF THRESHOLD PRESSURE FOR INFILTRATION OF LIQUID ALUMINIUM INTO SHORT ALUMINA FIBER PREFORM

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Co_(47.5)Fe_(28.·5)Ni_(19)Si_(3.3)Al_(1.7)High-entropy Skeletons Fabricated by Selective Laser Melting and Properties tuned by pressure infiltration of Al

High saturation magnetization and low coercivity are required for soft magnetic materials.This study investigated the Co_(47.5)Fe_(28.5)Ni_(19)Si_(3.3)Al_(1.7)high-entropy soft magnetic skeleton was prepared by selective laser melting.Then Al wpressure infiltrated into skeletons to obtain a dense composite material.The high-entropy composite materials possessed favorable compressive ductility and moderate soft magnetic properties.The high-entropy composite materials were obtained with Ms being 97.1 emu/g,79.8 emu/g,33 emu/g and possessing 19 Oe,15.8Oe and 17Oe of Hc,respectively.However,the magnetostriction coefficient remains low level,about 5ppm.These reported properties are attributed to the special structure of the material studied in present experiment.Nevertheless,a novel strategy of structural designing was proposed in this paper.

Experimental determination of threshold pressure and permeability based on equation-solving method for liquid metal infiltration processes

A new method for determining two key parameters(threshold pressure and permeability)for fabricating metal matrix composites was proposed based on the equation-solving method.An infiltration experimental device was devised to measure the infiltration behavior precisely with controllable infiltration velocity.Two experiments with alloy Pb-Sn infiltrating into Al2O3 preform were conducted independently under two different pressures so as to get two different infiltration curves.Two sets of coefficients which are functions of threshold pressure and permeability can be obtained through curve fitting method.By solving the two-variable equation set,two unknown variables were determined.It is shown that the determined threshold pressure and permeability are very close to the calculated ones and are also verified by another independent infiltration experiment.The proposed method is also feasible to determine the key infiltration parameters for other metal matrix composite systems.

Thermal expansion and mechanical properties of Al/Si composites fabricated by pressure infiltration

High reinforcement content Al/Si composites were fabricated by pressure infiltration technology. The composites are free of porosity and silicon particles distribute uniformly in the composites. The properties and fracture behavior of the composites were studied. The composites fracture is aroused by silicon brittle fracture and extends to the composites inward through the metallurgical structure and fracture analysis. The thermal expansion behavior of the composites was investigated by a high-precision thermomechanical analyzer,and compared with the predictions of theoretical model. The mean linear coefficient of thermal expansion(CET) of Al/Si composites ranges from 8×10-6 to 10×10-6/ ℃ and decreases with increasing silicon volume fraction.

Pressure evolution in shock-compacted granular media

The pressure evolution associated with the transient shock-induced infiltration of gas flow through granular media consisting of mobile particles is numerically investigated using a coupled Eulerian–Lagrangian approach.The coupling between shock compaction and interstitial flow has been revealed.A distinctive two-stage diffusing pressure field with deflection occurring at the tail of the compaction front is found,with corresponding spikes in both gaseous velocity and temperature profiles emerging within the width of the compaction front.The compaction front,together with the deflection pressure,reaches a steady state during the later period.An analytical prediction of the steady deflection pressure that considers the contributions of porosity and the non-isothermal effect is proposed.The isothermal single-phase method we developed,combining the porosity jump condition across the compaction front,shows consistent pressure evolution with the non-isothermal CMP-PIC one under weak shock strength and low column permeability.Lastly,the microscale mechanism governing the formation of not only pressure deflection but also gaseous velocity and temperature spikes within the width of the compaction front has been described.These aforementioned evolutions of the flow field are shown to arise from the nozzling effects associated with the particle-scale variations in the volume fraction.

Stability analysis of unsaturated soil slope during rainfall infiltration using coupled liquid-gas-solid three-phase model

Generally, most soil slope failures are induced by rainfall infiltration, a process that involves interactions between the liquid phase, gas phase,and solid skeleton in an unsaturated soil slope. In this study, a loosely coupled liquid-gas-solid three-phase model, linking two numerical codes,TOUGH2/EOS3, which is used for water-air two-phase flow analysis, and FLAC^(3D), which is used for mechanical analysis, was established. The model was validated through a documented water drainage experiment over a sandy column and a comparison of the results with measured data and simulated results from other researchers. The proposed model was used to investigate the features of water-air two-phase flow and stress fields in an unsaturated soil slope during rainfall infiltration. The slope stability analysis was then performed based on the simulated water-air two-phase seepage and stress fields on a given slip surface. The results show that the safety factor for the given slip surface decreases first, then increases, and later decreases until the rainfall stops. Subsequently, a sudden rise occurs. After that, the safety factor decreases continually and reaches its lowest value, and then increases slowly to a steady value. The lowest value does not occur when the rainfall stops, indicating a delayed effect of the safety factor. The variations of the safety factor for the given slip surface are therefore caused by a combination of pore-air pressure, matric suction, normal stress, and net normal stress.

Negative Pressure Wound Therapy—An Effective, Minimally Invasive Therapeutic Modality in Burn Wound Management

Despite the advancement in burn therapy in the last decades the treatment of burn wounds still remains a challenging task. Infection is still a common complication;while sepsis remains the leading cause of death in severe burns. The research guided integration of new and effective techniques in burn wound management is mandatory. Negative pressure wound therapy (NPWT) is an effective and widely used technique in the management of problematic wounds. Previously existing indications include soft tissue traumas and chronic wounds such as diabetic, arterial, venous and pressure ulcers. The characteristics and challenges of these wounds have a lot in common with burns. Since the early 2000’s there are experiences with the use of NPWT for the healing of second degree burn wounds. Our clinical experience shows that it is a minimally invasive and effective way of improving burn wound management. In this article we give a review of the literature showing the mechanisms, unmapped future opportunities, financial issues, and possible adverse effects of NPWT in burn therapy.

Earth Pressure of Retaining Structure Induced by Subgrade under Rainfall

This article selects the retaining wall as the research object, introducing the rainfall infiltration model, considering the infiltration of rainwater into the groundwater recharge, analysizing the variation of earth pressure in the subgrade retaining wall. On this occasion, the back of retaining wall produces stable seepage water and compares with the non drainage water body. The results show that, with the infiltration of rainwater into the groundwater recharge, the greater the active earth pressure under the condition of rainfall appears, more quickly the active earth pressure of the retaining wall with the drainage body increases. The matrix suction of unsaturated soils, which is infiltrated into soil of subgrade, has a positive effect on the shear strength of the earth pressure.

充水作用下露天煤矿内排土场边坡稳定性分析

为分析废弃矿坑改造成蓄水湖时充水高度对内排土场边坡稳定性的影响,采用室内相似试验、数值模拟和理论分析的方法对不同水位高度下内排土场边坡稳定性进行研究。研究结果表明:随着充水高度的增加,浸润线运移速度、边坡最大位移、孔隙水压力和边坡土体受到的压力整体呈增长趋势。充水高度越大,边坡倾角越大,边坡稳定系数越低。研究结论为露天煤矿改造成蓄水湖或蓄能水电站项目工程提供参考。

稳态渗流下非饱和土涵洞竖向土压力的迭代解与简化

为描述稳态渗流下不同类别非饱和土涵洞的竖向土压力变化,应用圆弧小主应力轨迹法和Mohr应力圆获得考虑土拱效应的滑移面土压力系数,继而基于非饱和土的有效应力强度公式与吸应力理论,由水平薄层单元的竖向力平衡分别建立稳态渗流下上埋式/沟埋式非饱和土涵洞竖向土压力的迭代解,给出应用步骤并开展对比验证与方法拓展,最后结合吸应力沿深度分布规律提出涵洞竖向土压力的简化实用公式。研究结果表明:涵洞竖向土压力迭代解能合理反映土体类别、水分蒸发、降雨入渗和土拱效应的综合影响,并得到文献现场实测和理论公式数据的正确性验证以及对非饱和土涵洞的适用性;涵洞竖向土压力实用公式可显式表达且精度良好,方便估算不同稳态渗流下涵洞主要荷载;砂土涵洞可忽略非饱和特性影响而按饱和土计算竖向土压力,粉土和黏土涵洞可简化吸应力沿深度为线性分布;上埋式涵洞土拱负效应使得竖向土压力增大,而沟埋式涵洞土拱正效应使得竖向土压力减小。