X80 pipeline steel was welded with submerged arc automatic welding, the microstructures, cavity sizes, fusion depths and plane scanning of chemical elements in the welded zone, fusion zone, heat affected zone and base...X80 pipeline steel was welded with submerged arc automatic welding, the microstructures, cavity sizes, fusion depths and plane scanning of chemical elements in the welded zone, fusion zone, heat affected zone and base steel were observed with OM(optical microscope) and SEM(scanning electron microscope), respectively. The experimental results show that there is main acicular ferrite in the base steel and welded zone, the microscopic structure of fusion zone is a blocked bainite, and the heat affected zone is composed of multilateral ferrite and pearlite. M-A unit of the welded zone is the main factor to strengthen the welded zone, composed of acicular ferrites. The percentage of cavities in the welded joint is less than that in the base steel, which is beneficial to increasing its mechanical performance and corrosion resistance. The fusion depth in the fusion zone and welded zone is 101.13 μm and 115.85 μm, respectively, and the distribution of chemical elements in the welded zone is uniform, no enrichment phenomena.展开更多
The successive alteration o the microstructure from the weld metal zone through weld bond to the heat affected zone of a Cr18Ni13 austenitic-0.45%C steels weld joint was observed in situ using transmission electron mi...The successive alteration o the microstructure from the weld metal zone through weld bond to the heat affected zone of a Cr18Ni13 austenitic-0.45%C steels weld joint was observed in situ using transmission electron microscopy.It was found a new type of microstructure called pearlite-like structure and observed the characteristics of the boundary of dissimilar phases. Based on the definition of various zones of the dissimilar steels weld joint under the optical mi- croscope,the transmission electron microscopic characteristics,including microstructures and compositions,of each zone are described and discussed.展开更多
The oxide distribution and microstructure in longitudinal and transverse welding zones during the billet-to-billet extrusion process through porthole die were adequately investigated by means of finite element method,...The oxide distribution and microstructure in longitudinal and transverse welding zones during the billet-to-billet extrusion process through porthole die were adequately investigated by means of finite element method,scanning electron microscopy and optical microscopy.The results indicate that the oxides exist at the interface between the matrix and transverse welding zone rather than longitudinal welding seam.The longitudinal welding zone reveals a darker band including the largest grain with irregular shape due to the abnormal grain growth under the heavy shear deformation and high temperature.The transverse welding zone consists of equiaxed recrystallized grains which are a little finer than those in the longitudinal welding seam.展开更多
Effects of the weld microstructure and inclusions on brittle fracture initiation are investigated in a thermally aged ferritic high-nickel weld of a reactor pressure vessel head from a decommissioned nuclear power pla...Effects of the weld microstructure and inclusions on brittle fracture initiation are investigated in a thermally aged ferritic high-nickel weld of a reactor pressure vessel head from a decommissioned nuclear power plant.As-welded and reheated regions mainly consist of acicular and polygonal ferrite,respectively.Fractographic examination of Charpy V-notch impact toughness specimens reveals large inclusions(0.5-2.5μm)at the brittle fracture primary initiation sites.High impact energies were measured for the specimens in which brittle fracture was initiated from a small inclusion or an inclusion away from the V-notch.The density,geometry,and chemical composition of the primary initiation inclusions were investigated.A brittle fracture crack initiates as a microcrack either within the multiphase oxide inclusions or from the debonded interfaces between the uncracked inclusions and weld metal matrix.Primary fracture sites can be determined in all the specimens tested in the lower part of the transition curve at and below the 41-J reference impact toughness energy but not above the mentioned value because of the changes in the fracture mechanism and resulting changes in the fracture appearance.展开更多
Butt joints between Mg alloy AZ31 B and pure Al 1 060 sheets were produced via metal inert gas welding process with Zn-Cd alloy foil. Crack-free Al/Mg butt joints between AZ31 B Mg alloy and pure Al 1060 sheets were o...Butt joints between Mg alloy AZ31 B and pure Al 1 060 sheets were produced via metal inert gas welding process with Zn-Cd alloy foil. Crack-free Al/Mg butt joints between AZ31 B Mg alloy and pure Al 1060 sheets were obtained. Intermetallic compound layer 1 and layer 2 had formed in fusion zone/Mg alloy and the average thickness of the layer 1 was about 50 μm. The intermetallic compound layer 1 consisted of Al12Mg17 and Mg2Si phases while layer 2 consisted of Al12Mg17, Mg2Si and Mg Zn2 phases. The crack started from the IMC layer at the bottom of the joint and propagated along the brittle IMC layer, then expanded into weld metal during the SEM in situ tensile test. The highest tensile strength of the dissimilar metal butt joints could reach 46.8 MPa and the effect ofinterfacial IMC layer on mechanical property of the joint was discussed in detail in the present study.展开更多
Ultrasonic assisted friction stir welding (UAFSW) is a recent modification of conventional friction stir welding, which adds ultrasonic energy directly into the friction stir welding area by the pin. In this study, ...Ultrasonic assisted friction stir welding (UAFSW) is a recent modification of conventional friction stir welding, which adds ultrasonic energy directly into the friction stir welding area by the pin. In this study, 2A12 aluminum alloy was welded by this process and conventional, respectively. The tensile tests, microstructure and fracture surface of FSW joint and UAFSW joint were analyzed. The research results show that the surface forming texture of ultrasonic assisted friction stir welding joint, compared with conventional, is finer and more uniform, showing metallic matte color. The grains are much finer in weld nugget zone, thermo-mechanically affected zone and heat-affected zone; S-phase particles size is much smaller and distribution is more homogeneous in the matrix. The tensile strength of UAFSW joint is 94. 13% of base metal, and the elongation is 11.77%. The tensile strength of FSW joint is 83.15% of base metal, and the elongation is 8.81%. The tests results reveal that ultrasonic vibration can improve the tensile strength and the elongation of welded joints.展开更多
Microstructure and alloy element distribution in the welded joint between austenitic stainless steel (1Cr18Ni9Ti) and pearlitic heat-resistant steel (1Cr5Mo) were researched by means of light microscopy, scanning elec...Microstructure and alloy element distribution in the welded joint between austenitic stainless steel (1Cr18Ni9Ti) and pearlitic heat-resistant steel (1Cr5Mo) were researched by means of light microscopy, scanning electron microscopy (SEM) and electron probe microanalysis (EPMA). Microstructure, divisions of the fusion zone and elemental diffusion distributions in the welded joints were investigated. Furthermore, solidification microstructure and S-ferrite distribution in the weld metal of these steels are also discussed.展开更多
The laser bonding technology between the Zr41 Ti14 Cu12 Ni10 Be23 bulk metallic glass and zirconium metal was investigated under welding parameters of 1.3 kW and 7 m/min. The welded bead, microstructure, and micro-har...The laser bonding technology between the Zr41 Ti14 Cu12 Ni10 Be23 bulk metallic glass and zirconium metal was investigated under welding parameters of 1.3 kW and 7 m/min. The welded bead, microstructure, and micro-hardness of the welded joint were examined by Keyence, transmission electron microscopy, scanning electron microscopy, and Vickers hardness, respectively. The experimental results showed that the Zr41 Ti14 Cu12 Ni10 Be2 bulk metallic glass and zirconium metal were successfully bonded together. The Zr41 Ti14 Cu12 Ni10 Be2 in the base material zone maintained amorphous structure, and the welding fusion zone kept the hardness as high as as-received BMG. Therefore, the laser welding technology can be used to achieve successful bonding of bulk metallic glasses and crystallization metal.展开更多
Friction stir welding is a new and innovative welding method used to fuse materials. In this welding method, the heat generated by friction and plastic flow causes significant changes in the microstructure of the mate...Friction stir welding is a new and innovative welding method used to fuse materials. In this welding method, the heat generated by friction and plastic flow causes significant changes in the microstructure of the material, which leads to local changes in the mechanical properties of the weld. In this study, the effects of various welding parameters such as the rotational and traverse speeds of the tool on the microstructural and mechanical properties of copper plates were investigated; additionally, Charpy tests were performed on copper plates for the first time. Also, the effect of the number of welding passes on the aforementioned properties has not been investigated in previous studies. The results indicated that better welds with superior properties are produced when less heat is transferred to the workpiece during the welding process. It was also found that although the properties of the stir zone improved with an increasing number of weld passes, the properties of its weakest zone, the heat-affected zone, deteriorated.展开更多
The effect of post weld heat treatment on the microstructure and fracture toughness of friction welded joints of Ti-6.5Al-1Mo-1V-2Zr alloy was studied. The experimental results show that equiaxial grains were formed a...The effect of post weld heat treatment on the microstructure and fracture toughness of friction welded joints of Ti-6.5Al-1Mo-1V-2Zr alloy was studied. The experimental results show that equiaxial grains were formed at the center of the weld metal while highly deformed grains were observed in the thermomechanically affected zone. The fracture toughness of the weld metal was lower than that of the thermomechanically affected zone under as-weld and post weld heat treatment conditions. With increasing temperature of post weld heat treatment, the fracture toughness of weld center and thermomechanically affected zone increased. The fractographic observation revealed that the friction welded joints fractured in a ductile mode.展开更多
Tungsten inert gas(TIG) welding was performed on 2.7 mm thick commercial extruded AZ31 B magnesium alloy plates. We investigated the effect of post-weld heat treatment(PWHT) on the microstructure, mechanical prope...Tungsten inert gas(TIG) welding was performed on 2.7 mm thick commercial extruded AZ31 B magnesium alloy plates. We investigated the effect of post-weld heat treatment(PWHT) on the microstructure, mechanical properties and precipitated phase of the weld joints. The results showed that during the annealing treatment(200 ℃-1 h, 250 ℃-1 h, 300 ℃-1 h, 350 ℃-1 h, 400 ℃-1 h, and 450 ℃-1 h), the average grain size in the weld seam was the minimum after annealing at 400 ℃ for 1 hour, and then abnormally grew up after annealing at 450 ℃ for 1 hour. The mechanical properties enhanced when the joints were processed from 200 ℃-1 h to 400 ℃-1 h but sharply decreased with increasing annealing temperature. In contrast to the annealing treatment, solution treatment(250 ℃-10 h, 300 ℃-10 h, 350 ℃-10 h, 400 ℃-10 h, and 450 ℃-10 h) exhibited a better ductility but a slight deterioration in tensile strength. Especially speaking, no eutectic compounds(such as Mg17 Al12) were observed in the weld seam. The supersaturated Al atoms were precipitated in a coarse spherical shape dispersed in the weld seam. The precipitated Al atoms dissolved in the matrix substances at the condition(400 ℃-1 h) or(250 ℃-10 h). The solution treatment caused grain coarsening and precipitated Al atoms dissolved in the weld seam substantially, which resulted in a drop in micro-hardness at the weld seam compared to the area of the annealed joints.展开更多
The AA6005A-T6 aluminum hollow extrusions were friction stir welded at a high welding speed of 2000mm/min and various axial forces. The results show that the nugget zone (NZ) is characterized by fine equiaxed grains...The AA6005A-T6 aluminum hollow extrusions were friction stir welded at a high welding speed of 2000mm/min and various axial forces. The results show that the nugget zone (NZ) is characterized by fine equiaxed grains, in which a low density of equilibrium phase β is observed. The grains in the thermo-mechanically affected zone (TMAZ) are elongated, and the highest density of dislocations and a low density of β precipitates can be found in grains. The heat affected zone (HAZ) only experiences a low thermal cycle, and a high density of β precipitates and a low density of β precipitates remain in the coarsened grains. The microhardness evolutions in the NZ, TMAZ and HAZ are governed by the grain refinement and dislocation strengthening, the dislocation and precipitation strengthening, and the precipitation and solid solution strengthening, respectively. When increasing the axial force, the changing trend of one strengthening mechanism is contrary to the other in each zone, and the microhardness increases in different zones. As a result, the tensile strength roughly increases with raising the axial force, and all joints show good tensile properties as the high welding speed inhibits the coarsening and dissolution of strengthening precipitates significantly.展开更多
This study was conducted to understand the relationship between various critical temperatures and the stability of the secondary phases inside the heat-affected-zone(HAZ)of welded Grade 91(Gr.91)steel parts.Type IV cr...This study was conducted to understand the relationship between various critical temperatures and the stability of the secondary phases inside the heat-affected-zone(HAZ)of welded Grade 91(Gr.91)steel parts.Type IV cracking has been observed in the HAZ,and it is widely accepted that the stabilities of the secondary phases in Gr.91 steel are critical to the creep resistance,which is related to the crack failure of this steel.In this work,the stabilities of the secondary phases,including those of the M23C6,MX,and Z phases,were simulated by computational thermodynamics.Equilibrium cooling and Scheil simulations were carried out in order to understand the phase stability in welded Gr.91 steel.The effect of four critical temperatures—that is,Acl(the threshold temperature at which austenite begins to form),Ac3(the threshold temperature at which ferrite is fully transformed into austenite),and the M23C6 and Z phase threshold temperatures—on the thickness of the HAZ and phase stability in the HAZ is discussed.Overall,the simulations presented in this paper explain the mechanisms that can affect the creep resistance of Gr.91 steel,and can offer a possible solution to the problem of how to increase creep resistance at elevated temperatures by optimizing the steel composition,welding,and heat treatment process parameters.The simulation results from this work provide guidance for future alloy development to improve creep resistance in order to prevent type IV cracking.展开更多
For Al 6k21-T4 overlap weld joint,the shear-tensile strength by using the weaving laser was improved as compared to the case of linear laser.For the specimen of low strength,the porosity was distributed continuously a...For Al 6k21-T4 overlap weld joint,the shear-tensile strength by using the weaving laser was improved as compared to the case of linear laser.For the specimen of low strength,the porosity was distributed continuously along the intersection between the plates and fusion line.However,for the optimized welding condition,large oval-shaped porosities were located only in the advancing track of the concave part.Therefore,the continuity of cracks and porosities played a key role to determine the strength.And,the weaving width was also the important parameter to control the strength.Furthermore,the concave part had more significant hot and cold cracking in the weld and heat-affected zone(HAZ),respectively,than the convex part.展开更多
The microstructure and corrosion resistance of dissimilar weld-joints between stainless steel SAF 2205 and stainless steel AISI 316L were investigated. Welding was accomplished by different types of welding wires AWS ...The microstructure and corrosion resistance of dissimilar weld-joints between stainless steel SAF 2205 and stainless steel AISI 316L were investigated. Welding was accomplished by different types of welding wires AWS ER 347, AWS ER 316L and AWS ER 309L. To verify soundness of welded samples, nondestructive tests were performed. Metallographic samples were prepared from cross-section areas of weld- joints to investigate microstructure of different regions of weld-joints by optical microscopy and scanning electron microscopy. Corrosion resistance of weld-joints was evaluated in NaCI solution by potentiodynamic polarization and electrochemical impedance techniques. In the weld metal AWS ER 347, the brittle sigma phase was created, resulting in the decrease of weld-joint corrosion resistance. According to the results of metallurgical investigations and corrosion tests, welding wire AWS ER 309L was suitable for welding duplex stainless steel (SAF 2205) to austenitic stainless steel (AIS1316L) by gas tungsten arc welding (GTAW) process.展开更多
In this work, the current understanding and development of fliction-stir welding and processing of Ti- 6Al-4V alloy are briefly reviewed. The critical issues of these processes are addressed, including welding tool ma...In this work, the current understanding and development of fliction-stir welding and processing of Ti- 6Al-4V alloy are briefly reviewed. The critical issues of these processes are addressed, including welding tool materials and design, tool wea,, processing temperature, material flow, processing window and residual stresses. A particular emphasis is given to microstructural aspects and microstructure-properties relationship. Potential engineering applications are highlighted.展开更多
The dissimilar combinations of Inconel 625 and duplex stainless steel SAF 2205 obtained from manual GTA welding process employing ER2209 and ERNi CrMo-3 filler metals have been investigated. Formation of secondary pha...The dissimilar combinations of Inconel 625 and duplex stainless steel SAF 2205 obtained from manual GTA welding process employing ER2209 and ERNi CrMo-3 filler metals have been investigated. Formation of secondary phases at the HAZ of Inconel 625 and grain coarsening at the HAZ of SAF 2205 were witnessed while using these filler wires. The average hardness of ER2209 weldments was found to be greater than ERNi CrMo-3 weld. Tensile fracture was observed at the weld zones for both the fillers. Impact test trials showed brittle mode of fracture on employing ER2209 filler and mixed(ductile–brittle) mode of fracture while using ERNi CrMo-3 filler. Further optical microscopy and SEM/EDS analysis were carried out across the weldments to investigate the structure–property relationships.展开更多
The microstructure and mechanical properties(strength, fatigue and formability) of dissimilar/similar weld joints between DP780 and DP980 steels were studied. The microstructure in fusion zone(FZ) was lath martens...The microstructure and mechanical properties(strength, fatigue and formability) of dissimilar/similar weld joints between DP780 and DP980 steels were studied. The microstructure in fusion zone(FZ) was lath martensite(LM), and alloying elements in the FZ were uniformly distributed. The hardness in the FZ of dissimilar weld joint was similar to the average value(375 HV) of the two similar weld joints. The microstructural evolution in heat affected zone(HAZ) of dissimilar/similar weld joints was as follows:LM(coarse-grained HAZ) →finer LM(fine-grained HAZ) →M-A constituent and ferrite(intercritically HAZ) →tempered martensite(TM) and ferrite(sub-critical HAZ). Lower hardness in intercritically HAZ and sub-critical HAZ(softening zones) was observed compared to base metal(BM) in dissimilar/similar weld joints. The size of softening zone was 0.2-0.3 mm and reduction in hardness was ~7.6%-12.7% of BM in all the weld joints, which did not influence the tensile properties of weld joints such that fracture location was in BM. Formability of dissimilar weld joints was inferior compared to similar weld joints because of the softening zone, non-uniform microstructure and hardness on the two sides of FZ. The effect of microstructure on fatigue life was not influenced due to the presence of welding concavity.展开更多
In this study, 20 mm thick AA7075-T6 alloy plates were joined by friction stir welding. The microstructure and mechanical properties of the nugget zone along the thickness direction from the top to the bottom was inve...In this study, 20 mm thick AA7075-T6 alloy plates were joined by friction stir welding. The microstructure and mechanical properties of the nugget zone along the thickness direction from the top to the bottom was investigated. The results showed that the microstructure including the grain size, the degree of dynamic recrystallization, the misorientation angle distribution and the precipitation phase containing its size, type and content exhibited a gradient distribution along the thickness direction. The testing results of mechanical properties of the slices showed that the nugget was gradually weakened along the depth from the top to the bottom. The maximum ultimate tensile strength, yield strength and elongation of the slice in the nugget top-middle are obtained, which are 415 MPa, 255 MPa and 8.1%, respectively.展开更多
The fatigue performance and fracture mechanism of laser welded twinning induced plasticity(TWIP)steel joint were investigated experimentally based on the evolution of microstructure and micromechanical properties.Th...The fatigue performance and fracture mechanism of laser welded twinning induced plasticity(TWIP)steel joint were investigated experimentally based on the evolution of microstructure and micromechanical properties.The optical microscopy was used to analyze the evolution of microstructure.The variation of composition and phase structure of fusion zone were detected by energy dispersive X-ray and X-ray diffraction spectrometers.The micromechanical behaviors of the various zones were characterized using nanoindentation.The static tensile test and high cycle fatigue test were performed to evaluate the mechanical properties of welded joint and base metal.The microstructures,tensile properties and fatigue strength of base metal as well as welded metal were analyzed.The fatigue fracture surfaces of base metal and welded joint were observed by means of scanning electron microscopy,in order to identify fatigue crack initiation sites and propagation mechanisms.Moreover,the fatigue fracture characteristics and mechanisms for the laser welded TWIP steel joints were analyzed.展开更多
基金Funded by the Chief Expert (Engineer) Project of Jiangsu Provincial Association for Science(No.2013-216)the Innovation Program of Graduated Student of Jiangsu Province(CXLX2014-1098)
文摘X80 pipeline steel was welded with submerged arc automatic welding, the microstructures, cavity sizes, fusion depths and plane scanning of chemical elements in the welded zone, fusion zone, heat affected zone and base steel were observed with OM(optical microscope) and SEM(scanning electron microscope), respectively. The experimental results show that there is main acicular ferrite in the base steel and welded zone, the microscopic structure of fusion zone is a blocked bainite, and the heat affected zone is composed of multilateral ferrite and pearlite. M-A unit of the welded zone is the main factor to strengthen the welded zone, composed of acicular ferrites. The percentage of cavities in the welded joint is less than that in the base steel, which is beneficial to increasing its mechanical performance and corrosion resistance. The fusion depth in the fusion zone and welded zone is 101.13 μm and 115.85 μm, respectively, and the distribution of chemical elements in the welded zone is uniform, no enrichment phenomena.
文摘The successive alteration o the microstructure from the weld metal zone through weld bond to the heat affected zone of a Cr18Ni13 austenitic-0.45%C steels weld joint was observed in situ using transmission electron microscopy.It was found a new type of microstructure called pearlite-like structure and observed the characteristics of the boundary of dissimilar phases. Based on the definition of various zones of the dissimilar steels weld joint under the optical mi- croscope,the transmission electron microscopic characteristics,including microstructures and compositions,of each zone are described and discussed.
基金Project(2012CB619501) supported by the National Basic Research Program of ChinaProject supported by the Chinese Defence Advance Research Program of Science and Technology
文摘The oxide distribution and microstructure in longitudinal and transverse welding zones during the billet-to-billet extrusion process through porthole die were adequately investigated by means of finite element method,scanning electron microscopy and optical microscopy.The results indicate that the oxides exist at the interface between the matrix and transverse welding zone rather than longitudinal welding seam.The longitudinal welding zone reveals a darker band including the largest grain with irregular shape due to the abnormal grain growth under the heavy shear deformation and high temperature.The transverse welding zone consists of equiaxed recrystallized grains which are a little finer than those in the longitudinal welding seam.
基金the SAFIR2022 BRUTE project (Barseback RPV material used for true evaluation of embrittlement) for funding the study
文摘Effects of the weld microstructure and inclusions on brittle fracture initiation are investigated in a thermally aged ferritic high-nickel weld of a reactor pressure vessel head from a decommissioned nuclear power plant.As-welded and reheated regions mainly consist of acicular and polygonal ferrite,respectively.Fractographic examination of Charpy V-notch impact toughness specimens reveals large inclusions(0.5-2.5μm)at the brittle fracture primary initiation sites.High impact energies were measured for the specimens in which brittle fracture was initiated from a small inclusion or an inclusion away from the V-notch.The density,geometry,and chemical composition of the primary initiation inclusions were investigated.A brittle fracture crack initiates as a microcrack either within the multiphase oxide inclusions or from the debonded interfaces between the uncracked inclusions and weld metal matrix.Primary fracture sites can be determined in all the specimens tested in the lower part of the transition curve at and below the 41-J reference impact toughness energy but not above the mentioned value because of the changes in the fracture mechanism and resulting changes in the fracture appearance.
文摘Butt joints between Mg alloy AZ31 B and pure Al 1 060 sheets were produced via metal inert gas welding process with Zn-Cd alloy foil. Crack-free Al/Mg butt joints between AZ31 B Mg alloy and pure Al 1060 sheets were obtained. Intermetallic compound layer 1 and layer 2 had formed in fusion zone/Mg alloy and the average thickness of the layer 1 was about 50 μm. The intermetallic compound layer 1 consisted of Al12Mg17 and Mg2Si phases while layer 2 consisted of Al12Mg17, Mg2Si and Mg Zn2 phases. The crack started from the IMC layer at the bottom of the joint and propagated along the brittle IMC layer, then expanded into weld metal during the SEM in situ tensile test. The highest tensile strength of the dissimilar metal butt joints could reach 46.8 MPa and the effect ofinterfacial IMC layer on mechanical property of the joint was discussed in detail in the present study.
文摘Ultrasonic assisted friction stir welding (UAFSW) is a recent modification of conventional friction stir welding, which adds ultrasonic energy directly into the friction stir welding area by the pin. In this study, 2A12 aluminum alloy was welded by this process and conventional, respectively. The tensile tests, microstructure and fracture surface of FSW joint and UAFSW joint were analyzed. The research results show that the surface forming texture of ultrasonic assisted friction stir welding joint, compared with conventional, is finer and more uniform, showing metallic matte color. The grains are much finer in weld nugget zone, thermo-mechanically affected zone and heat-affected zone; S-phase particles size is much smaller and distribution is more homogeneous in the matrix. The tensile strength of UAFSW joint is 94. 13% of base metal, and the elongation is 11.77%. The tensile strength of FSW joint is 83.15% of base metal, and the elongation is 8.81%. The tests results reveal that ultrasonic vibration can improve the tensile strength and the elongation of welded joints.
基金The work was supported by the Foundation of KeyLaboratory of Liquid Structure and Heredity of Materi-als, Ministry of Educat
文摘Microstructure and alloy element distribution in the welded joint between austenitic stainless steel (1Cr18Ni9Ti) and pearlitic heat-resistant steel (1Cr5Mo) were researched by means of light microscopy, scanning electron microscopy (SEM) and electron probe microanalysis (EPMA). Microstructure, divisions of the fusion zone and elemental diffusion distributions in the welded joints were investigated. Furthermore, solidification microstructure and S-ferrite distribution in the weld metal of these steels are also discussed.
基金Funded by the National Natural Science Foundation of China(Nos.51222508 and 51175211)the Science&Technology Research Projects of Hubei Provincial Committee of Education(No.Q20133004)
文摘The laser bonding technology between the Zr41 Ti14 Cu12 Ni10 Be23 bulk metallic glass and zirconium metal was investigated under welding parameters of 1.3 kW and 7 m/min. The welded bead, microstructure, and micro-hardness of the welded joint were examined by Keyence, transmission electron microscopy, scanning electron microscopy, and Vickers hardness, respectively. The experimental results showed that the Zr41 Ti14 Cu12 Ni10 Be2 bulk metallic glass and zirconium metal were successfully bonded together. The Zr41 Ti14 Cu12 Ni10 Be2 in the base material zone maintained amorphous structure, and the welding fusion zone kept the hardness as high as as-received BMG. Therefore, the laser welding technology can be used to achieve successful bonding of bulk metallic glasses and crystallization metal.
文摘Friction stir welding is a new and innovative welding method used to fuse materials. In this welding method, the heat generated by friction and plastic flow causes significant changes in the microstructure of the material, which leads to local changes in the mechanical properties of the weld. In this study, the effects of various welding parameters such as the rotational and traverse speeds of the tool on the microstructural and mechanical properties of copper plates were investigated; additionally, Charpy tests were performed on copper plates for the first time. Also, the effect of the number of welding passes on the aforementioned properties has not been investigated in previous studies. The results indicated that better welds with superior properties are produced when less heat is transferred to the workpiece during the welding process. It was also found that although the properties of the stir zone improved with an increasing number of weld passes, the properties of its weakest zone, the heat-affected zone, deteriorated.
基金Funded by the Commission of Science,Techonology and Industry for National Defense(No.AXXD1818)
文摘The effect of post weld heat treatment on the microstructure and fracture toughness of friction welded joints of Ti-6.5Al-1Mo-1V-2Zr alloy was studied. The experimental results show that equiaxial grains were formed at the center of the weld metal while highly deformed grains were observed in the thermomechanically affected zone. The fracture toughness of the weld metal was lower than that of the thermomechanically affected zone under as-weld and post weld heat treatment conditions. With increasing temperature of post weld heat treatment, the fracture toughness of weld center and thermomechanically affected zone increased. The fractographic observation revealed that the friction welded joints fractured in a ductile mode.
基金Funded by the National Natural Science Foundation of China(Nos.51505322,51175364)Natural Science Foundation of Shanxi Province of China(No.2013011014-3)
文摘Tungsten inert gas(TIG) welding was performed on 2.7 mm thick commercial extruded AZ31 B magnesium alloy plates. We investigated the effect of post-weld heat treatment(PWHT) on the microstructure, mechanical properties and precipitated phase of the weld joints. The results showed that during the annealing treatment(200 ℃-1 h, 250 ℃-1 h, 300 ℃-1 h, 350 ℃-1 h, 400 ℃-1 h, and 450 ℃-1 h), the average grain size in the weld seam was the minimum after annealing at 400 ℃ for 1 hour, and then abnormally grew up after annealing at 450 ℃ for 1 hour. The mechanical properties enhanced when the joints were processed from 200 ℃-1 h to 400 ℃-1 h but sharply decreased with increasing annealing temperature. In contrast to the annealing treatment, solution treatment(250 ℃-10 h, 300 ℃-10 h, 350 ℃-10 h, 400 ℃-10 h, and 450 ℃-10 h) exhibited a better ductility but a slight deterioration in tensile strength. Especially speaking, no eutectic compounds(such as Mg17 Al12) were observed in the weld seam. The supersaturated Al atoms were precipitated in a coarse spherical shape dispersed in the weld seam. The precipitated Al atoms dissolved in the matrix substances at the condition(400 ℃-1 h) or(250 ℃-10 h). The solution treatment caused grain coarsening and precipitated Al atoms dissolved in the weld seam substantially, which resulted in a drop in micro-hardness at the weld seam compared to the area of the annealed joints.
基金supported by the National Natural Science Foundation of China(51435004,51175117,U1404502)by the National Science and Technology Major Project of China(2010ZX04007-011)
文摘The AA6005A-T6 aluminum hollow extrusions were friction stir welded at a high welding speed of 2000mm/min and various axial forces. The results show that the nugget zone (NZ) is characterized by fine equiaxed grains, in which a low density of equilibrium phase β is observed. The grains in the thermo-mechanically affected zone (TMAZ) are elongated, and the highest density of dislocations and a low density of β precipitates can be found in grains. The heat affected zone (HAZ) only experiences a low thermal cycle, and a high density of β precipitates and a low density of β precipitates remain in the coarsened grains. The microhardness evolutions in the NZ, TMAZ and HAZ are governed by the grain refinement and dislocation strengthening, the dislocation and precipitation strengthening, and the precipitation and solid solution strengthening, respectively. When increasing the axial force, the changing trend of one strengthening mechanism is contrary to the other in each zone, and the microhardness increases in different zones. As a result, the tensile strength roughly increases with raising the axial force, and all joints show good tensile properties as the high welding speed inhibits the coarsening and dissolution of strengthening precipitates significantly.
基金This material is based upon work supported by the US Department of Energy(DOE)(DE-FE0027800).The authors would like to thank the DOE National Energy Technology Laboratory program managers,Dr.Karol Schrems and Dr.Jessica Mullen,and Dr.Wei Zhang from Ohio State University,for their support and guidance.
文摘This study was conducted to understand the relationship between various critical temperatures and the stability of the secondary phases inside the heat-affected-zone(HAZ)of welded Grade 91(Gr.91)steel parts.Type IV cracking has been observed in the HAZ,and it is widely accepted that the stabilities of the secondary phases in Gr.91 steel are critical to the creep resistance,which is related to the crack failure of this steel.In this work,the stabilities of the secondary phases,including those of the M23C6,MX,and Z phases,were simulated by computational thermodynamics.Equilibrium cooling and Scheil simulations were carried out in order to understand the phase stability in welded Gr.91 steel.The effect of four critical temperatures—that is,Acl(the threshold temperature at which austenite begins to form),Ac3(the threshold temperature at which ferrite is fully transformed into austenite),and the M23C6 and Z phase threshold temperatures—on the thickness of the HAZ and phase stability in the HAZ is discussed.Overall,the simulations presented in this paper explain the mechanisms that can affect the creep resistance of Gr.91 steel,and can offer a possible solution to the problem of how to increase creep resistance at elevated temperatures by optimizing the steel composition,welding,and heat treatment process parameters.The simulation results from this work provide guidance for future alloy development to improve creep resistance in order to prevent type IV cracking.
基金supported by a grant from the Ministry of Knowledge Economy,Republic of Koreaby NCRC (National Core Research Center) Program through the National Research Foundation of Korea funded by the Ministry of Education,Science and Technology (2010-0001-222)
文摘For Al 6k21-T4 overlap weld joint,the shear-tensile strength by using the weaving laser was improved as compared to the case of linear laser.For the specimen of low strength,the porosity was distributed continuously along the intersection between the plates and fusion line.However,for the optimized welding condition,large oval-shaped porosities were located only in the advancing track of the concave part.Therefore,the continuity of cracks and porosities played a key role to determine the strength.And,the weaving width was also the important parameter to control the strength.Furthermore,the concave part had more significant hot and cold cracking in the weld and heat-affected zone(HAZ),respectively,than the convex part.
文摘The microstructure and corrosion resistance of dissimilar weld-joints between stainless steel SAF 2205 and stainless steel AISI 316L were investigated. Welding was accomplished by different types of welding wires AWS ER 347, AWS ER 316L and AWS ER 309L. To verify soundness of welded samples, nondestructive tests were performed. Metallographic samples were prepared from cross-section areas of weld- joints to investigate microstructure of different regions of weld-joints by optical microscopy and scanning electron microscopy. Corrosion resistance of weld-joints was evaluated in NaCI solution by potentiodynamic polarization and electrochemical impedance techniques. In the weld metal AWS ER 347, the brittle sigma phase was created, resulting in the decrease of weld-joint corrosion resistance. According to the results of metallurgical investigations and corrosion tests, welding wire AWS ER 309L was suitable for welding duplex stainless steel (SAF 2205) to austenitic stainless steel (AIS1316L) by gas tungsten arc welding (GTAW) process.
文摘In this work, the current understanding and development of fliction-stir welding and processing of Ti- 6Al-4V alloy are briefly reviewed. The critical issues of these processes are addressed, including welding tool materials and design, tool wea,, processing temperature, material flow, processing window and residual stresses. A particular emphasis is given to microstructural aspects and microstructure-properties relationship. Potential engineering applications are highlighted.
文摘The dissimilar combinations of Inconel 625 and duplex stainless steel SAF 2205 obtained from manual GTA welding process employing ER2209 and ERNi CrMo-3 filler metals have been investigated. Formation of secondary phases at the HAZ of Inconel 625 and grain coarsening at the HAZ of SAF 2205 were witnessed while using these filler wires. The average hardness of ER2209 weldments was found to be greater than ERNi CrMo-3 weld. Tensile fracture was observed at the weld zones for both the fillers. Impact test trials showed brittle mode of fracture on employing ER2209 filler and mixed(ductile–brittle) mode of fracture while using ERNi CrMo-3 filler. Further optical microscopy and SEM/EDS analysis were carried out across the weldments to investigate the structure–property relationships.
基金financially supported by the National Natural Science Foundation of China(Grant Nos.51274063 and 51305285)the National Program on Key Basic Research Project(Grant No.2011CB606306-2)+1 种基金the Open Research Fund from the State Key Laboratory of Rolling and Automation,Northeastern University(Grant No.2016005)the Project Funded by China Postdoctoral Science Foundation(Grant No.2016M601877)
文摘The microstructure and mechanical properties(strength, fatigue and formability) of dissimilar/similar weld joints between DP780 and DP980 steels were studied. The microstructure in fusion zone(FZ) was lath martensite(LM), and alloying elements in the FZ were uniformly distributed. The hardness in the FZ of dissimilar weld joint was similar to the average value(375 HV) of the two similar weld joints. The microstructural evolution in heat affected zone(HAZ) of dissimilar/similar weld joints was as follows:LM(coarse-grained HAZ) →finer LM(fine-grained HAZ) →M-A constituent and ferrite(intercritically HAZ) →tempered martensite(TM) and ferrite(sub-critical HAZ). Lower hardness in intercritically HAZ and sub-critical HAZ(softening zones) was observed compared to base metal(BM) in dissimilar/similar weld joints. The size of softening zone was 0.2-0.3 mm and reduction in hardness was ~7.6%-12.7% of BM in all the weld joints, which did not influence the tensile properties of weld joints such that fracture location was in BM. Formability of dissimilar weld joints was inferior compared to similar weld joints because of the softening zone, non-uniform microstructure and hardness on the two sides of FZ. The effect of microstructure on fatigue life was not influenced due to the presence of welding concavity.
基金supported by the National Natural Science Foundation of China(NSFC)(No.51265043 and 51265042)the Special Construction Project of Advanced Science and Technology Innovation Team of Jiangxi Province(No.20171BCB24007)
文摘In this study, 20 mm thick AA7075-T6 alloy plates were joined by friction stir welding. The microstructure and mechanical properties of the nugget zone along the thickness direction from the top to the bottom was investigated. The results showed that the microstructure including the grain size, the degree of dynamic recrystallization, the misorientation angle distribution and the precipitation phase containing its size, type and content exhibited a gradient distribution along the thickness direction. The testing results of mechanical properties of the slices showed that the nugget was gradually weakened along the depth from the top to the bottom. The maximum ultimate tensile strength, yield strength and elongation of the slice in the nugget top-middle are obtained, which are 415 MPa, 255 MPa and 8.1%, respectively.
基金Item Sponsored by National Natural Science Foundation of China(51374151,21201129)Science and Technology Major Project of Shanxi Province of China(20111101053)Natural Science Foundation of Shanxi Province of China(2011011020-2)
文摘The fatigue performance and fracture mechanism of laser welded twinning induced plasticity(TWIP)steel joint were investigated experimentally based on the evolution of microstructure and micromechanical properties.The optical microscopy was used to analyze the evolution of microstructure.The variation of composition and phase structure of fusion zone were detected by energy dispersive X-ray and X-ray diffraction spectrometers.The micromechanical behaviors of the various zones were characterized using nanoindentation.The static tensile test and high cycle fatigue test were performed to evaluate the mechanical properties of welded joint and base metal.The microstructures,tensile properties and fatigue strength of base metal as well as welded metal were analyzed.The fatigue fracture surfaces of base metal and welded joint were observed by means of scanning electron microscopy,in order to identify fatigue crack initiation sites and propagation mechanisms.Moreover,the fatigue fracture characteristics and mechanisms for the laser welded TWIP steel joints were analyzed.