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Optimization of Wickerhamomyces anomalus Fermentation Conditions for Pectinase Production Based on Wet Processing of Arabica Coffee in Yunnan Province 被引量:2
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作者 ZHANG Shu-zhu MENG Jin +6 位作者 XUE Xiao-ran KONG De-ting TIE Li-ping HUANG Jia-xiong QIN Shi-wen HE Fei-fei SUO Yu-kai 《Agricultural Science & Technology》 CAS 2022年第3期30-39,共10页
In order to improve the pectin-degrading efficiency in wet processing of Arabica coffee in Yunnan, Box-Behnken design and single factor experiment were used to optimize the fermentation conditions of five pectinolytic... In order to improve the pectin-degrading efficiency in wet processing of Arabica coffee in Yunnan, Box-Behnken design and single factor experiment were used to optimize the fermentation conditions of five pectinolytic Wickerhamomyces anomalus strains from the fermentation broth of Arabica coffee in Baoshan, Yunnan during wet processing with pectase activity as an indicator. The results showed that the five strains all synthesized pectin lyase(PL), polygalacturonase(PG), and pectin methylesterase(PM).Among them, strain CAP5 had strong ability to produce PG and PL,while strain CAP4 secreted a large amount of PM. Under optimized conditions, the activity of PG, PL, and PM of the five strains came in at 250.17~411.20 U/mL, 12.98~16.55 U/mL, and 208.52~322.83 U/mL,respectively. The four factors of nitrogen source concentration,fermentation time, Mn2+ concentration, and pH value were optimized and the optimal pectinase-producing fermentation conditions for five strains were as follows: peptone 2.2 g/L, fermentation time 30 h, Mn2+ 1.5 mmol/L, and pH 4.3. After fermentation under the optimized conditions, the maximum PG activity of CAP5 amounted to 411.20 U/mL, 114.03% higher than that before optimization.Meanwhile, the PG activity of strains CAP3, CAP4, CAP8, and CAP10 increased by 86.74%, 114.55%, 65.79%, and 66.07%,respectively, and the activity of PL and PM of the five strains rose 150.35%~218.56% and 341.07%~418.52%, respectively. These findings suggested that W. anomalus strains could be used as coffee starter and had great potential for the lysis of pectin. 展开更多
关键词 Wickerhamomyces anomalus COFFEE wet processing PECTINASE Box–Behnken design
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PHASE SEPARATION AND MICROVOID FORMATION AT PHASE INTERFACES OF HYDROPHOBIC-HYDROPHILIC POLYMER BLENDS DURING WET PROCESSING
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作者 郑亚国 周鈜 《Journal of Donghua University(English Edition)》 EI CAS 1989年第Z1期119-124,共6页
In this paper,morphological structure,thermodynamic compatibility and relationship be-tween porosities and blend ratios of the wet coagulated PU/PVA sheets were studied by meansof observation of scanning electronic mi... In this paper,morphological structure,thermodynamic compatibility and relationship be-tween porosities and blend ratios of the wet coagulated PU/PVA sheets were studied by meansof observation of scanning electronic micrographies,tests of dynamic mechanical properties,moisture regain and vapor permeability.Furthermore,the formation of microvoids at interfacesof separated phases was discussed and a microvoid formation mechanism at phase interfaces ofhydrophobic-hydrophilic blends was suggested and compared with that ofhydrophobic-hydrophobic blends. 展开更多
关键词 phase separation interface HYDROPHOBIC HYDROPHILIC POLYURETHANE polyvinyl ALCOHOL wet process porosity microvoid polymer BLEND
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Study on the Genetics and Development of Fiber Pigments and Color Deviation After Wetting Process of Naturally Colored Cotton 被引量:4
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作者 QIUXin-mian ZHOUWen-long 《Agricultural Sciences in China》 CAS CSCD 2003年第4期377-383,共7页
The genetic control of fiber pigment color in naturally colored cotton was studied. The expression of brown and green fiber color was controlled by incompletely dominant single genes and incompletely dominant major ge... The genetic control of fiber pigment color in naturally colored cotton was studied. The expression of brown and green fiber color was controlled by incompletely dominant single genes and incompletely dominant major genes, respectively. Production and accumulation of the fiber pigment were related to special expression of enzymatic genes for pigment synthesis in fiber cells. At the stage of fiber lengthening, naturally colored cotton, like white cotton, appeared purely white. But when fiber cell walls entered the thickening stage, pigment appeared by degrees. When the fiber was completely matured (on boll dehiscence), the color reached its darkest level. After wetting process treatment, the hues of the fiber pigment changed in regular patterns. The hue circle for brown and green cotton changed in the opposite direction with wetting process treatment. In general, the treated cotton color and luster became dark and vivid, and this trend provided the possibility for enhancing the fiber quality by suitable environmental friendly finishing. The analysis showed that the color and luster of the cotton may be controlled by a series of pigments which show different chemical performance. 展开更多
关键词 Naturally colored cotton Fiber pigment GENETICS wetting process
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Simulation of Wetting and Drying Processes in A Depth Integrated Shallow Water Flow Model by Slot Method 被引量:2
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作者 袁德奎 孙健 李小宝 《China Ocean Engineering》 SCIE EI 2008年第3期491-502,共12页
A particular porosity method named "slot method" is implemented in a depth-integrated shallow water flow model (DIVAST) to simulate wetting and drying processes. Discussed is the relationship between the shape fac... A particular porosity method named "slot method" is implemented in a depth-integrated shallow water flow model (DIVAST) to simulate wetting and drying processes. Discussed is the relationship between the shape factors of the "slot" and the preset depth used in "wetting-drying" algorithm. Two typical tests are conducted to examine the performance of the method with the effect of the shape factors of the "slot" being checked in detail in the first test. Numerical results demonstrate that: 1 ) no additional effort to improve the finite difference scheme is needed to implement "slot method" in DIVAST, and 2) "slot method" will simulate wetting and diying processes correctly if the shape factors of the "slot" being selected properly. 展开更多
关键词 wetting and drying processes shallow water flow slot method wetting-drying algorithm tidal fiat
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Characteristics of coal sludge slurry prepared by a wet-grinding process 被引量:3
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作者 Ma Shaolian Wu Guoguang +4 位作者 Meng Xianliang Zhou Rui Chu Ruizhi Miao Zhenyong Qi Yueming 《International Journal of Mining Science and Technology》 SCIE EI CSCD 2016年第5期947-953,共7页
Coal sludge slurry(CSS) is an alternative fuel and a potential competitive method for sludge reduction.Based on the researches of coal water slurry, we studied CSSs by using a wet-grinding process with different types... Coal sludge slurry(CSS) is an alternative fuel and a potential competitive method for sludge reduction.Based on the researches of coal water slurry, we studied CSSs by using a wet-grinding process with different types of regional municipal sludge(sludge) in an orthogonal experiment. The sludge type,sludge mixing proportion, dosage of dispersant, and grinding time were tested in this study. The results show that water content and its occurrence characteristics in the sludge have primary hindering influences on slurry ability. The range of fixed-viscosity concentrations with raw wet sludge is from 50.78%to 44.40%(by weight), while the range is from 53.35% to 51.51%(by weight) with dry sludge. All of the CSSs exhibit shear-thinning behaviors with different variation trends, especially the CSSs with more than 15%(by weight) raw wet sludge in it. Adding the same proportion of raw wet sludge increases the thixotropic properties of CSSs and the highest area of thixotropy loop is 3065 Pa/s, while the highest value of dry sludge is 1798 Pa/s. Hydrophilic group plays an important role in adsorbing water and building three-dimension networks with other particles, which is the main reason for CSS properties.Therefore, the mechanism can be used to find the way for making high quality CSS. 展开更多
关键词 Coal sludge slurry Municipal sludge wet-grinding process Fixed-viscosity concentration Hydrophilic groups
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Response of Freezing/Thawing Indexes to the Wetting Trend under Warming Climate Conditions over the Qinghai–Tibetan Plateau during 1961–2010:A Numerical Simulation 被引量:2
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作者 Xuewei FANG Zhi LI +5 位作者 Chen CHENG Klaus FRAEDRICH Anqi WANG Yihui CHEN Yige XU Shihua LYU 《Advances in Atmospheric Sciences》 SCIE CAS CSCD 2023年第2期211-222,共12页
Since the 1990s,the Qinghai–Tibetan Plateau(QTP)has experienced a strikingly warming and wetter climate that alters the thermal and hydrological properties of frozen ground.A positive correlation between the warming ... Since the 1990s,the Qinghai–Tibetan Plateau(QTP)has experienced a strikingly warming and wetter climate that alters the thermal and hydrological properties of frozen ground.A positive correlation between the warming and thermal degradation in permafrost or seasonally frozen ground(SFG)has long been recognized.Still,a predictive relationship between historical wetting under warming climate conditions and frozen ground has not yet been well demonstrated,despite the expectation that it will become even more important because precipitation over the QTP has been projected to increase continuously in the near future.This study investigates the response of the thermal regime to historical wetting in both permafrost and SFG areas and examines their relationships separately using the Community Land Surface Model version 4.5.Results show that wetting before the 1990s across the QTP mainly cooled the permafrost body in the arid and semiarid zones,with significant correlation coefficients of 0.60 and 0.48,respectively.Precipitation increased continually at the rate of 6.16 mm decade–1 in the arid zone after the 1990s but had a contrasting warming effect on permafrost through a significant shortening of the thawing duration within the active layer.However,diminished rainfall in the humid zone after the 1990s also significantly extended the thawing duration of SFG.The relationship between the ground thawing index and precipitation was significantly negatively correlated(−0.75).The dual effects of wetting on the thermal dynamics of the QTP are becoming critical because of the projected increases in future precipitation. 展开更多
关键词 freezing/thawing indexes numerical modeling wetting process frozen ground Qinghai–Tibetan Plateau
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Distribution of REE of Phosphate Concentrate in Wet-Phosphoric Acid Process 被引量:2
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作者 金会心 李军旗 +1 位作者 王华 毛小浩 《Journal of Rare Earths》 SCIE EI CAS CSCD 2007年第S1期78-84,共7页
There exists the most important REE-bearing phosphorite deposit in Southwest of China. Due to the fact that the REE are present in the form of ions in the lattices of collophanite or carbonatfluorapatite, the REE can ... There exists the most important REE-bearing phosphorite deposit in Southwest of China. Due to the fact that the REE are present in the form of ions in the lattices of collophanite or carbonatfluorapatite, the REE can be enriched in phosphate concentrate by flotation method. The phosphate concentrate is the main raw materials to produce phosphoric acid, therefore, it is significant to further investigate the distribution rule of REE in wet process. In this paper, the single leaching and recycled leaching technology were carried out to investigate the effect of various parameter conditions on distribution of REE in products. The REE compositions of products were analyzed by Inductively Coupled Plasma Emission Mass Spectrometry (ICP-MS) method. It was found that the acidic value of leaching liquor was the main effect factor on the distribution of REE in products. In single leaching stage, P2O5 concentration of leaching liquor slightly varied from 8% to about 10% when the excessive coefficient of sulphuric acid ranged from 1.03 to 1.05, and the distribution proportions of ∑REO in phosphoric acid solution was lower than 40%. However, in recycled leaching process(the condition similar to practical wet process), with an increase of P2O5 concentration as well as the acidic value of leaching liquor, the distribution proportions of ∑REO in phosphoric acid solution could be decreased to 2.56%. That is to say that under the condition similar to practical wet process, more than 90% of REE of phosphate concentrate became precipitation entering into the phosphogypsum product. This investigation will provide valid reference for reasonably recovering or reserving REE in wet-phosphoric acid process. 展开更多
关键词 wet-phosphoric acid process distribution of REE single leaching recycled leaching rare earths
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Energy and Cost Analysis of Cement Production Using the Wet and Dry Processes in Nigeria
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作者 Olayinka S. Ohunakin Oluwafemi R. Leramo +2 位作者 Olatunde A. Abidakun Moradeyo K. Odunfa Oluwafemi B. Bafuwa 《Energy and Power Engineering》 2013年第9期537-550,共14页
The study evaluates the energy consumption of both wet and dry processes cement manufacturing plant in Nigeria. Enrgy consumption data collected for the period 2003 to 2011 were used to estimate the energy consumption... The study evaluates the energy consumption of both wet and dry processes cement manufacturing plant in Nigeria. Enrgy consumption data collected for the period 2003 to 2011 were used to estimate the energy consumption of the crushing, milling, agitation, burning, grinding and bagging operations. The total energy evaluation was based on the three primary energy sources which include electrical, combustion and human. The total estimated energy intensities were 6545 MJ/ton and 4197 MJ/ton for wet and dry processes respectively. The percentage consumption of energy in each operation is 93.68 and 90.34% (burning), 2.11 and 4.33% (milling), 0.43 and 0.67% (crushing), 1.39 and 0% (agitation), 2.12 and 3.90% (grinding), and 0.27 and 0.75% (bagging) of the total energy inputs for the wet and dry processes respectively. Furthermore, the average total energy cost of production showed that wet process is approximately 40% more cost intensive in cement production than the dry process while at the same time it is cost effective to run production on energy through gas powered plant than the national grid. 展开更多
关键词 wet process Dry process CEMENT CRUSHING MILLING NIGERIA
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Wet Coffee Processing Discharges Affecting Quality of River Water at Kayanza Ecological Zone, Burundi
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作者 Emile Bisekwa Paul M. Njogu Taye Kufa-Obso 《Open Journal of Applied Sciences》 2021年第6期707-721,共15页
Wet coffee processing leads to the generation of large volumes of wastewater, whose discharge to the environment leads to pollution of freshwater bodies. Kayanza is a major coffee growing area in Burundi with more tha... Wet coffee processing leads to the generation of large volumes of wastewater, whose discharge to the environment leads to pollution of freshwater bodies. Kayanza is a major coffee growing area in Burundi with more than 40 wet coffee processing factories (WCPF) that discharge effluents directly to receiving water bodies without treatment. This study was carried out to assess the effect of coffee wastewater on the physicochemical properties of receiving waterbodies in Kayanza coffee growing ecological zone. Currently, no study has been done to analyze the effluent from the WCPF and assess the level of pollution. This study will therefore provide valuable data on the water pollution from coffee processing plants. Ten (10) rivers in the Kayanza coffee growing zone were studied during the months of April and June, 2020. Water samples were collected upstream (U) and downstream (D) of the effluent discharge points in triplicate. Samples were analyzed for pH, Chemical Oxygen Demand (COD), Biochemical Oxygen Demand (BOD<sub>5</sub>), Temperature, Salinity, Electrical Conductivity (EC), Total Dissolved Solids (TDS), Dissolved Oxygen (DO), Total Suspended Solids (TSS), Nitrates, Nitrites, Lead (Pb), Copper (Cu), Chlorides and Ammonium ions using standard methods. <span style="letter-spacing:0.1pt;">Ph</span>ysical parameters were analyzed in situ whereas chemical param<span style="letter-spacing:0.1pt;">eters w</span><span style="letter-spacing:-0.05pt;">ere analy</span>zed in the laboratories in Burundi Institute of Agricultural Science<span style="letter-spacing:0.1pt;">s</span> (ISA<span style="letter-spacing:-0.2pt;">BU) and University of Burundi. Data were analyzed u</span>sing R-studio-1.0.153, GenStat 64-bit Release 14.1 and SSPS. Results on the physicochemical parameters indicated that coffee factory effluent has a polluting potential during coffee processing peak. The concentrations of the physicochemical parameters were significantly (p < 0.05) higher downstream (D) compared to upstream (U) of the river water sampling points. All downstream sites had COD, BOD<sub>5</sub>, TSS and pH values above allowable limits set by WHO and Burundi. The polluting impact of public wet coffee processing factories was significantly higher than that of private and cooperatives owned factories (p < 0.05). Measures should be taken in order to protect water bodies. 展开更多
关键词 Wastewater Water Pollution Kayanza Zone wet Coffee processing
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THERMAL PROCESS OF VACUUM FLUXLESS LASER SOLDERING AND ANALYSIS ON SOLDER SPREADING AND WETTING
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作者 Wang Chunqing Li Mingyu +1 位作者 SunFujiang Feng Wufeng (National key laboratory of welding, Harbin Institute of Technology) 《Chinese Journal of Mechanical Engineering》 SCIE EI CAS CSCD 2000年第2期127-133,共7页
In order to study the mechanism of vacuum fluxless soldering on the conditions of laser heating, the method of measuring temperature by the thermocouple is used to analyze the spreading and wetting process of both flu... In order to study the mechanism of vacuum fluxless soldering on the conditions of laser heating, the method of measuring temperature by the thermocouple is used to analyze the spreading and wetting process of both fluxless Sn-Pb solder in the vacuum surroundings and flux Sn-Pb solder on Cu pad. Solder spreading and wetting affected by the soldering thermal process is also discussed according to the thermodynamics principle. Results show that vacuum fluxless soldering demands higher temperature, and the fall of the solder surface tension is the important factor achieving fluxless laser soldering. 展开更多
关键词 Fluxless soldering Soldering thermal process Spreading and wetting
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Short wet-steam dyeing process of cotton fabrics with reactive dyes 被引量:1
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作者 SUN Fu-yun WANG Zhao-feng FANG Kuan-jun 《科技视界》 2017年第34期38-39,共2页
The effects of Reactive Black 5 utilized to cotton fabrics by short wet-steam process on the dyeing properties were investigated. This study will provide a theoretical reference for short wet-steam process of cotton f... The effects of Reactive Black 5 utilized to cotton fabrics by short wet-steam process on the dyeing properties were investigated. This study will provide a theoretical reference for short wet-steam process of cotton fabrics with bifunctional reactive dyes. The optimal amount of Selilao agent was 20 g/L, while the soaping and rubbing fastness of the dyed cotton fabrics were both reached to 4-5 rating. 展开更多
关键词 wet-steam
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Research on the application of the wet scrubber on the BSSF slag processing system at Baosteel
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作者 LI Yongqian LIU Yin XIAO Yongli 《Baosteel Technical Research》 CAS 2009年第3期38-40,共3页
Based on the analysis results of the dust size distribution of flue gas from Baosteel's short-flow (BSSF) slag processing system and the mechanism of the wet scrubber,a wet scrubber system was designed and installe... Based on the analysis results of the dust size distribution of flue gas from Baosteel's short-flow (BSSF) slag processing system and the mechanism of the wet scrubber,a wet scrubber system was designed and installed in the No. 1 BSSF slag processing system at Baosteel. The results show that the dust removal efficiency of the previous system that had conventional water nozzles was only 69% with a liquid-gas ratio of 0.79 L/m^3 ,while the dust removal efficiency reached 94% when three sets of high-efficiency dual phase spray guns were installed inside both the flue and the chimney. For the latter system,the liquid-gas ratio was 0. 84 L/m^3 ,and the dust concentration in the cleaned emissions reduced to less than 40 mg/m^3. 展开更多
关键词 slag processing wet scrubber NOZZLE particle size distribution dust removal efficiency
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锌浮渣干湿法处理工艺对比与干法处理工艺关键设备选型及应用 被引量:1
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作者 陈向强 宋言 《有色设备》 2024年第1期86-93,共8页
在湿法炼锌的工业生产中,电解阴极锌片在熔锌感应电炉内熔化除杂时产出副产品锌浮渣,锌浮渣中含锌约80%,其中70%以上锌以单质形态存在。本文对比了干法和湿法两种处理工艺的优缺点,重点介绍了干法处理工艺中关键设备选择和能力计算,并... 在湿法炼锌的工业生产中,电解阴极锌片在熔锌感应电炉内熔化除杂时产出副产品锌浮渣,锌浮渣中含锌约80%,其中70%以上锌以单质形态存在。本文对比了干法和湿法两种处理工艺的优缺点,重点介绍了干法处理工艺中关键设备选择和能力计算,并结合实际生产情况对投产后的工艺设备进行改进和完善。 展开更多
关键词 锌浮渣 干法 湿法 球磨 分离 锌粉
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湿法热解法制备L-焦谷氨酸的工艺优化研究
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作者 王艳领 田春美 《化工管理》 2024年第14期150-152,共3页
采用湿法热解法,以L-谷氨酸为原料,探究L-焦谷氨酸的制备工艺条件。通过单因素和正交试验对反应的条件进行优化,确定了制备L-焦谷氨酸的最佳工艺条件是反应时间4 h、加水量15 g、反应温度150℃,此时所得L-谷氨酸的转化率为97.37%。这种... 采用湿法热解法,以L-谷氨酸为原料,探究L-焦谷氨酸的制备工艺条件。通过单因素和正交试验对反应的条件进行优化,确定了制备L-焦谷氨酸的最佳工艺条件是反应时间4 h、加水量15 g、反应温度150℃,此时所得L-谷氨酸的转化率为97.37%。这种方法是用水作为反应载体,无需催化剂与压力等条件,既节能减排,又产量高,为清洁高效生产L-焦谷氨酸提供了一定的理论指导和实验数据参考。 展开更多
关键词 L-焦谷氨酸 L-谷氨酸 湿法热解 工艺优化
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膨润土矿物选矿提纯方法研究
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作者 李彩霞 徐猛 +4 位作者 徐依 邢博文 李树蔚 周洪博 寇吉良 《贵州大学学报(自然科学版)》 2024年第1期20-26,共7页
膨润土是我国的一种优势资源,其主要矿物成分为层状结构的蒙脱石,但天然膨润土中蒙脱石的含量不高,一些低质的膨润土蒙脱石含量仅在50%左右,杂质含量较高,必须经过提纯才能用于开发高端产品。膨润土提纯方法及效果一直是行业急需的技术... 膨润土是我国的一种优势资源,其主要矿物成分为层状结构的蒙脱石,但天然膨润土中蒙脱石的含量不高,一些低质的膨润土蒙脱石含量仅在50%左右,杂质含量较高,必须经过提纯才能用于开发高端产品。膨润土提纯方法及效果一直是行业急需的技术,但不同的膨润土性能及伴生的杂质不同,提纯方法不同,针对膨润土提纯方法的现状,通过综述回顾膨润土提纯的研究进展,为膨润土提纯在实际生产中应用提供指导。 展开更多
关键词 膨润土 提纯 干法 湿法
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锌湿法冶炼渣污染物及综合利用研究 被引量:1
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作者 刘安强 《世界有色金属》 2024年第10期23-25,共3页
锌湿法冶炼是一种常用的锌冶炼工艺,它在生产过程中会产生大量的渣污染物。这些渣污染物主要包含氧化锌、氧化铁、浸出渣、净化渣等。由于这些渣含有大量有价值的金属元素和资源,对其进行综合利用具有重要意义。本文通过详细分析渣污染... 锌湿法冶炼是一种常用的锌冶炼工艺,它在生产过程中会产生大量的渣污染物。这些渣污染物主要包含氧化锌、氧化铁、浸出渣、净化渣等。由于这些渣含有大量有价值的金属元素和资源,对其进行综合利用具有重要意义。本文通过详细分析渣污染物形成过程、组成及含量,介绍常用的渣污染物处理方法,探讨综合利用渣污染物的技术方法,能为相关领域提供参考,并促进该领域技术与应用的进一步发展。 展开更多
关键词 锌湿法 冶炼 渣污染物 综合利用
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涂装漆雾治理干湿法分离技术试验对比
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作者 何曦 叶明强 +7 位作者 周益辉 邱敬贤 黄仕良 刘胜强 黄安涛 胡献舟 李二平 杨利平 《电镀与涂饰》 CAS 北大核心 2024年第7期144-151,共8页
[目的]漆雾作为涂装作业产生的主要污染物之一,其治理效果是影响其他污染物治理成败的关键。常见的治理方式主要有干法和湿法两类,但同一工况下的对比研究鲜有报道。[方法]以喷涂车间产生的漆雾为治理目标,分别以干法工艺(球滤与玻璃纤... [目的]漆雾作为涂装作业产生的主要污染物之一,其治理效果是影响其他污染物治理成败的关键。常见的治理方式主要有干法和湿法两类,但同一工况下的对比研究鲜有报道。[方法]以喷涂车间产生的漆雾为治理目标,分别以干法工艺(球滤与玻璃纤维棉过滤相结合)和湿法工艺(水旋分离)进行漆雾治理试验研究。[结果]干法工艺去除漆雾的平均效率达到95%,湿法工艺则达到98%。湿法工艺较干法工艺有更低的排放浓度和更稳定的表现,但两者均出现了漆雾附着在设备内壁的情况。[结论]在工程应用中,应根据项目的具体情况来选择合适的漆雾治理工艺。 展开更多
关键词 涂装 漆雾 干法 湿法 微观形貌
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湿法磷酸脱氟工艺的研究现状与发展方向 被引量:5
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作者 哀鹏鹏 彭朝凯 +3 位作者 刘成龙 陈迎新 翁孝卿 李洪强 《湿法冶金》 CAS 北大核心 2024年第1期9-14,共6页
阐述了氟对湿法磷酸生产工艺的影响,综述了针对湿法磷酸的主要脱氟工艺的原理、应用现状及优缺点。指出了目前湿法磷酸脱氟工艺存在的问题,并分析了未来的研究发展方向,以期为我国湿法磷酸中氟资源的综合利用提供参考。
关键词 湿法 磷酸 脱氟 去除 回收 现状 进展 发展方向
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磷酸法低灰分活性炭的制备研究
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作者 张丽 张丹 +3 位作者 潘红艳 董永刚 李文飞 秦红 《无机盐工业》 CAS CSCD 北大核心 2024年第2期95-103,120,共10页
磷酸活化法是目前工业上生产生物质基活性炭的主要方法,但较高的灰分含量限制其在医药、食品等高端领域应用。基于此,以湿法磷酸为活化剂、废木屑为碳源,研究活化条件(温度、时间等)和洗涤条件(介质、酸浓度、温度等)对活性炭灰分及性... 磷酸活化法是目前工业上生产生物质基活性炭的主要方法,但较高的灰分含量限制其在医药、食品等高端领域应用。基于此,以湿法磷酸为活化剂、废木屑为碳源,研究活化条件(温度、时间等)和洗涤条件(介质、酸浓度、温度等)对活性炭灰分及性能的影响,运用TG、FT-IR、XRD、SEM和TEM等表征方法分析活性炭的表面性质和微观结构。结果表明,难溶性磷酸盐是活性炭灰分产生的主要因素,通过控制活性炭制备和洗涤工艺可调控难溶性磷酸盐含量,从而调控活性炭灰分、碘值和亚甲蓝值。获得最佳工艺条件:活化温度为500℃、活化剂H_(3)PO_(4)质量分数为70%、酸屑质量比为2∶1、活化时间为60min及N_(2)气氛保护;洗涤液用量为100mL、洗涤介质为H_(3)PO_(4)、H_(3)PO_(4)质量分数为20%、洗涤温度为80℃及洗涤时间为60 min。最佳工艺条件下制备的活性炭灰分为1.07%、碘值为1241.4 mg/g、亚甲蓝值为285 mg/g、比表面积为2290 m^(2)/g,表明该技术制备的活性炭具有应用于食品、医药等高端行业领域的潜质。 展开更多
关键词 活性炭 湿法磷酸 灰分 吸附性能
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基于正交设计的鞋面革湿态染整工艺设计与优化 被引量:1
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作者 韦永红 郭文翰 +3 位作者 李瑞强 张琪 温会涛 但卫华 《中国皮革》 CAS 2024年第5期1-7,共7页
应用正交设计方法,以坯革收缩温度、废液铬含量、坯革增厚率、撕裂力、柔软度、得革率为考察指标,对牛鞋面革湿态染整工艺的复鞣、填充、加脂工序进行设计与优化。试验结果表明,复鞣最佳工艺为醛酸复鞣剂用量6%,转动时间60 min,铬鞣剂用... 应用正交设计方法,以坯革收缩温度、废液铬含量、坯革增厚率、撕裂力、柔软度、得革率为考察指标,对牛鞋面革湿态染整工艺的复鞣、填充、加脂工序进行设计与优化。试验结果表明,复鞣最佳工艺为醛酸复鞣剂用量6%,转动时间60 min,铬鞣剂用量4%,转动时间90 min;填充最佳工艺为丙烯酸树脂用量4%,氨基树脂用量6%,合成鞣剂用量8%,植物栲胶用量4%;加脂最佳工艺为合成油用量6%,牛蹄油用量3%,卵磷脂用量4%,合成酯用量3%;最佳工艺集成后所制得的鞋面革性能满足QB/T 1873—2010的要求。 展开更多
关键词 制革工程 正交设计 鞋面革 湿态染整
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