介绍了近年来微纳米材料强度实验测试研究方面的最新进展,重点综述了可用于微纳米材料及其结构中界面强度测试的实验系统、测试方法及结果.主要内容包括:测试微纳米薄膜界面端分层裂纹启裂的夹层悬臂梁方法,测试纳米岛/衬底间界面结合...介绍了近年来微纳米材料强度实验测试研究方面的最新进展,重点综述了可用于微纳米材料及其结构中界面强度测试的实验系统、测试方法及结果.主要内容包括:测试微纳米薄膜界面端分层裂纹启裂的夹层悬臂梁方法,测试纳米岛/衬底间界面结合强度的改进AFM(atomic force microscopy)方法,测试裂纹沿界面扩展的预裂纹法,可实现纳米薄膜界面裂纹原位观察的实验测试方法,测试薄膜在疲劳、蠕变条件下界面裂纹扩展的改进4点弯曲法等.除了总结分析测试结果,还讨论了上述实验方法的优缺点和适用范围,并指出了微纳米材料界面强度实验研究方面的一些挑战与难点,最后提出了若干需要继续研究的课题.展开更多
The title complex, [Cu(Hsal)2(py)2], was synthesized by layered solution technique and structurally characterized by single crystal X ray. The copper atom has a square pyramidal geometry and the coordination number is...The title complex, [Cu(Hsal)2(py)2], was synthesized by layered solution technique and structurally characterized by single crystal X ray. The copper atom has a square pyramidal geometry and the coordination number is five. The molecular structure is linear one dimensional network. There is a stacking effect between pyridine ligands of neighbouring 1 D chains and the molecular structure is extended into two dimensional stacking network. Two salicylates in the complex have a position of crab pincers like, in which one salicylate is unidentate and another coordinates through the carboxylate group and phenyl group unidentately.展开更多
文摘介绍了近年来微纳米材料强度实验测试研究方面的最新进展,重点综述了可用于微纳米材料及其结构中界面强度测试的实验系统、测试方法及结果.主要内容包括:测试微纳米薄膜界面端分层裂纹启裂的夹层悬臂梁方法,测试纳米岛/衬底间界面结合强度的改进AFM(atomic force microscopy)方法,测试裂纹沿界面扩展的预裂纹法,可实现纳米薄膜界面裂纹原位观察的实验测试方法,测试薄膜在疲劳、蠕变条件下界面裂纹扩展的改进4点弯曲法等.除了总结分析测试结果,还讨论了上述实验方法的优缺点和适用范围,并指出了微纳米材料界面强度实验研究方面的一些挑战与难点,最后提出了若干需要继续研究的课题.
文摘The title complex, [Cu(Hsal)2(py)2], was synthesized by layered solution technique and structurally characterized by single crystal X ray. The copper atom has a square pyramidal geometry and the coordination number is five. The molecular structure is linear one dimensional network. There is a stacking effect between pyridine ligands of neighbouring 1 D chains and the molecular structure is extended into two dimensional stacking network. Two salicylates in the complex have a position of crab pincers like, in which one salicylate is unidentate and another coordinates through the carboxylate group and phenyl group unidentately.
