The uniaxial tensile test of the 5A06-O aluminium−magnesium(Al−Mg)alloy sheet was performed in the temperature range of 20−300℃ to obtain the true stress−true strain curves at different temperatures and strain rates....The uniaxial tensile test of the 5A06-O aluminium−magnesium(Al−Mg)alloy sheet was performed in the temperature range of 20−300℃ to obtain the true stress−true strain curves at different temperatures and strain rates.The constitutive model of 5A06-O Al−Mg alloy sheet with the temperature range from 150 to 300℃ was established.Based on the test results,a unique finite element simulation platform for warm hydroforming of 5A06-O Al−Mg alloy was set up using the general finite element software MSC.Marc to simulate warm hydroforming of classic specimen,and a coupled thermo-mechanical finite element model for warm hydroforming of cylindrical cup was built up.Combined with the experiment,the influence of the temperature field distribution and loading conditions on the sheet formability was studied.The results show that the non-isothermal temperature distribution conditions can significantly improve the forming performance of the material.As the temperature increases,the impact of the punching speed on the forming becomes particularly obvious;the optimal values of the fluid pressure and blank holder force required for forming are reduced.展开更多
Solid-state bonding between pure titanium and Ti6Al4V(TC4)alloy was conducted by a new bonding method named as rigid restraint thermal self-compressing bonding.Effects of heating time on bonding interface,atom diffusi...Solid-state bonding between pure titanium and Ti6Al4V(TC4)alloy was conducted by a new bonding method named as rigid restraint thermal self-compressing bonding.Effects of heating time on bonding interface,atom diffusion and mechanical properties of the joints were studied.Results show that atom diffusion between pure titanium and TC4 alloy significantly takes place during bonding.The diffusion depths of Al and V in pure titanium side are increased with increasing heating time.Due to the enhancement of atom diffusion,bond quality of the bonding interface is improved along with the increase of heating time.The heating time seems to have little effect on microhardness distribution across the joint.However,the tensile strength and ductility of the joint have close relation to heating time.Prolonging heating time can improve the tensile strength and ductility of the joint,especially the latter.When the heating time increases to 450 s,solid-state joint with good combination of strength and ductility is attained.展开更多
In order to clarify the influence of grain size on cyclic deformation response of superalloy sheets and springback behavior,cyclic loading-unloading and shearing tests were performed on the superalloy foils with 0.2 m...In order to clarify the influence of grain size on cyclic deformation response of superalloy sheets and springback behavior,cyclic loading-unloading and shearing tests were performed on the superalloy foils with 0.2 mm in thickness and diverse grain sizes.The results show that,the decline ratio of elastic modulus is weakened with increasing grain size,and the Bauschinger effect becomes evident with decreasing grain size.Meanwhile,U-bending test results determine that the springback is diminished with increasing grain size.The Chaboche,Anisotropic Nonlinear Kinematic(ANK)and Yoshida-Uemori(Y-U)models were utilized to fit the shear stress-strain curves of specimens.It is found that Y-U model is sufficient of predicting the springback.However,the prediction accuracy is degraded with increasing grain size.展开更多
The influence of initial groove angle on strain rate inside and outside groove of Ti6Al4V alloy was investigated.Based on the evolution of strain rate inside and outside groove,the effect of strain rate difference on ...The influence of initial groove angle on strain rate inside and outside groove of Ti6Al4V alloy was investigated.Based on the evolution of strain rate inside and outside groove,the effect of strain rate difference on the evolution of normal stress and effective stress inside and outside groove was also analyzed.The results show that when linear loading path changes from uniaxial tension to equi-biaxial tension,the initial groove angle plays a weaker role in the evolution of strain rate in the M-K model.Due to the constraint of force equilibrium between inside and outside groove,the strain rate difference makes the normal stress inside groove firstly decrease and then increase during calculation,which makes the prediction algorithm of forming limit convergent at elevated temperature.The decrease of normal stress inside groove is mainly caused by high temperature softening effect and the rotation of groove,while the increase of normal stress inside groove is mainly due to strain rate hardening effect.展开更多
The Ti−6Al−4V(TC4)alloy powder and forged solid were diffusion bonded by hot isostatic pressing(HIP)to fabricate a powder−solid part.The microstructure of the powder−solid part was observed by scanning electron micros...The Ti−6Al−4V(TC4)alloy powder and forged solid were diffusion bonded by hot isostatic pressing(HIP)to fabricate a powder−solid part.The microstructure of the powder−solid part was observed by scanning electron microscope(SEM).The microhardness and tensile tests were conducted to investigate the mechanical properties.The results showed that the powder compact was near-fully dense,and the powder/solid interface was tight and complete.The microhardness of the interface was higher than that of the powder compact and solid.The fractures of all powder−solid tensile specimens were on the solid side rather than at the interface,which indicated that a good interfacial strength was obtained.The tensile strength and elongation of the powder compact were higher than those of the solid.It is concluded that the HIP process can successfully fabricate high-quality Ti−6Al−4V powder−solid parts,which provides a novel near net shape technology for titanium alloys.展开更多
The novel Ni-based brazing filler was used to join C/C composites.When brazing temperature increased from 1080 to 1100°C,the wetting angle decreased from 23°to 14°,and the brazing filler had good wettab...The novel Ni-based brazing filler was used to join C/C composites.When brazing temperature increased from 1080 to 1100°C,the wetting angle decreased from 23°to 14°,and the brazing filler had good wettability on the surface of C/C composites.The brazing seam of the brazed joint consisted of Ni(s,s)and Cr_(3)C_(2) phases.As brazing temperature increased,lots of Cr_(3)C_(2) phases were generated at the bonding interface,and the thick reaction layer was formed.When brazing temperature was 1120°C,the shear strength of C/C joint reached the maximum value of 31.5 MPa.The fracture path extended in the C/C matrix close to the bonding interface.展开更多
A novel experimental approach was presented, namely the overlapping elliptical bulge test, which can load and research thickness normal stress. Theoretical analysis model of the overlapping elliptical bulging was desc...A novel experimental approach was presented, namely the overlapping elliptical bulge test, which can load and research thickness normal stress. Theoretical analysis model of the overlapping elliptical bulging was described, the equivalent stress?strain curves of target sheets with different ellipticity ratios were determined experimentally, and influences of the material performance and thickness of overlapping sheets on the flow property of the target sheet were also researched. The results show that, in the overlapping hydraulic bulge test, the equivalent stress?strain curve can be determined up to larger strains before necking than in the no overlapping hydraulic bulge test. And as the die ellipticity ratio decreases, the flow stress curves tend to move away from the curve obtained by circular (b/a=1) bulging test. Meanwhile, the flow property of the target sheet can be improved by choosing higher strength coefficient K, larger work hardening exponent n and proper thickness of the overlapping sheet.展开更多
The hot isostatic pressing-diffusion bonding(HIP-DB)was proposed to achieve the joining of CuAgZn and GH909 directly without an interlayer.The microstructure of joint was characterized by scanning electron microscope(...The hot isostatic pressing-diffusion bonding(HIP-DB)was proposed to achieve the joining of CuAgZn and GH909 directly without an interlayer.The microstructure of joint was characterized by scanning electron microscope(SEM),energy dispersive spectrometer(EDS)and X-ray diffraction(XRD).The microhardness and shear strength were tested to investigate the mechanical properties of joint.The results showed that the interface was complete,and the joint was compact,uniform and free of unbonded defects.The maximum microhardness of joint was HV 443,higher than that of two base alloys,and the average shear strength of joint reached 172 MPa.It is concluded that a good metallurgical bonding between CuAgZn and GH909 can be obtained by HIP-DB with the process parameters of 700℃,150 MPa and 3 h.展开更多
As a result of the recently increasing demands on high-performance aero-engine,the machining accuracy of blade profile is becoming more stringent. However,in the current profile,precision milling,grinding or near-nets...As a result of the recently increasing demands on high-performance aero-engine,the machining accuracy of blade profile is becoming more stringent. However,in the current profile,precision milling,grinding or near-netshape technology has to undergo a tedious iterative error compensation. Thus,if the profile error area and boundary can be determined automatically and quickly,it will help to improve the efficiency of subsequent re-machining correction process. To this end,an error boundary intersection approach is presented aiming at the error area determination of complex profile,including the phaseⅠof cross sectional non-rigid registration based on the minimum error area and the phaseⅡof boundary identification based on triangular meshes intersection. Some practical cases are given to demonstrate the effectiveness and superiority of the proposed approach.展开更多
To get an optimal product of orthopaedic implant or regenerative medicine needs to follow trialand-error analyses to investigate suitable product’s material,structure,mechanical properites etc.The whole process from ...To get an optimal product of orthopaedic implant or regenerative medicine needs to follow trialand-error analyses to investigate suitable product’s material,structure,mechanical properites etc.The whole process from in vivo tests to clinical trials is expensive and time-consuming.Computational model is seen as a useful analysis tool to make the product development.A series of models for simulating tissue engineering process from cell attachment to tissue regeneration are reviewed.The challenging is that models for simulating tissue engineering processes are developed separately.From cell to tissue regeneration,it would go through blood injection after moving out the defect;to cell disperse and attach on the scaffold;to proliferation,migration and differentiation;and to the final part-becoming mature tissues.This paper reviewed models that related to tissue engineering process,aiming to provide an opportunity for researchers to develop a mature model for whole tissue engineering process.This article focuses on the model analysis methods of cell adhesion,nutrient transport and cell proliferation,differentiation and migration in tissue engineering.In cell adhesion model,one of the most accurate method is to use discrete phase model to govern cell movement and use Stanton-Rutland model for simulating cell attachment.As for nutrient transport model,numerical model coupling with volume of fluid model and species transport model together is suitable for predicting nutrient transport process.For cell proliferation,differentiation and migration,finite element method with random-walk algorithm is one the most advanced way to simulate these processes.Most of the model analysis methods require further experiments to verify the accuracy and effectiveness.Due to the lack of technology to detect the rate of nutrient diffusion,there are especially few researches on model analysis methods in the area of blood coagulation.Therefore,there is still a lot of work to be done in the research of the whole process model method of tissue engineering.In the future,the numerical model would be seen as an optimal way to investigate tissue engineering products bioperformance and also enable to optimize the parameters and material types of the tissue engineering products.展开更多
Ti6Al4V alloy manufactured by electron powder bed fusion(EPBF)was separately heat-treated by stress-relief annealing at 600℃,annealing at 800℃,and solid solution at 920℃ for 1 h.Then,the friction and wear tests wer...Ti6Al4V alloy manufactured by electron powder bed fusion(EPBF)was separately heat-treated by stress-relief annealing at 600℃,annealing at 800℃,and solid solution at 920℃ for 1 h.Then,the friction and wear tests were conducted on the samples before and after heat treatment to analyze the properties and mechanism of friction and wear behavior.Results show that the sample annealed at 600℃ for 1 h has the optimal wear resistance,and the wear mass loss reduces by 44%.The sample annealed at 800℃ for 1 h possesses the optimal anti-friction performance,and the coefficient of friction reduces by 14%.This research provides a simple heat treatment method to improve the friction and wear resistance of Ti6Al4V alloy manufactured by EPBF.展开更多
The aim of this study was to prepare pulsatile release tablets which provide different drug delayed-release time and realize personalized administration according to the needs of patients.Fused deposition modeling(FDM...The aim of this study was to prepare pulsatile release tablets which provide different drug delayed-release time and realize personalized administration according to the needs of patients.Fused deposition modeling(FDM)3D printing technology was introduced into the field of pharmaceutics in this study,and the feasibility to prepare core-shell pulsatile release tablets was explored by combing 3D printing technology with the traditional manufacturing technology.The core of the pulsatile tablets was a commercial tablet obtained from the traditional technology,and the drug-free shell was prepared by the FDM 3D printing technology.Three kinds of tablet shells were designed using different parameters.Furthermore,the morphology,size,weight,hardness,and in vitro drug release of the 3D printed famotidine pusatile tablets were characterized and evaluated.The results showed that the 3D printed tablets appeared intact without any defects.Different parameters of outer shell affected the size,weight,hardness,and in vitro drug release of the tablets.The tablets achieved a personalized delayed release time varying from 5 to 7 h in vitro.In this way,a new method for preparing pulsatile release tablets and a new way for the personalized administration of pulsatile tablets were explored in this study.展开更多
文摘The uniaxial tensile test of the 5A06-O aluminium−magnesium(Al−Mg)alloy sheet was performed in the temperature range of 20−300℃ to obtain the true stress−true strain curves at different temperatures and strain rates.The constitutive model of 5A06-O Al−Mg alloy sheet with the temperature range from 150 to 300℃ was established.Based on the test results,a unique finite element simulation platform for warm hydroforming of 5A06-O Al−Mg alloy was set up using the general finite element software MSC.Marc to simulate warm hydroforming of classic specimen,and a coupled thermo-mechanical finite element model for warm hydroforming of cylindrical cup was built up.Combined with the experiment,the influence of the temperature field distribution and loading conditions on the sheet formability was studied.The results show that the non-isothermal temperature distribution conditions can significantly improve the forming performance of the material.As the temperature increases,the impact of the punching speed on the forming becomes particularly obvious;the optimal values of the fluid pressure and blank holder force required for forming are reduced.
基金financial support provided by Beijing Aeronautical Manufacturing Technology Research Institutethe help provided by Science and Technology, China, on Power Beam Processes Laboratory at Beijing Aeronautical Manufacturing Technology Research Institute, China
文摘Solid-state bonding between pure titanium and Ti6Al4V(TC4)alloy was conducted by a new bonding method named as rigid restraint thermal self-compressing bonding.Effects of heating time on bonding interface,atom diffusion and mechanical properties of the joints were studied.Results show that atom diffusion between pure titanium and TC4 alloy significantly takes place during bonding.The diffusion depths of Al and V in pure titanium side are increased with increasing heating time.Due to the enhancement of atom diffusion,bond quality of the bonding interface is improved along with the increase of heating time.The heating time seems to have little effect on microhardness distribution across the joint.However,the tensile strength and ductility of the joint have close relation to heating time.Prolonging heating time can improve the tensile strength and ductility of the joint,especially the latter.When the heating time increases to 450 s,solid-state joint with good combination of strength and ductility is attained.
基金the National Natural Science Foundation of China(Nos.51975031,52075023,51635005)Defense Industrial Technology Development Program,China(No.JCKY2018601C207)。
文摘In order to clarify the influence of grain size on cyclic deformation response of superalloy sheets and springback behavior,cyclic loading-unloading and shearing tests were performed on the superalloy foils with 0.2 mm in thickness and diverse grain sizes.The results show that,the decline ratio of elastic modulus is weakened with increasing grain size,and the Bauschinger effect becomes evident with decreasing grain size.Meanwhile,U-bending test results determine that the springback is diminished with increasing grain size.The Chaboche,Anisotropic Nonlinear Kinematic(ANK)and Yoshida-Uemori(Y-U)models were utilized to fit the shear stress-strain curves of specimens.It is found that Y-U model is sufficient of predicting the springback.However,the prediction accuracy is degraded with increasing grain size.
基金Project(51775023)supported by the National Natural Science Foundation of ChinaProject(YWF-18-BJ-J-75)supported by the Fundamental Research Funds for the Central Universities,China
文摘The influence of initial groove angle on strain rate inside and outside groove of Ti6Al4V alloy was investigated.Based on the evolution of strain rate inside and outside groove,the effect of strain rate difference on the evolution of normal stress and effective stress inside and outside groove was also analyzed.The results show that when linear loading path changes from uniaxial tension to equi-biaxial tension,the initial groove angle plays a weaker role in the evolution of strain rate in the M-K model.Due to the constraint of force equilibrium between inside and outside groove,the strain rate difference makes the normal stress inside groove firstly decrease and then increase during calculation,which makes the prediction algorithm of forming limit convergent at elevated temperature.The decrease of normal stress inside groove is mainly caused by high temperature softening effect and the rotation of groove,while the increase of normal stress inside groove is mainly due to strain rate hardening effect.
基金the National Natural Science Foundation of China(No.51675029).
文摘The Ti−6Al−4V(TC4)alloy powder and forged solid were diffusion bonded by hot isostatic pressing(HIP)to fabricate a powder−solid part.The microstructure of the powder−solid part was observed by scanning electron microscope(SEM).The microhardness and tensile tests were conducted to investigate the mechanical properties.The results showed that the powder compact was near-fully dense,and the powder/solid interface was tight and complete.The microhardness of the interface was higher than that of the powder compact and solid.The fractures of all powder−solid tensile specimens were on the solid side rather than at the interface,which indicated that a good interfacial strength was obtained.The tensile strength and elongation of the powder compact were higher than those of the solid.It is concluded that the HIP process can successfully fabricate high-quality Ti−6Al−4V powder−solid parts,which provides a novel near net shape technology for titanium alloys.
基金the financial support from the National Natural Science Foundation of China (Nos. 51675030, 51871010, 52005022)Shanghai Aerospace Scienceand Technology Innovation Fund, China (No. SAST2020-117)。
文摘The novel Ni-based brazing filler was used to join C/C composites.When brazing temperature increased from 1080 to 1100°C,the wetting angle decreased from 23°to 14°,and the brazing filler had good wettability on the surface of C/C composites.The brazing seam of the brazed joint consisted of Ni(s,s)and Cr_(3)C_(2) phases.As brazing temperature increased,lots of Cr_(3)C_(2) phases were generated at the bonding interface,and the thick reaction layer was formed.When brazing temperature was 1120°C,the shear strength of C/C joint reached the maximum value of 31.5 MPa.The fracture path extended in the C/C matrix close to the bonding interface.
基金Project(2014ZX04002041)supported by the National Science and Technology Major Project,ChinaProject(51175024)supported by the National Natural Science Foundation of China
文摘A novel experimental approach was presented, namely the overlapping elliptical bulge test, which can load and research thickness normal stress. Theoretical analysis model of the overlapping elliptical bulging was described, the equivalent stress?strain curves of target sheets with different ellipticity ratios were determined experimentally, and influences of the material performance and thickness of overlapping sheets on the flow property of the target sheet were also researched. The results show that, in the overlapping hydraulic bulge test, the equivalent stress?strain curve can be determined up to larger strains before necking than in the no overlapping hydraulic bulge test. And as the die ellipticity ratio decreases, the flow stress curves tend to move away from the curve obtained by circular (b/a=1) bulging test. Meanwhile, the flow property of the target sheet can be improved by choosing higher strength coefficient K, larger work hardening exponent n and proper thickness of the overlapping sheet.
基金The authors are grateful for the financial support from the Advanced Space Propulsion Technology Laboratory Open Fund,China(LabASP-2018-16).
文摘The hot isostatic pressing-diffusion bonding(HIP-DB)was proposed to achieve the joining of CuAgZn and GH909 directly without an interlayer.The microstructure of joint was characterized by scanning electron microscope(SEM),energy dispersive spectrometer(EDS)and X-ray diffraction(XRD).The microhardness and shear strength were tested to investigate the mechanical properties of joint.The results showed that the interface was complete,and the joint was compact,uniform and free of unbonded defects.The maximum microhardness of joint was HV 443,higher than that of two base alloys,and the average shear strength of joint reached 172 MPa.It is concluded that a good metallurgical bonding between CuAgZn and GH909 can be obtained by HIP-DB with the process parameters of 700℃,150 MPa and 3 h.
基金supported by the Aeronautical Science Foundation of China (No.20200016112001)。
文摘As a result of the recently increasing demands on high-performance aero-engine,the machining accuracy of blade profile is becoming more stringent. However,in the current profile,precision milling,grinding or near-netshape technology has to undergo a tedious iterative error compensation. Thus,if the profile error area and boundary can be determined automatically and quickly,it will help to improve the efficiency of subsequent re-machining correction process. To this end,an error boundary intersection approach is presented aiming at the error area determination of complex profile,including the phaseⅠof cross sectional non-rigid registration based on the minimum error area and the phaseⅡof boundary identification based on triangular meshes intersection. Some practical cases are given to demonstrate the effectiveness and superiority of the proposed approach.
基金supported by the Versus Arthritis Research UK(Grant No:21977)European Commission via a H2020-MSCA-RISE programme(BAMOS,Grant No:734156)+1 种基金Innovative UK via Newton Fund(Grant No:102872)Engineering and Physical Science Research Council(EPSRC)via DTP CASE programme(Grant No:EP/T517793/1)。
文摘To get an optimal product of orthopaedic implant or regenerative medicine needs to follow trialand-error analyses to investigate suitable product’s material,structure,mechanical properites etc.The whole process from in vivo tests to clinical trials is expensive and time-consuming.Computational model is seen as a useful analysis tool to make the product development.A series of models for simulating tissue engineering process from cell attachment to tissue regeneration are reviewed.The challenging is that models for simulating tissue engineering processes are developed separately.From cell to tissue regeneration,it would go through blood injection after moving out the defect;to cell disperse and attach on the scaffold;to proliferation,migration and differentiation;and to the final part-becoming mature tissues.This paper reviewed models that related to tissue engineering process,aiming to provide an opportunity for researchers to develop a mature model for whole tissue engineering process.This article focuses on the model analysis methods of cell adhesion,nutrient transport and cell proliferation,differentiation and migration in tissue engineering.In cell adhesion model,one of the most accurate method is to use discrete phase model to govern cell movement and use Stanton-Rutland model for simulating cell attachment.As for nutrient transport model,numerical model coupling with volume of fluid model and species transport model together is suitable for predicting nutrient transport process.For cell proliferation,differentiation and migration,finite element method with random-walk algorithm is one the most advanced way to simulate these processes.Most of the model analysis methods require further experiments to verify the accuracy and effectiveness.Due to the lack of technology to detect the rate of nutrient diffusion,there are especially few researches on model analysis methods in the area of blood coagulation.Therefore,there is still a lot of work to be done in the research of the whole process model method of tissue engineering.In the future,the numerical model would be seen as an optimal way to investigate tissue engineering products bioperformance and also enable to optimize the parameters and material types of the tissue engineering products.
基金National Natural Science Foundation of China(51975036)Guangdong Province Key R&D Project(2018B090904004)。
文摘Ti6Al4V alloy manufactured by electron powder bed fusion(EPBF)was separately heat-treated by stress-relief annealing at 600℃,annealing at 800℃,and solid solution at 920℃ for 1 h.Then,the friction and wear tests were conducted on the samples before and after heat treatment to analyze the properties and mechanism of friction and wear behavior.Results show that the sample annealed at 600℃ for 1 h has the optimal wear resistance,and the wear mass loss reduces by 44%.The sample annealed at 800℃ for 1 h possesses the optimal anti-friction performance,and the coefficient of friction reduces by 14%.This research provides a simple heat treatment method to improve the friction and wear resistance of Ti6Al4V alloy manufactured by EPBF.
文摘The aim of this study was to prepare pulsatile release tablets which provide different drug delayed-release time and realize personalized administration according to the needs of patients.Fused deposition modeling(FDM)3D printing technology was introduced into the field of pharmaceutics in this study,and the feasibility to prepare core-shell pulsatile release tablets was explored by combing 3D printing technology with the traditional manufacturing technology.The core of the pulsatile tablets was a commercial tablet obtained from the traditional technology,and the drug-free shell was prepared by the FDM 3D printing technology.Three kinds of tablet shells were designed using different parameters.Furthermore,the morphology,size,weight,hardness,and in vitro drug release of the 3D printed famotidine pusatile tablets were characterized and evaluated.The results showed that the 3D printed tablets appeared intact without any defects.Different parameters of outer shell affected the size,weight,hardness,and in vitro drug release of the tablets.The tablets achieved a personalized delayed release time varying from 5 to 7 h in vitro.In this way,a new method for preparing pulsatile release tablets and a new way for the personalized administration of pulsatile tablets were explored in this study.