The characteristics of temperatures, stresses and strains fields have been studied numerically for a titanium alloy sheet welded with an improved gas tungsten arc welding method, in which a trailing spot heat sink is ...The characteristics of temperatures, stresses and strains fields have been studied numerically for a titanium alloy sheet welded with an improved gas tungsten arc welding method, in which a trailing spot heat sink is introduced to control the welding stress and distortion. The impinging jet model is employed to describe the internee heat transfer between the cooling media and the top suufuce of the workpiece. The influcnee of the distance between arc and heat sink is investigated. Results show that there is an ideal range of distance. Using the ideal distance, a low stress and no distortion welding structure can be derived.展开更多
To prevent buckling distortions of thin-walled elements, Low Stress No Distortion welding techniques have been pioneered and developed for product engineering and component manufacturing of aerospace structures with m...To prevent buckling distortions of thin-walled elements, Low Stress No Distortion welding techniques have been pioneered and developed for product engineering and component manufacturing of aerospace structures with material thickness less than 4 mm. In this paper, the nature of Low Stress No Distortion (LSND) welding techniques using thermal tensioning effects is described and special emphases are given to the mechanism of localized thermal tensioning effect. The fundamental principle of Low Stress No Distortion welding is to create active in-process control of incompatible (inherent) plastic strains and stresses formation during welding to achieve distortion-free results implying that no post weld costly reworking operations for distortion correction is required. Finite element analysis is applied to predict and optimize the localized thermal tensioning technique with a trailing spot heat sink coupled to the welding heat source. Comparisons of the thermal elastic-plastic stress-strain cycles are given between conventional gas tungsten arc welding and GTAW with a trailing spot heat sink.展开更多
The microstructure of Ti-6-4 components produced by additive manufacturing suffers from the coarse and elongated prior-β grain,which leads to a decrease of the tensile behavior and the occurrence of anisotropy.To und...The microstructure of Ti-6-4 components produced by additive manufacturing suffers from the coarse and elongated prior-β grain,which leads to a decrease of the tensile behavior and the occurrence of anisotropy.To understand and control the grain evolution,a multiscale simulation is applied to investigate the relationship between the grain selection,growth orientation,and the molten pool morphology with the different deposition layer numbers and processing parameters.The accuracy of the simulation is validated by experiments in both qualitative and quantitative ways.Results show that when the grain with unfavorable orientation loses the competitive growth with its neighbors,there will be a great chance that the blocked grain is eliminated in the following layer-and-layer deposition,which leads to the increase of the grain width.The size of the molten pool increases remarkably as the layer number increases,which lays a heavy burden on the stability of the molten pool.The analytical relationship between the molten pool morphology and the grain growth orientation is also deduced.The flat molten pool causes the grains with the <001> direction close to the building direction to have greater survival potential.Besides,decreasing the line power energy shows little effect on the stability of the molten pool and the grain growth orientation,especially when the deposited layer number is large.The revealing mechanisms will help in understanding and further controlling the grain evolution.展开更多
Aiming at the surface integrity of titanium alloy Ti-6Al-4V in high speed side milling, a series of side mill- ing tests were carried out with uncoated carbide milling cutter at various milling speeds. Surface roughne...Aiming at the surface integrity of titanium alloy Ti-6Al-4V in high speed side milling, a series of side mill- ing tests were carried out with uncoated carbide milling cutter at various milling speeds. Surface roughness, residual stress, subsurface microstructure and microhardness variations were investigated. The surface roughness measurement results present that the milling speed from 80 to 120 m/min fails to produce better and more stable roughness values compared with the result obtained from 320 to 380 m/min. The residual stresses in the feed direction and axial depth of cut direction are in similar trends for the two milling speed levels mentioned above. Moreover, the residual stress pro- duced at 320 to 380 m/min is lower and more stable than that at 80 to 120 m/min. The microstructure analysis shows that the volume of β phase in the near surface becomes smaller and the deformation of β phase in the near surface be- comes obvious with the increase of the milling speed. Subsurface microhardness variation was observed down to 200 μm below the machined surface at 80 to 120 m/min and down to 160 μm at 320 to 380 m/min. It is concluded that better surface integrity and higher material removal rate can be obtained at 320 to 380 m/min than at 80 to 120 m/min.展开更多
The microstructure and mechanical properties of friction stir welded 2. 5 mm 7050-T7451 aluminum alloy natural aging 72 h and 17 520 h were investigated, respectively. The uniaxial tensile test showed that yield stren...The microstructure and mechanical properties of friction stir welded 2. 5 mm 7050-T7451 aluminum alloy natural aging 72 h and 17 520 h were investigated, respectively. The uniaxial tensile test showed that yield strength, tensile strength and elongation of the joints 17 520 h natural aging were about 20%, 12% and 24% higher than those joints natural aging 72 h. Hardness profile of natural aging 17 520 h joint witnessed significant enhancement in nugget zone, compared with 72 h natural aging. Differential scanning calorimetry ( DSC ) and transmission electron microscopy (TEM) test revealed that more Guinier-Preston zone, η' and 71 phase emerged in nugget zone as natural aging duration increased, high density of dislocation located within grain boundary in nugget zone of joints natural aging 72 h. It is concluded that natural aging was feasible to enhalwe strength and plasticity of FSW joints simultaneously.展开更多
TiAl-based alloys sheet with thickness of 0.3-0.4 mm as well as dimension of 150 mm×100 mm was fabricated successfully by using electron beam-physical vapor deposition(EB-PVD) method. The microscopic morphology a...TiAl-based alloys sheet with thickness of 0.3-0.4 mm as well as dimension of 150 mm×100 mm was fabricated successfully by using electron beam-physical vapor deposition(EB-PVD) method. The microscopic morphology and phase composition of specimens in various states were analyzed by atomic force microscope(AFM), scanning electron microscope(SEM) and X-ray diffractometer(XRD), respectively. The results indicate that the as-deposited TiAl-based alloys sheet has good surface quality and is composed of γ, α2 and τ phase. There is natural delamination inside the sheet, of which the microstructure is columnar crystal, and the component shows a gradient change along the normal direction of substrate. After the vacuum hot pressing treatment and subsequent homogenization treatment, the columnar crystal transforms into the coarse fully lamellar microstructure, the delamination phenomenon and τ phase disappear, α2 phase decreases obviously, and the composition tends to uniformization.展开更多
Solid-state bonding between pure titanium and Ti6Al4V(TC4)alloy was conducted by a new bonding method named as rigid restraint thermal self-compressing bonding.Effects of heating time on bonding interface,atom diffusi...Solid-state bonding between pure titanium and Ti6Al4V(TC4)alloy was conducted by a new bonding method named as rigid restraint thermal self-compressing bonding.Effects of heating time on bonding interface,atom diffusion and mechanical properties of the joints were studied.Results show that atom diffusion between pure titanium and TC4 alloy significantly takes place during bonding.The diffusion depths of Al and V in pure titanium side are increased with increasing heating time.Due to the enhancement of atom diffusion,bond quality of the bonding interface is improved along with the increase of heating time.The heating time seems to have little effect on microhardness distribution across the joint.However,the tensile strength and ductility of the joint have close relation to heating time.Prolonging heating time can improve the tensile strength and ductility of the joint,especially the latter.When the heating time increases to 450 s,solid-state joint with good combination of strength and ductility is attained.展开更多
A crystal plasticity finite element(CPFE)model was established and 2D simulations were carried out to study the relationship between microvoids and the microplasticity deformation behavior of the dual-phase titanium a...A crystal plasticity finite element(CPFE)model was established and 2D simulations were carried out to study the relationship between microvoids and the microplasticity deformation behavior of the dual-phase titanium alloy under high cyclic loading.Results show that geometrically necessary dislocations(GND)tend to accumulate around the microvoids,leading to an increment of average GND density.The influence of curvature in the tip plastic zone(TPZ)on GND density is greater than that of the size of the microvoid.As the curvature in TPZ and the size of the microvoid increase,the cumulative shear strain(CSS)in the primaryα,secondaryα,andβphases increases.Shear deformation in the prismatic slip system is dominant in the primaryαphase.As the distance between the microvoids increases,the interactive influence of the microvoids on the cumulative shear strain decreases.展开更多
Thermal self-compressing bonding(TSCB) is a new solid-state bonding method pioneered by the authors. With electron beam as the non-melted heat source, previous experimental study performed on titanium alloys has prove...Thermal self-compressing bonding(TSCB) is a new solid-state bonding method pioneered by the authors. With electron beam as the non-melted heat source, previous experimental study performed on titanium alloys has proved the feasibility of TSCB. However, the thermal stress–strain process during bonding, which is of very important significance in revealing the mechanism of TSCB, was not analysed. In this paper, finite element analysis method is adopted to numerically study the thermal elasto-plastic stress–strain cycle of thermal self-compressing bonding. It is found that due to the localized heating, a non-uniform temperature distribution is formed during bonding, with the highest temperature existed on the bond interface. The expansion of high temperature materials adjacent to the bond interface are restrained by surrounding cool materials and rigid restraints, and thus an internal elasto-plastic stress–strain field is developed by itself which makes the bond interface subjected to thermal compressive action. This thermal self-compressing action combined with the high temperature on the bond interface promotes the atom diffusion across the bond interface to produce solid-state joints. Due to the relatively large plastic deformation, rigid restraint TSCB obtains sound joints in relatively short time compared to diffusion bonding.展开更多
The laser beam welding of BT20 titanium alloy was conducted to investigate the weld shape, microstructures and properties. The full penetration weld characteristics produced by CO_2 laser and by YAG laser were compare...The laser beam welding of BT20 titanium alloy was conducted to investigate the weld shape, microstructures and properties. The full penetration weld characteristics produced by CO_2 laser and by YAG laser were compared. The results show that the full penetration weld of YAG laser welding closes to “X” shape, and weld of CO_2 laser welding is “nail-head” shape. Those result from special heating mode of laser deep penetration welding. The tension strength of CO_2 laser and YAG laser joints equal to that of the base metal, but the former has better ductility. All welds consist mainly of the acicular α phase and a few β phase in microstructure. The dendritic crystal of CO_2 laser weld is a little finer than YAG laser weld. According the research CO_2 laser is better than YAG laser for welding of BT20 titanium alloy.展开更多
This paper introduces a brazing process between Al2O3 ceramic and Invar alloy.Al2O3 can be brazed with Invar effectively.The interfacial structure of Al2O3/Invar joint can be expressed as:Invar/Ag(s,s)+Cu(s,s)+...This paper introduces a brazing process between Al2O3 ceramic and Invar alloy.Al2O3 can be brazed with Invar effectively.The interfacial structure of Al2O3/Invar joint can be expressed as:Invar/Ag(s,s)+Cu(s,s)+Fe2Ti(zone Ⅰ)/Ag(s,s)+Cu(s,s)+Fe2Ti+NiTi+Cu3Ti(zone Ⅱ)/Ag(s,s)+Cu(s,s)+Cu2Ti+Al(s,s)+TiC+TiO(zone Ⅲ)/Al2O3.The maximum shear strength of 139 MPa was measured for as-brazed Al2O3/Invar joint brazed at 850℃ for 25 min or 900℃ for 15 min.展开更多
Microstructure of transient liquid phase( TLP) diffusion bonded a third generation single crystal superalloy joint was investigated using scanning electron microscopy( SEM),and mechanical properties test of joint was ...Microstructure of transient liquid phase( TLP) diffusion bonded a third generation single crystal superalloy joint was investigated using scanning electron microscopy( SEM),and mechanical properties test of joint was carried out,for obtaining relationship between microstructure and mechanical properties of joint. The results showed that the joint contained bonding zone and base metal. The diffusion zone was obviously observed. When it was not finished for isothermal solidification process,the bonding zone would contain isothermal solidification zone and rapid solidification zone. Metallographic examination revealed that isothermal solidification zone was consisted of γ and γ' phase. Rapid solidification zone was consisted of two different structures,which were ternary eutectic of borides,γ and γ' phase developing at the edge of joint,binary eutectic of γ and γ' phase appearing in the portion of joint. When it was not enough for homogenization process under the condition of finishing isothermal solidification process,the bonding zone would contain isothermal solidification zone and borides at the interface. Under the conditions of relatively high welding temperature and long welding time,average tensile strength of joint was equivalent to that of parent material.展开更多
Cold-rolled 2024-T3 sheet alloy was subjected to bobbin-tool friction stir welding (BTFSW). The microstructural characteristics and mechanical properties of the nugget zone in the as-welded state were investigated. ...Cold-rolled 2024-T3 sheet alloy was subjected to bobbin-tool friction stir welding (BTFSW). The microstructural characteristics and mechanical properties of the nugget zone in the as-welded state were investigated. The results show that the equiaxed grain size of BTFSW 2024-T3 alloy decreases from 7.6 to 2.8 μm as the welding speed is increased from 80 to 120 mm/min; in addition, fine grains are generated in the nugget zone and the size distribution is non-uniform. All A12CuMg (S') precipitates dissolve into the A1 matrix, whereas Mn-rich phases confirmed as T phases (Al20CuEMn3, A16Mn, or AlaMn) remain unchanged. The optimized parameters for BTFSW are veri- fied as the rotation speed of 350 r/min and the travel speed of 100 mm/min. The variations in precipitation and dislocation play more impor- tant roles than grain size in the nugget zone with respect to influencing the mechanical properties during the BTFSW process. After the BTFSW process, the fracture mode of base material 2024-T3 alloy transforms from ductile rupture to ductile-brittle mixed fi'acture.展开更多
A three-dimensional finite volume model was established by the ANSYS FLUENT software to simulate the material flow behavior during the friction stir spot welding (FSSW) process. Effects of the full-threaded pin and ...A three-dimensional finite volume model was established by the ANSYS FLUENT software to simulate the material flow behavior during the friction stir spot welding (FSSW) process. Effects of the full-threaded pin and the reverse-threaded pin on the material flow behavior were mainly discussed. Results showed that the biggest material flow velocity appeared at the outer edge of the tool shoulder. The velocity value became smaller with the increase of the distance away from the tool surface. In general, material flows downwards along the pin thread when the full-threaded pin is used. Meanwhile, both the materials of the upper and the lower plates flow towards the lap interface along the pin thread when the reverse-threaded pin is used. The numerical simulation results were investigated by experiment, in which 2A12 aluminum alloy was used as the research object. The effective sheet thickness (EST) and stir zone (SZ) width of the joint by the reverse-threaded pin were much bigger than those by the full-threaded pin. Accordingly, cross tension failure load of the joint by the reverse-threaded pin is 23% bigger than the joint by the full-threaded pin.展开更多
In this paper, laser induced plasma signals were analyzed during keyhole welding through three methods. According to the results, the relativity between optical and acoustic signals of plasma is shown when welds are i...In this paper, laser induced plasma signals were analyzed during keyhole welding through three methods. According to the results, the relativity between optical and acoustic signals of plasma is shown when welds are in full-penetration, or partial-penetration and non-penetration.展开更多
Thin films of titanium carbide and amorphous hydrogenated carbon have been synthesized on titanium aluminium alloy substrates by PSII assisted MW-ECRCVD with a mirror field. The microstructure, chemical composition an...Thin films of titanium carbide and amorphous hydrogenated carbon have been synthesized on titanium aluminium alloy substrates by PSII assisted MW-ECRCVD with a mirror field. The microstructure, chemical composition and mechanical property were investigated. Using XPS and TEM, the films were identified to be a-C:H film containing TiC nanometre grains (namely, the so-called nanocomposite structure). The size of TiC grains of nanocomposite TiC/DLC film is about 5 nm. The nanocomposite structure has obvious improvement in the mechanical properties of DLC film. The hardness of a-C:H film with Ti is enhanced to 34 G Pa~ while that of a-C:H film without Ti is about 12 G Pa, and the coherent strength is also obviously enhanced at the critical load of about 35N.展开更多
The surface nanostructures of commercial pure titanium was realized by the modified shot peening equipment commonly used in industry through the special treatment process. The results show that high-energy-shot-peenin...The surface nanostructures of commercial pure titanium was realized by the modified shot peening equipment commonly used in industry through the special treatment process. The results show that high-energy-shot-peening(HESP) commonly used to prepare nanostructured surface layers can be achieved by the increase of pill size, pill speed, and treatment time in the commercial shot peening equipment. XRD, SEM and TEM were used to characterize the surface layer microstructure of treated specimens. The analytic results show that the main deformation mode of commercial pure Ti is twinning. At the beginning of deformation, the dislocations are formed and twins occur within or on plane, then twins in intersection plane appear, and at last the twin characteristics disappear in the surface layer after longer treatment time. The deformation layer depth increases with treatment time in a certain period when the pill size and speed are unchanged. And in the severe plastic deformation (SPD) layer in which the twins are not identified easily by using SEM, the nanocrystalline microstructures are found under TEM. The finest grain size in the surface layer is about 40 nm, and the depth of nanostructured layers is over 60 μm. The microhardness of the nanostructured surface layers is enhanced significantly after shot peening compared with that of the initial simple.展开更多
This paper was concerned with the tensile mechanics behavior of the composite π-joint under static tensile loading. The numerical strength analysis methodology was presented containing the basis assumption for the an...This paper was concerned with the tensile mechanics behavior of the composite π-joint under static tensile loading. The numerical strength analysis methodology was presented containing the basis assumption for the analysis, the material modeling, and the selected element type. It was assumed that the composite ply had transverse isotropic material properties and the adhesive had linear elastic properties. With the goal of the strength analysis to determine the onset of the damage initiation and the ultimate failure load, two stiffness degradation models were discussed and a modified maximum stress failure criteria was presented. To verify the numerical model, a pull-off test scheme was performed and the experimental data of five specimens were given. The experimental results indicate that the damage initiation location and the failure load were consistent with numerical predictions and verified the feasibility of the numerical model.展开更多
The CO2 laser welding of BT20 titanium alloy and Ti-23Al-17Nb titanium aluminide was conducted to investigate into the porosity in titanium alloy weld. The results show that there are two sorts of porosities observed ...The CO2 laser welding of BT20 titanium alloy and Ti-23Al-17Nb titanium aluminide was conducted to investigate into the porosity in titanium alloy weld. The results show that there are two sorts of porosities observed in welds of titanium alloy laser welding based on the microscopic characteristics of the porosities. One is the metallurgical porosity with round and smooth inner wall, which results from the surface contamination. The other is the processing porosity with irregular and rough inner wall that displays the trace of the pool flowing, which results from the ruffle on the keyhole wall gathering together locally and closing down the gas in the keyhole into bubbles because of the keyhole fluctuating. The CO2 laser welding could break down easily the surface oxide film and produce little metallurgical porosity, but produces easily processing porosity when partial penetration or unstable-full penetration laser welding is conducted, which always occurs in the center of weld.展开更多
Laser shock processing(LSP),also known as laser peening,is a novel surface treatment technique in the past few years.Compressive residual stresses which imparted by LSP are very important for improving fatigue,corro...Laser shock processing(LSP),also known as laser peening,is a novel surface treatment technique in the past few years.Compressive residual stresses which imparted by LSP are very important for improving fatigue,corrosion and wea rresistance of metals.Finite element analysis(FEA) simulation using ABAQUS software has been applied to predict residualstresses induced by LSP on Ti-6Al-4V titanium alloy with laser pulse duration 30 ns and water confined ablation mode.The residual stress field generated by different shape laser spots was studied,and the square laser spot is shown the most suitability for avoiding stress lack phenomenon and overlapping LSP.Surface residual stresses and plastically affected depth within single square spot both increased with the increase of laser intensity and laser shock times.Furthermore,compared with circle and ellipse spot,the residual stress distribution in overlapping square spots is very uniform only with small overlapping ratio.LSP with square spot can process advantageous residual stress field,and this technique will be used widely.展开更多
基金This work is supported by The Aeronautical Funds of China
文摘The characteristics of temperatures, stresses and strains fields have been studied numerically for a titanium alloy sheet welded with an improved gas tungsten arc welding method, in which a trailing spot heat sink is introduced to control the welding stress and distortion. The impinging jet model is employed to describe the internee heat transfer between the cooling media and the top suufuce of the workpiece. The influcnee of the distance between arc and heat sink is investigated. Results show that there is an ideal range of distance. Using the ideal distance, a low stress and no distortion welding structure can be derived.
文摘To prevent buckling distortions of thin-walled elements, Low Stress No Distortion welding techniques have been pioneered and developed for product engineering and component manufacturing of aerospace structures with material thickness less than 4 mm. In this paper, the nature of Low Stress No Distortion (LSND) welding techniques using thermal tensioning effects is described and special emphases are given to the mechanism of localized thermal tensioning effect. The fundamental principle of Low Stress No Distortion welding is to create active in-process control of incompatible (inherent) plastic strains and stresses formation during welding to achieve distortion-free results implying that no post weld costly reworking operations for distortion correction is required. Finite element analysis is applied to predict and optimize the localized thermal tensioning technique with a trailing spot heat sink coupled to the welding heat source. Comparisons of the thermal elastic-plastic stress-strain cycles are given between conventional gas tungsten arc welding and GTAW with a trailing spot heat sink.
基金supported by the National Key Research and Development Program of China (No. 2017YFB1103700)the National Natural Science Foundation of China (No. 51575304 and No. 51674153)。
文摘The microstructure of Ti-6-4 components produced by additive manufacturing suffers from the coarse and elongated prior-β grain,which leads to a decrease of the tensile behavior and the occurrence of anisotropy.To understand and control the grain evolution,a multiscale simulation is applied to investigate the relationship between the grain selection,growth orientation,and the molten pool morphology with the different deposition layer numbers and processing parameters.The accuracy of the simulation is validated by experiments in both qualitative and quantitative ways.Results show that when the grain with unfavorable orientation loses the competitive growth with its neighbors,there will be a great chance that the blocked grain is eliminated in the following layer-and-layer deposition,which leads to the increase of the grain width.The size of the molten pool increases remarkably as the layer number increases,which lays a heavy burden on the stability of the molten pool.The analytical relationship between the molten pool morphology and the grain growth orientation is also deduced.The flat molten pool causes the grains with the <001> direction close to the building direction to have greater survival potential.Besides,decreasing the line power energy shows little effect on the stability of the molten pool and the grain growth orientation,especially when the deposited layer number is large.The revealing mechanisms will help in understanding and further controlling the grain evolution.
基金National High Technology Research and Development Program of China ( "863"Program, No.2008AA042509)
文摘Aiming at the surface integrity of titanium alloy Ti-6Al-4V in high speed side milling, a series of side mill- ing tests were carried out with uncoated carbide milling cutter at various milling speeds. Surface roughness, residual stress, subsurface microstructure and microhardness variations were investigated. The surface roughness measurement results present that the milling speed from 80 to 120 m/min fails to produce better and more stable roughness values compared with the result obtained from 320 to 380 m/min. The residual stresses in the feed direction and axial depth of cut direction are in similar trends for the two milling speed levels mentioned above. Moreover, the residual stress pro- duced at 320 to 380 m/min is lower and more stable than that at 80 to 120 m/min. The microstructure analysis shows that the volume of β phase in the near surface becomes smaller and the deformation of β phase in the near surface be- comes obvious with the increase of the milling speed. Subsurface microhardness variation was observed down to 200 μm below the machined surface at 80 to 120 m/min and down to 160 μm at 320 to 380 m/min. It is concluded that better surface integrity and higher material removal rate can be obtained at 320 to 380 m/min than at 80 to 120 m/min.
文摘The microstructure and mechanical properties of friction stir welded 2. 5 mm 7050-T7451 aluminum alloy natural aging 72 h and 17 520 h were investigated, respectively. The uniaxial tensile test showed that yield strength, tensile strength and elongation of the joints 17 520 h natural aging were about 20%, 12% and 24% higher than those joints natural aging 72 h. Hardness profile of natural aging 17 520 h joint witnessed significant enhancement in nugget zone, compared with 72 h natural aging. Differential scanning calorimetry ( DSC ) and transmission electron microscopy (TEM) test revealed that more Guinier-Preston zone, η' and 71 phase emerged in nugget zone as natural aging duration increased, high density of dislocation located within grain boundary in nugget zone of joints natural aging 72 h. It is concluded that natural aging was feasible to enhalwe strength and plasticity of FSW joints simultaneously.
基金Project(90405016) supported by the National Natural Science Foundation of China
文摘TiAl-based alloys sheet with thickness of 0.3-0.4 mm as well as dimension of 150 mm×100 mm was fabricated successfully by using electron beam-physical vapor deposition(EB-PVD) method. The microscopic morphology and phase composition of specimens in various states were analyzed by atomic force microscope(AFM), scanning electron microscope(SEM) and X-ray diffractometer(XRD), respectively. The results indicate that the as-deposited TiAl-based alloys sheet has good surface quality and is composed of γ, α2 and τ phase. There is natural delamination inside the sheet, of which the microstructure is columnar crystal, and the component shows a gradient change along the normal direction of substrate. After the vacuum hot pressing treatment and subsequent homogenization treatment, the columnar crystal transforms into the coarse fully lamellar microstructure, the delamination phenomenon and τ phase disappear, α2 phase decreases obviously, and the composition tends to uniformization.
基金financial support provided by Beijing Aeronautical Manufacturing Technology Research Institutethe help provided by Science and Technology, China, on Power Beam Processes Laboratory at Beijing Aeronautical Manufacturing Technology Research Institute, China
文摘Solid-state bonding between pure titanium and Ti6Al4V(TC4)alloy was conducted by a new bonding method named as rigid restraint thermal self-compressing bonding.Effects of heating time on bonding interface,atom diffusion and mechanical properties of the joints were studied.Results show that atom diffusion between pure titanium and TC4 alloy significantly takes place during bonding.The diffusion depths of Al and V in pure titanium side are increased with increasing heating time.Due to the enhancement of atom diffusion,bond quality of the bonding interface is improved along with the increase of heating time.The heating time seems to have little effect on microhardness distribution across the joint.However,the tensile strength and ductility of the joint have close relation to heating time.Prolonging heating time can improve the tensile strength and ductility of the joint,especially the latter.When the heating time increases to 450 s,solid-state joint with good combination of strength and ductility is attained.
基金the National Key Research and Development Program of China(No.2021YFB3702603).
文摘A crystal plasticity finite element(CPFE)model was established and 2D simulations were carried out to study the relationship between microvoids and the microplasticity deformation behavior of the dual-phase titanium alloy under high cyclic loading.Results show that geometrically necessary dislocations(GND)tend to accumulate around the microvoids,leading to an increment of average GND density.The influence of curvature in the tip plastic zone(TPZ)on GND density is greater than that of the size of the microvoid.As the curvature in TPZ and the size of the microvoid increase,the cumulative shear strain(CSS)in the primaryα,secondaryα,andβphases increases.Shear deformation in the prismatic slip system is dominant in the primaryαphase.As the distance between the microvoids increases,the interactive influence of the microvoids on the cumulative shear strain decreases.
基金Supported by National Natural Science Foundation of China(Grant No.51705491)
文摘Thermal self-compressing bonding(TSCB) is a new solid-state bonding method pioneered by the authors. With electron beam as the non-melted heat source, previous experimental study performed on titanium alloys has proved the feasibility of TSCB. However, the thermal stress–strain process during bonding, which is of very important significance in revealing the mechanism of TSCB, was not analysed. In this paper, finite element analysis method is adopted to numerically study the thermal elasto-plastic stress–strain cycle of thermal self-compressing bonding. It is found that due to the localized heating, a non-uniform temperature distribution is formed during bonding, with the highest temperature existed on the bond interface. The expansion of high temperature materials adjacent to the bond interface are restrained by surrounding cool materials and rigid restraints, and thus an internal elasto-plastic stress–strain field is developed by itself which makes the bond interface subjected to thermal compressive action. This thermal self-compressing action combined with the high temperature on the bond interface promotes the atom diffusion across the bond interface to produce solid-state joints. Due to the relatively large plastic deformation, rigid restraint TSCB obtains sound joints in relatively short time compared to diffusion bonding.
文摘The laser beam welding of BT20 titanium alloy was conducted to investigate the weld shape, microstructures and properties. The full penetration weld characteristics produced by CO_2 laser and by YAG laser were compared. The results show that the full penetration weld of YAG laser welding closes to “X” shape, and weld of CO_2 laser welding is “nail-head” shape. Those result from special heating mode of laser deep penetration welding. The tension strength of CO_2 laser and YAG laser joints equal to that of the base metal, but the former has better ductility. All welds consist mainly of the acicular α phase and a few β phase in microstructure. The dendritic crystal of CO_2 laser weld is a little finer than YAG laser weld. According the research CO_2 laser is better than YAG laser for welding of BT20 titanium alloy.
文摘This paper introduces a brazing process between Al2O3 ceramic and Invar alloy.Al2O3 can be brazed with Invar effectively.The interfacial structure of Al2O3/Invar joint can be expressed as:Invar/Ag(s,s)+Cu(s,s)+Fe2Ti(zone Ⅰ)/Ag(s,s)+Cu(s,s)+Fe2Ti+NiTi+Cu3Ti(zone Ⅱ)/Ag(s,s)+Cu(s,s)+Cu2Ti+Al(s,s)+TiC+TiO(zone Ⅲ)/Al2O3.The maximum shear strength of 139 MPa was measured for as-brazed Al2O3/Invar joint brazed at 850℃ for 25 min or 900℃ for 15 min.
文摘Microstructure of transient liquid phase( TLP) diffusion bonded a third generation single crystal superalloy joint was investigated using scanning electron microscopy( SEM),and mechanical properties test of joint was carried out,for obtaining relationship between microstructure and mechanical properties of joint. The results showed that the joint contained bonding zone and base metal. The diffusion zone was obviously observed. When it was not finished for isothermal solidification process,the bonding zone would contain isothermal solidification zone and rapid solidification zone. Metallographic examination revealed that isothermal solidification zone was consisted of γ and γ' phase. Rapid solidification zone was consisted of two different structures,which were ternary eutectic of borides,γ and γ' phase developing at the edge of joint,binary eutectic of γ and γ' phase appearing in the portion of joint. When it was not enough for homogenization process under the condition of finishing isothermal solidification process,the bonding zone would contain isothermal solidification zone and borides at the interface. Under the conditions of relatively high welding temperature and long welding time,average tensile strength of joint was equivalent to that of parent material.
文摘Cold-rolled 2024-T3 sheet alloy was subjected to bobbin-tool friction stir welding (BTFSW). The microstructural characteristics and mechanical properties of the nugget zone in the as-welded state were investigated. The results show that the equiaxed grain size of BTFSW 2024-T3 alloy decreases from 7.6 to 2.8 μm as the welding speed is increased from 80 to 120 mm/min; in addition, fine grains are generated in the nugget zone and the size distribution is non-uniform. All A12CuMg (S') precipitates dissolve into the A1 matrix, whereas Mn-rich phases confirmed as T phases (Al20CuEMn3, A16Mn, or AlaMn) remain unchanged. The optimized parameters for BTFSW are veri- fied as the rotation speed of 350 r/min and the travel speed of 100 mm/min. The variations in precipitation and dislocation play more impor- tant roles than grain size in the nugget zone with respect to influencing the mechanical properties during the BTFSW process. After the BTFSW process, the fracture mode of base material 2024-T3 alloy transforms from ductile rupture to ductile-brittle mixed fi'acture.
基金This work is supported by the National Natural Science Foundation of China (No. 51204111 ), the Natural Science Foundation of Liaoning Province ( No. 2013024004 and No. 2014024008).
文摘A three-dimensional finite volume model was established by the ANSYS FLUENT software to simulate the material flow behavior during the friction stir spot welding (FSSW) process. Effects of the full-threaded pin and the reverse-threaded pin on the material flow behavior were mainly discussed. Results showed that the biggest material flow velocity appeared at the outer edge of the tool shoulder. The velocity value became smaller with the increase of the distance away from the tool surface. In general, material flows downwards along the pin thread when the full-threaded pin is used. Meanwhile, both the materials of the upper and the lower plates flow towards the lap interface along the pin thread when the reverse-threaded pin is used. The numerical simulation results were investigated by experiment, in which 2A12 aluminum alloy was used as the research object. The effective sheet thickness (EST) and stir zone (SZ) width of the joint by the reverse-threaded pin were much bigger than those by the full-threaded pin. Accordingly, cross tension failure load of the joint by the reverse-threaded pin is 23% bigger than the joint by the full-threaded pin.
文摘In this paper, laser induced plasma signals were analyzed during keyhole welding through three methods. According to the results, the relativity between optical and acoustic signals of plasma is shown when welds are in full-penetration, or partial-penetration and non-penetration.
文摘Thin films of titanium carbide and amorphous hydrogenated carbon have been synthesized on titanium aluminium alloy substrates by PSII assisted MW-ECRCVD with a mirror field. The microstructure, chemical composition and mechanical property were investigated. Using XPS and TEM, the films were identified to be a-C:H film containing TiC nanometre grains (namely, the so-called nanocomposite structure). The size of TiC grains of nanocomposite TiC/DLC film is about 5 nm. The nanocomposite structure has obvious improvement in the mechanical properties of DLC film. The hardness of a-C:H film with Ti is enhanced to 34 G Pa~ while that of a-C:H film without Ti is about 12 G Pa, and the coherent strength is also obviously enhanced at the critical load of about 35N.
基金Project(50171017) support by the National Natural Science Foundation of China project(2001101054) supported by the Science and Technology Foundation of Liaoning Province project(02H25008) supported by the Aeronautical Basic Science Foundation
文摘The surface nanostructures of commercial pure titanium was realized by the modified shot peening equipment commonly used in industry through the special treatment process. The results show that high-energy-shot-peening(HESP) commonly used to prepare nanostructured surface layers can be achieved by the increase of pill size, pill speed, and treatment time in the commercial shot peening equipment. XRD, SEM and TEM were used to characterize the surface layer microstructure of treated specimens. The analytic results show that the main deformation mode of commercial pure Ti is twinning. At the beginning of deformation, the dislocations are formed and twins occur within or on plane, then twins in intersection plane appear, and at last the twin characteristics disappear in the surface layer after longer treatment time. The deformation layer depth increases with treatment time in a certain period when the pill size and speed are unchanged. And in the severe plastic deformation (SPD) layer in which the twins are not identified easily by using SEM, the nanocrystalline microstructures are found under TEM. The finest grain size in the surface layer is about 40 nm, and the depth of nanostructured layers is over 60 μm. The microhardness of the nanostructured surface layers is enhanced significantly after shot peening compared with that of the initial simple.
文摘This paper was concerned with the tensile mechanics behavior of the composite π-joint under static tensile loading. The numerical strength analysis methodology was presented containing the basis assumption for the analysis, the material modeling, and the selected element type. It was assumed that the composite ply had transverse isotropic material properties and the adhesive had linear elastic properties. With the goal of the strength analysis to determine the onset of the damage initiation and the ultimate failure load, two stiffness degradation models were discussed and a modified maximum stress failure criteria was presented. To verify the numerical model, a pull-off test scheme was performed and the experimental data of five specimens were given. The experimental results indicate that the damage initiation location and the failure load were consistent with numerical predictions and verified the feasibility of the numerical model.
文摘The CO2 laser welding of BT20 titanium alloy and Ti-23Al-17Nb titanium aluminide was conducted to investigate into the porosity in titanium alloy weld. The results show that there are two sorts of porosities observed in welds of titanium alloy laser welding based on the microscopic characteristics of the porosities. One is the metallurgical porosity with round and smooth inner wall, which results from the surface contamination. The other is the processing porosity with irregular and rough inner wall that displays the trace of the pool flowing, which results from the ruffle on the keyhole wall gathering together locally and closing down the gas in the keyhole into bubbles because of the keyhole fluctuating. The CO2 laser welding could break down easily the surface oxide film and produce little metallurgical porosity, but produces easily processing porosity when partial penetration or unstable-full penetration laser welding is conducted, which always occurs in the center of weld.
基金Project supported by the Foundation of National Key Laboratory of Science and Technology on Power Beam Processing(Grant No.9140C4505020705)
文摘Laser shock processing(LSP),also known as laser peening,is a novel surface treatment technique in the past few years.Compressive residual stresses which imparted by LSP are very important for improving fatigue,corrosion and wea rresistance of metals.Finite element analysis(FEA) simulation using ABAQUS software has been applied to predict residualstresses induced by LSP on Ti-6Al-4V titanium alloy with laser pulse duration 30 ns and water confined ablation mode.The residual stress field generated by different shape laser spots was studied,and the square laser spot is shown the most suitability for avoiding stress lack phenomenon and overlapping LSP.Surface residual stresses and plastically affected depth within single square spot both increased with the increase of laser intensity and laser shock times.Furthermore,compared with circle and ellipse spot,the residual stress distribution in overlapping square spots is very uniform only with small overlapping ratio.LSP with square spot can process advantageous residual stress field,and this technique will be used widely.