The present work aims to study the influence of direct current and pulse current techniques as well as embedded SiC nanoparticles on the mechanical properties of the electrodeposited Ni-W coating.The electrodeposited ...The present work aims to study the influence of direct current and pulse current techniques as well as embedded SiC nanoparticles on the mechanical properties of the electrodeposited Ni-W coating.The electrodeposited coatings were studied for morphological,microstructural,mechanical,and scratch resistance properties using the surface roughness tester,scanning electron microscopy,energy-dispersive X-ray spectroscopy,X-ray diffraction,Vickers microhardness,and scratch tester.Application of pulse current exhibited relatively homogeneous and smooth surface of the coatings.A remarkable increment of microhardness was observed in both Ni-W and Ni-W-SiC coatings prepared under pulse current as compared to the direct current technique.Similarly,the scratch test revealed a considerable improvement in the scratch resistance behavior of the Ni-W alloy and the composite coatings from the pulsed current condition.Hence,the application of pulse current not only improved the surface-and microstructure-related properties but also enhanced the Vickers microhardness and scratch resistance properties of the coatings.In addition,the reduction in micro-cracks revealed the improvement in scratch resistance properties of the coatings due to the incorporated SiC nanoparticles into the Ni-W alloy matrix.展开更多
Ni-W-TiC composite coatings were prepared via electrodeposition technique by dispersing the different amount of TiC particles into the plating bath.The Ni-W and Ni-W-TiC composite coatings containing different concent...Ni-W-TiC composite coatings were prepared via electrodeposition technique by dispersing the different amount of TiC particles into the plating bath.The Ni-W and Ni-W-TiC composite coatings containing different concentrations of TiC particles were characterized by using the scanning electron microscope,X-ray diffraction technique,Vickers microhardness test,surface roughness test,and tribology test.The results show that the Ni-W coatings containing reinforced TiC particles have shown a typical FCC Ni-W crystal structure with significantly higher Vickers microhardness.The amount of dispersed TiC particles into the plating bath considerably affected codeposition weight percent of TiC into the Ni-W matrix,as revealed by the EDS analysis.Ni-W-TiC samples demonstrated the decreased abrasive wear as compared to Ni-W coating and no characteristic features observed for the adhesive wear.Similarly,an improvement in coefficient of friction was observed in Ni-W-TiC composite coating as compared to Ni-W coating.展开更多
基金financially supported by the PhD full funding scholarship from the National Institute for International Education(NIIED),Republic of Korea.
文摘The present work aims to study the influence of direct current and pulse current techniques as well as embedded SiC nanoparticles on the mechanical properties of the electrodeposited Ni-W coating.The electrodeposited coatings were studied for morphological,microstructural,mechanical,and scratch resistance properties using the surface roughness tester,scanning electron microscopy,energy-dispersive X-ray spectroscopy,X-ray diffraction,Vickers microhardness,and scratch tester.Application of pulse current exhibited relatively homogeneous and smooth surface of the coatings.A remarkable increment of microhardness was observed in both Ni-W and Ni-W-SiC coatings prepared under pulse current as compared to the direct current technique.Similarly,the scratch test revealed a considerable improvement in the scratch resistance behavior of the Ni-W alloy and the composite coatings from the pulsed current condition.Hence,the application of pulse current not only improved the surface-and microstructure-related properties but also enhanced the Vickers microhardness and scratch resistance properties of the coatings.In addition,the reduction in micro-cracks revealed the improvement in scratch resistance properties of the coatings due to the incorporated SiC nanoparticles into the Ni-W alloy matrix.
基金This research was supported by the“International standardization of nickel-phosphorous ceramics electroless composite plating for industrial use”program through the “Korea Evaluation Institute of Industrial Technology”of Korea funded by the Ministry of Science,ICT and Future planning(Grant No.10080067)。
文摘Ni-W-TiC composite coatings were prepared via electrodeposition technique by dispersing the different amount of TiC particles into the plating bath.The Ni-W and Ni-W-TiC composite coatings containing different concentrations of TiC particles were characterized by using the scanning electron microscope,X-ray diffraction technique,Vickers microhardness test,surface roughness test,and tribology test.The results show that the Ni-W coatings containing reinforced TiC particles have shown a typical FCC Ni-W crystal structure with significantly higher Vickers microhardness.The amount of dispersed TiC particles into the plating bath considerably affected codeposition weight percent of TiC into the Ni-W matrix,as revealed by the EDS analysis.Ni-W-TiC samples demonstrated the decreased abrasive wear as compared to Ni-W coating and no characteristic features observed for the adhesive wear.Similarly,an improvement in coefficient of friction was observed in Ni-W-TiC composite coating as compared to Ni-W coating.
