The dynamic process of non-equilibrium grain boundary segregation of traceboron in Fe-40 percent Ni alloy during cooling and the effect of cooling rate were investigated byboron tracking autoradiography technique. The...The dynamic process of non-equilibrium grain boundary segregation of traceboron in Fe-40 percent Ni alloy during cooling and the effect of cooling rate were investigated byboron tracking autoradiography technique. The results indicate that during cooling process, theamount of segregated boron on grain boundary firstly increases fast, then enters a comparativelyeven increasing stage and increases rapidly again at the third stage. The details of each stagevaried with cooling rate are explained. When the segregation develops to a certain degree, thesegregated boron atoms transform from solute status to precipitate status.展开更多
The moving boundary non-equilibrium segregation duringrecrystallization and the influence of pre-deformation in Fe-30/100Ni alloy at 1000 deg. C was investigated by the PTA(particle trackingautoradiography)technique, ...The moving boundary non-equilibrium segregation duringrecrystallization and the influence of pre-deformation in Fe-30/100Ni alloy at 1000 deg. C was investigated by the PTA(particle trackingautoradiography)technique, optical and electron microscopy. The re-Sults indicated that intensity of boron segregation on movingboundary after different deformation is concerned with thepre-deformation Degree and the moving speed of the boundary. TheTEM(transmission electron microscopy(result showed that thedislocation density Nearby the moving boundary increase obviously.The phenomena are discussed by the widening grain boundary mechanism.展开更多
基金This work was financially supported by the Projects of Development of the State Key Fundamental Research(National 973 Project)(No.G19980601507).]
文摘The dynamic process of non-equilibrium grain boundary segregation of traceboron in Fe-40 percent Ni alloy during cooling and the effect of cooling rate were investigated byboron tracking autoradiography technique. The results indicate that during cooling process, theamount of segregated boron on grain boundary firstly increases fast, then enters a comparativelyeven increasing stage and increases rapidly again at the third stage. The details of each stagevaried with cooling rate are explained. When the segregation develops to a certain degree, thesegregated boron atoms transform from solute status to precipitate status.
基金financially supported by the National Natural Science foundation of China (No.59291000).
文摘The moving boundary non-equilibrium segregation duringrecrystallization and the influence of pre-deformation in Fe-30/100Ni alloy at 1000 deg. C was investigated by the PTA(particle trackingautoradiography)technique, optical and electron microscopy. The re-Sults indicated that intensity of boron segregation on movingboundary after different deformation is concerned with thepre-deformation Degree and the moving speed of the boundary. TheTEM(transmission electron microscopy(result showed that thedislocation density Nearby the moving boundary increase obviously.The phenomena are discussed by the widening grain boundary mechanism.