A decrease in the weight of aerospace vehicles,large ships,weapons,and high-speed trains will increase the demand for wide-width magnesium alloy plates and their composite parts to replace steel and plastic.An investi...A decrease in the weight of aerospace vehicles,large ships,weapons,and high-speed trains will increase the demand for wide-width magnesium alloy plates and their composite parts to replace steel and plastic.An investigation was conducted to study the variation in deformation behaviors along the transverse direction during the warm rolling of a 1480-mm-wide AZ31B plate.A uniaxial thermal compression test with a 59%reduction was performed at different positions on a 13.7-mm-thick rolled plate along the width direction at a temperature of 220℃ and 270℃ and strain rate of 15 s^(−1).At the same time,the 13.7-mm-thick plate was rolled in a single pass to 5.6 mm on a mill with a 1725-mm-wide roll to confirm the thermal deformation behavior and the dynamic recrystallization(DRX).The results show that the main texture type does not change and the grain size does not have a clear deflection when the magnesium alloy plate reaches a certain value under rolling accumulative reduction.The grain size of a 13.7-mm-thick plate increases with a decrease in the distance to the center layer in the thickness direction.In the width direction,the edge(R6)first decreases and then increases toward the symmetric plane(R1).The critical stress required for dynamic recrystallization in the transition zone R3 of the rolled plate width is minimum,and the average grain size is minimum owing to the relatively complete recrystallization.展开更多
In this study,accumulated extrusion bonding(AEB)process with application of artificial water cooling was successfully performed to fabricate fined-grains AZ31B Mg alloy sheets at 150℃,200℃ and 250℃.The resultant mi...In this study,accumulated extrusion bonding(AEB)process with application of artificial water cooling was successfully performed to fabricate fined-grains AZ31B Mg alloy sheets at 150℃,200℃ and 250℃.The resultant microstructure and mechanical properties are systematically investigated.It reveals that the processing temperature has an important effect on the microstructural evolution during extrusion.During AEB process at 150℃ and 200℃,{10-12}tensile twinning was activated at early stage of extrusion,and subsequently continuous dynamic recrystallization(CDRX)occurred and dominated the further deformation.However,for the sample extruded at 250℃,hardly any twins can be observed,and new fined dynamic recrystallized grains were found along grain boundaries.Artificial cooling was utilized to reduce the rate of grain growth out of the extrusion die,resulting the grains significantly refined from 11μm to 2.5μm.Local high dislocation density region was also observed in the microstructure of sample processed at 150℃ in artificial cooling condition,and the degree decreased with the processing temperature increase.The results summarized from tensile tests indicated that due to the grain refinement the strength and ductility was significantly enhanced(YS of 186 MPa vs.145 MPa,UTS of 391 MPa vs.336 MPa and FE of 31.5%vs.24.5%compared with the as-received sample).Subsequently,annealing treatment at different temperatures was applied to eliminate the high dislocation density.The sample annealed at 200℃ exhibited the best comprehensive mechanical property with YS of 179 MPa,UTS of 390 MPa and FE of 33.0%.As the annealing temperature increasing,the dislocation density was reduced by static recrystallization(SRX)and grain growth,leading to a decreased strength and ductility.展开更多
Currently, when magnesium alloy sheet is rolled, the method of controlling roll temperature is simple and inaccurate. Furthermore, roll temperature has a large influence on the quality of magnesium alloy sheet; theref...Currently, when magnesium alloy sheet is rolled, the method of controlling roll temperature is simple and inaccurate. Furthermore, roll temperature has a large influence on the quality of magnesium alloy sheet; therefore, a new model using circular fluid flow control roll temperature has been designed. A fluid heat transfer structure was designed, the heat transfer process model of the fluid heating roll was simplified, and the finite di erence method was used to cal?culate the heat transfer process. Fluent software was used to simulate the fluid?solid coupling heat transfer, and both the trend and regularity of the temperature field in the heat transfer process were identified. The results show that the heating e ciency was much higher than traditional heating methods(when the fluid heat of the roll and tempera?ture distribution of the roll surface was more uniform). Moreover, there was a bigger temperature di erence between the input and the output, and after using reverse flow the temperature di erence decreased. The axial and circum?ferential temperature distributions along the sheet were uniform. Both theoretical calculation results and numerical simulation results of the heat transfer between fluid and roll were compared. The error was 1.8%–12.3%, showing that the theoretical model can both forecast and regulate the temperature of the roll(for magnesium alloy sheets) in the rolling process.展开更多
In order to predict flow instability of wear-resistant steel BTW1, the hot compressions of wear-resistant steel BTW1 were firstly performed at the temperature of 900-1150 ℃ and at the strain rate of 0.05-15 s-1. Then...In order to predict flow instability of wear-resistant steel BTW1, the hot compressions of wear-resistant steel BTW1 were firstly performed at the temperature of 900-1150 ℃ and at the strain rate of 0.05-15 s-1. Then, the constitutive relation was established based on Arrhenius-type hyperbolic sine equation. The results demonstrated that the flow stress depended on the deformation temperature and strain rate. When the deformation temperature kept constant, the flow stress increased as the strain rate increased. When the strain rate remained constant, the flow stress decreased as the temperature increased. The flow stresses calculated by constitutive equations were in a good agreement with experimental results. The apparent activation energy for deformation in the above processing region was estimated to be 369 kJ tool-1. A processing map could be obtained by the superimposition of an instability map on a power dissipation map. Based on the analysis of processing map and the microstructures, the theological instability regimes of strain rate and temperature for hot deformation of wear-resistant steel BTWl had been identified.展开更多
Gradient microstructure modification is a cost-efficient strategy for high strength without compromising ductility,which is urgently needed in the fundamental science of engineering materials.In this study,heterogeneo...Gradient microstructure modification is a cost-efficient strategy for high strength without compromising ductility,which is urgently needed in the fundamental science of engineering materials.In this study,heterogeneous structures of AZ61 alloy bars with anisotropic gradients(with different grain size distributions from the surface to the center)were observed to exhibit strong strength-ductility synergies under different deformation tem peratures.The results reveal that the grain refinement process under mediumlow temperature deformation conditions(≤350℃)consists of four transition stages along the radial direction,i.e.,twin activations and deformation band formations,dislocation cells and pile-ups,ultrafine sub-grains,and randomly orientated quasi-micron grains.Different deformation temperatures have a great influence on twin activations and deformation band formations,and the high temperature can easily provoke the initiation of non-basal slip.The deformation bands were determined as a primary nucleation site due to their highly unstable dislocation hindrance ability.Analysis in combination with the Radial forging(RF)deformation process,the differences of dynamic precipitates can be attributed to microstructural difference and solubility limit of Al at different tem peratures.By summarizing the tensile test results,the sample forged at 350℃exhibited the best strength-ductility synergy,exhibiting the highest elongation(EL)of 23.2%with a 251 MPa yield strength(YS)and 394 MPa ultimate tensile strength(UTS)in center region,and combined with the highest strength value of 256 MPa YS and 420 MPa UTS in the center region,while the EL was slightly degraded to 19.8%.展开更多
基金Supported by National Natural Science Foundation of China(Grant Nos.U1910213,U1610253,51604181)Shanxi Provincial Key Research and Development Program of China(Grant Nos.201603D111004,201803D121026).
文摘A decrease in the weight of aerospace vehicles,large ships,weapons,and high-speed trains will increase the demand for wide-width magnesium alloy plates and their composite parts to replace steel and plastic.An investigation was conducted to study the variation in deformation behaviors along the transverse direction during the warm rolling of a 1480-mm-wide AZ31B plate.A uniaxial thermal compression test with a 59%reduction was performed at different positions on a 13.7-mm-thick rolled plate along the width direction at a temperature of 220℃ and 270℃ and strain rate of 15 s^(−1).At the same time,the 13.7-mm-thick plate was rolled in a single pass to 5.6 mm on a mill with a 1725-mm-wide roll to confirm the thermal deformation behavior and the dynamic recrystallization(DRX).The results show that the main texture type does not change and the grain size does not have a clear deflection when the magnesium alloy plate reaches a certain value under rolling accumulative reduction.The grain size of a 13.7-mm-thick plate increases with a decrease in the distance to the center layer in the thickness direction.In the width direction,the edge(R6)first decreases and then increases toward the symmetric plane(R1).The critical stress required for dynamic recrystallization in the transition zone R3 of the rolled plate width is minimum,and the average grain size is minimum owing to the relatively complete recrystallization.
基金the National Natural Science Foundation of China(No.51905366,51901149,51671041,51604181,U1910213 and U1610253)the Key Research and Development Program of Shanxi Province(No.201603D111004)+1 种基金the Fund for Shanxi“1331 Project”Key Subjects Construction,Scientific and Technological Innovation Programs of Higher Education Institutions in Shanxi(No.2019L0632)Taiyuan University of Science and Technology Scientific Research Initial Funding(20182030,20192003 and 20192008)。
文摘In this study,accumulated extrusion bonding(AEB)process with application of artificial water cooling was successfully performed to fabricate fined-grains AZ31B Mg alloy sheets at 150℃,200℃ and 250℃.The resultant microstructure and mechanical properties are systematically investigated.It reveals that the processing temperature has an important effect on the microstructural evolution during extrusion.During AEB process at 150℃ and 200℃,{10-12}tensile twinning was activated at early stage of extrusion,and subsequently continuous dynamic recrystallization(CDRX)occurred and dominated the further deformation.However,for the sample extruded at 250℃,hardly any twins can be observed,and new fined dynamic recrystallized grains were found along grain boundaries.Artificial cooling was utilized to reduce the rate of grain growth out of the extrusion die,resulting the grains significantly refined from 11μm to 2.5μm.Local high dislocation density region was also observed in the microstructure of sample processed at 150℃ in artificial cooling condition,and the degree decreased with the processing temperature increase.The results summarized from tensile tests indicated that due to the grain refinement the strength and ductility was significantly enhanced(YS of 186 MPa vs.145 MPa,UTS of 391 MPa vs.336 MPa and FE of 31.5%vs.24.5%compared with the as-received sample).Subsequently,annealing treatment at different temperatures was applied to eliminate the high dislocation density.The sample annealed at 200℃ exhibited the best comprehensive mechanical property with YS of 179 MPa,UTS of 390 MPa and FE of 33.0%.As the annealing temperature increasing,the dislocation density was reduced by static recrystallization(SRX)and grain growth,leading to a decreased strength and ductility.
基金National Natural Science Foundation of China(Grant No.U1510131)Key Research and Development Projects of Shanxi Province of China(Grant Nos.201603D121010,201603D111004)+3 种基金Science and Technology Project of Jin Cheng City of China(Grant No.20155010)Youth Program of National Natural Science Fund of China(Grant No.51604181)Project of Young Scholar of Shanxi ProvinceLeading Talent Project of Innovative Entrepreneurial Team of Jiangsu Province(Grant No.51501122)
文摘Currently, when magnesium alloy sheet is rolled, the method of controlling roll temperature is simple and inaccurate. Furthermore, roll temperature has a large influence on the quality of magnesium alloy sheet; therefore, a new model using circular fluid flow control roll temperature has been designed. A fluid heat transfer structure was designed, the heat transfer process model of the fluid heating roll was simplified, and the finite di erence method was used to cal?culate the heat transfer process. Fluent software was used to simulate the fluid?solid coupling heat transfer, and both the trend and regularity of the temperature field in the heat transfer process were identified. The results show that the heating e ciency was much higher than traditional heating methods(when the fluid heat of the roll and tempera?ture distribution of the roll surface was more uniform). Moreover, there was a bigger temperature di erence between the input and the output, and after using reverse flow the temperature di erence decreased. The axial and circum?ferential temperature distributions along the sheet were uniform. Both theoretical calculation results and numerical simulation results of the heat transfer between fluid and roll were compared. The error was 1.8%–12.3%, showing that the theoretical model can both forecast and regulate the temperature of the roll(for magnesium alloy sheets) in the rolling process.
基金This work was supported by the National Natural Science Foundation of China (No. U1510131) and the Applied Basic Research Project of Shanxi Province (Nos. 201701D121078 and 201701D221143).
文摘In order to predict flow instability of wear-resistant steel BTW1, the hot compressions of wear-resistant steel BTW1 were firstly performed at the temperature of 900-1150 ℃ and at the strain rate of 0.05-15 s-1. Then, the constitutive relation was established based on Arrhenius-type hyperbolic sine equation. The results demonstrated that the flow stress depended on the deformation temperature and strain rate. When the deformation temperature kept constant, the flow stress increased as the strain rate increased. When the strain rate remained constant, the flow stress decreased as the temperature increased. The flow stresses calculated by constitutive equations were in a good agreement with experimental results. The apparent activation energy for deformation in the above processing region was estimated to be 369 kJ tool-1. A processing map could be obtained by the superimposition of an instability map on a power dissipation map. Based on the analysis of processing map and the microstructures, the theological instability regimes of strain rate and temperature for hot deformation of wear-resistant steel BTWl had been identified.
基金the financial support of the National Natural Science Foundation of China(Nos.U1910213 and 52205400)the China Postdoctoral Science Foundation(No.2021M692626)+2 种基金the Fundamental Research Program of Shanxi Province(No.202203021212321)Technological Innovation Talent Team Special Plan of Shanxi Province(No.202204051002002)the Doctoral Starting up Foundation of Taiyuan University of Science and Technology(No.20222046).
文摘Gradient microstructure modification is a cost-efficient strategy for high strength without compromising ductility,which is urgently needed in the fundamental science of engineering materials.In this study,heterogeneous structures of AZ61 alloy bars with anisotropic gradients(with different grain size distributions from the surface to the center)were observed to exhibit strong strength-ductility synergies under different deformation tem peratures.The results reveal that the grain refinement process under mediumlow temperature deformation conditions(≤350℃)consists of four transition stages along the radial direction,i.e.,twin activations and deformation band formations,dislocation cells and pile-ups,ultrafine sub-grains,and randomly orientated quasi-micron grains.Different deformation temperatures have a great influence on twin activations and deformation band formations,and the high temperature can easily provoke the initiation of non-basal slip.The deformation bands were determined as a primary nucleation site due to their highly unstable dislocation hindrance ability.Analysis in combination with the Radial forging(RF)deformation process,the differences of dynamic precipitates can be attributed to microstructural difference and solubility limit of Al at different tem peratures.By summarizing the tensile test results,the sample forged at 350℃exhibited the best strength-ductility synergy,exhibiting the highest elongation(EL)of 23.2%with a 251 MPa yield strength(YS)and 394 MPa ultimate tensile strength(UTS)in center region,and combined with the highest strength value of 256 MPa YS and 420 MPa UTS in the center region,while the EL was slightly degraded to 19.8%.