Several Ni-W-P-TiO_(2) nanocomposite coatings were developed by the sol-enhanced electroplating method. The phase and elemental compositions of coatings were determined, and the surface and cross-section morphology we...Several Ni-W-P-TiO_(2) nanocomposite coatings were developed by the sol-enhanced electroplating method. The phase and elemental compositions of coatings were determined, and the surface and cross-section morphology were characterized. The mechanical and corrosion performance were systematically tested. The results revealed the addition of 5 ml·L^(-1) TiO_(2) sol caused a compact coating surface,while higher concentrations of TiO_(2) reduced the coating thickness and led to the inferior surface microstructure. The comparison in physiochemical properties of prepared coatings confirmed the superior performance of the Ni-W-P-TiO_(2) nanocomposite coating at 5 ml·L^(-1) TiO_(2) sol addition. Under this condition, the best mechanical properties were achieved when abrasive wear was the dominating wearresistance mechanism, and the best corrosion resistance was obtained due to its smooth and compact surface microstructure.展开更多
The effects of T4,T5,and T6 treatment on the microstructure and mechanical properties of the extruded Mg-4.3Gd-3.2Y-1.2Zn-0.5Zr(wt.%)alloy with a relatively low RE content(7.5 wt.%)were investigated.T4 treatment at 45...The effects of T4,T5,and T6 treatment on the microstructure and mechanical properties of the extruded Mg-4.3Gd-3.2Y-1.2Zn-0.5Zr(wt.%)alloy with a relatively low RE content(7.5 wt.%)were investigated.T4 treatment at 450–500°C induces a gradual grain growth ofα-Mg but an obvious transition of texture component from<0001>⊥ED to<0001>∥ED.Interdendritic LPSO phases are highly stable against annealing while intragranular ones experience dissolution and re-precipitation.After peak-ageing at 200°C,the elongation of as-extruded and T4 samples is just slightly reduced or even increased due to the weak ageing hardening response.T5 sample exhibits an attractive combination of strength and ductility,with a tensile yield strength(TYS)of 303 MPa and elongation of 20.0%.The Hall–Petch relation for the alloys with or without ageing treatment has been estimated.Grain boundary strengthening rather than precipitation strengthening has the dominant contribution to TYS,and a modified equation is developed to predict grain boundary strengthening values for Mg-Gd-Y-Zn-Zr alloys which contain different Schmid factors for basal slip.展开更多
基金funded by Natural Science Foundation of Jiangsu Province (BK20201008)Key Research and Development Project of Zhenjiang (GJ2020014)National Natural Science Foundation of China (51701087)。
文摘Several Ni-W-P-TiO_(2) nanocomposite coatings were developed by the sol-enhanced electroplating method. The phase and elemental compositions of coatings were determined, and the surface and cross-section morphology were characterized. The mechanical and corrosion performance were systematically tested. The results revealed the addition of 5 ml·L^(-1) TiO_(2) sol caused a compact coating surface,while higher concentrations of TiO_(2) reduced the coating thickness and led to the inferior surface microstructure. The comparison in physiochemical properties of prepared coatings confirmed the superior performance of the Ni-W-P-TiO_(2) nanocomposite coating at 5 ml·L^(-1) TiO_(2) sol addition. Under this condition, the best mechanical properties were achieved when abrasive wear was the dominating wearresistance mechanism, and the best corrosion resistance was obtained due to its smooth and compact surface microstructure.
基金the National Natural Science Foundation of China(Nos.51904036 and 51874049)the Hunan Provincial Natural Science Foundation of China(Nos.2020JJ5600 and 2018JJ2365)+1 种基金the Hunan Education Department Outstanding Youth Project of China(No.17B069)the Scientific Research Project of Hunan Education Department(No.20C0088).
文摘The effects of T4,T5,and T6 treatment on the microstructure and mechanical properties of the extruded Mg-4.3Gd-3.2Y-1.2Zn-0.5Zr(wt.%)alloy with a relatively low RE content(7.5 wt.%)were investigated.T4 treatment at 450–500°C induces a gradual grain growth ofα-Mg but an obvious transition of texture component from<0001>⊥ED to<0001>∥ED.Interdendritic LPSO phases are highly stable against annealing while intragranular ones experience dissolution and re-precipitation.After peak-ageing at 200°C,the elongation of as-extruded and T4 samples is just slightly reduced or even increased due to the weak ageing hardening response.T5 sample exhibits an attractive combination of strength and ductility,with a tensile yield strength(TYS)of 303 MPa and elongation of 20.0%.The Hall–Petch relation for the alloys with or without ageing treatment has been estimated.Grain boundary strengthening rather than precipitation strengthening has the dominant contribution to TYS,and a modified equation is developed to predict grain boundary strengthening values for Mg-Gd-Y-Zn-Zr alloys which contain different Schmid factors for basal slip.
