A columnar Al film was firstly deposited on the top of 7%Y2O3？stabilized zirconia （7YSZ） ceramic coating in thermal barrier coating （TBC） system by magnetron sputtering. A vacuum treatment was then carried out at...A columnar Al film was firstly deposited on the top of 7%Y2O3？stabilized zirconia （7YSZ） ceramic coating in thermal barrier coating （TBC） system by magnetron sputtering. A vacuum treatment was then carried out at 700 °C for 1 h and 900 °C for 5 h to improve the erosion resistance of Al-deposited TBC. Aα-Al2O3 layer was in situ synthesized on the top of 7YSZ coating via vacuum heat treatment. The microstructure evolution of Al-deposited TBC illustrated that a loose surface-layer and a dense sub-layer formed on the top of 7YSZ coating after vacuum treatment. The phase structures of the as-sprayed TBC and the Al-deposited TBC after vacuum heat treatment were characterized by X-ray diffraction （XRD） and transmission electron microscope （TEM） assisted with focused ion beam （FIB）. Particulate erosion resistances of the as-sprayed TBC and treated TBC were compared at room temperature. In addition, erosion mechanism and schematic diagram were proposed. The results show that the Al-deposited TBC after vacuum heat treatment has better particulate erosion resistance than the as-sprayed one.展开更多
基金Project(2012CB625100)supported by the National Basic Research Program of ChinaProject(2012AA03A512)supported by the National High-tech Research and Development Program of China
文摘A columnar Al film was firstly deposited on the top of 7%Y2O3？stabilized zirconia （7YSZ） ceramic coating in thermal barrier coating （TBC） system by magnetron sputtering. A vacuum treatment was then carried out at 700 °C for 1 h and 900 °C for 5 h to improve the erosion resistance of Al-deposited TBC. Aα-Al2O3 layer was in situ synthesized on the top of 7YSZ coating via vacuum heat treatment. The microstructure evolution of Al-deposited TBC illustrated that a loose surface-layer and a dense sub-layer formed on the top of 7YSZ coating after vacuum treatment. The phase structures of the as-sprayed TBC and the Al-deposited TBC after vacuum heat treatment were characterized by X-ray diffraction （XRD） and transmission electron microscope （TEM） assisted with focused ion beam （FIB）. Particulate erosion resistances of the as-sprayed TBC and treated TBC were compared at room temperature. In addition, erosion mechanism and schematic diagram were proposed. The results show that the Al-deposited TBC after vacuum heat treatment has better particulate erosion resistance than the as-sprayed one.
