Friction stir welding (FSW) has many advantages rather than fusion welding, but details of internal phenomena during its processes have not yet been clarified. In this study, a thermo-mechanically coupled process mode...Friction stir welding (FSW) has many advantages rather than fusion welding, but details of internal phenomena during its processes have not yet been clarified. In this study, a thermo-mechanically coupled process model was developed to investigate FSW phenomena inside a tool and workpiece. As a workpiece, 6061-T6 aluminum alloy was employed. The system of FSW process model includes several thermal boundaries. Among heat flows through these boundaries, heat transfers into the exterior of the system become more sensitive to tool and workpiece temperatures than heat transfers within the system. This paper especially focused on a heat transfer coefficient at a workpiece bottom, and optimized it through experiments and finite element method (FEM) analyses. The tool temperatures during FSW were measured with a special tooling system with imbedded thermocouples within a tool. As a result, an analysis model that is able to investigate details at a wide range of traverse speeds was developed for practical high speed welding. Then, the accuracy of developed FEM model was validated with them. Finally, the temperatures and stress distribution around workpiece/tool interfaces were investigated with the developed model.展开更多
On the basis of homogeneous liquid-liquid extraction (HoLLE) with Zonyl FSA to plating water containing 1 mg palladium, 96.6% of the palladium was extracted into the sedimented liquid phase. After phase separation, th...On the basis of homogeneous liquid-liquid extraction (HoLLE) with Zonyl FSA to plating water containing 1 mg palladium, 96.6% of the palladium was extracted into the sedimented liquid phase. After phase separation, the volume ratio (Va/Vs) of the aqueous phase (Va) and the sedimented liquid phase (Vs) was 556 (50 mL → 0.09 mL). The assessment of the potential implementation of this procedure to wastewater treatment showed that HoLLE was satisfactorily achieved when the volume was scaled up to 1000 mL. Moreover, HoLLE was conducted to real palladium plating wastewater generated in the plating industry. 94.5% of the palladium was extracted into the sedimented liquid phase. After phase separation, the volume ratio (Va/Vs) of the aqueous phase (Va) and the sedimented liquid phase (Vs) was 500 (50 mL → 0.1 mL). In addition, HoLLE could separate palladium from coexisting metals in real plating wastewater. This knowledge is expected to lead to the development of new separation and concentration technologies of rare metals from real plating wastewater.展开更多
文摘Friction stir welding (FSW) has many advantages rather than fusion welding, but details of internal phenomena during its processes have not yet been clarified. In this study, a thermo-mechanically coupled process model was developed to investigate FSW phenomena inside a tool and workpiece. As a workpiece, 6061-T6 aluminum alloy was employed. The system of FSW process model includes several thermal boundaries. Among heat flows through these boundaries, heat transfers into the exterior of the system become more sensitive to tool and workpiece temperatures than heat transfers within the system. This paper especially focused on a heat transfer coefficient at a workpiece bottom, and optimized it through experiments and finite element method (FEM) analyses. The tool temperatures during FSW were measured with a special tooling system with imbedded thermocouples within a tool. As a result, an analysis model that is able to investigate details at a wide range of traverse speeds was developed for practical high speed welding. Then, the accuracy of developed FEM model was validated with them. Finally, the temperatures and stress distribution around workpiece/tool interfaces were investigated with the developed model.
文摘On the basis of homogeneous liquid-liquid extraction (HoLLE) with Zonyl FSA to plating water containing 1 mg palladium, 96.6% of the palladium was extracted into the sedimented liquid phase. After phase separation, the volume ratio (Va/Vs) of the aqueous phase (Va) and the sedimented liquid phase (Vs) was 556 (50 mL → 0.09 mL). The assessment of the potential implementation of this procedure to wastewater treatment showed that HoLLE was satisfactorily achieved when the volume was scaled up to 1000 mL. Moreover, HoLLE was conducted to real palladium plating wastewater generated in the plating industry. 94.5% of the palladium was extracted into the sedimented liquid phase. After phase separation, the volume ratio (Va/Vs) of the aqueous phase (Va) and the sedimented liquid phase (Vs) was 500 (50 mL → 0.1 mL). In addition, HoLLE could separate palladium from coexisting metals in real plating wastewater. This knowledge is expected to lead to the development of new separation and concentration technologies of rare metals from real plating wastewater.
