Metal glycinate chelates are formed by glycine and metal compounds through chemical reactions.Calcium glycinate,magnesium glycinate and zinc glycinate are kinds of new-type and ideal nutrient supplements,which have sa...Metal glycinate chelates are formed by glycine and metal compounds through chemical reactions.Calcium glycinate,magnesium glycinate and zinc glycinate are kinds of new-type and ideal nutrient supplements,which have satisfactory physico-chemical properties and bioactivities.They are important for prophylaxis and treat metal deficiency.The structural characterization shows that the metal ion is bonded to the amino and carboxyl group to form two five-membered rings.This paper mainly studies the structure characterization of the metal chelated glycinates by their solubility,infrared spectrum,thermal analysis,mass spectrometry,polycrystal difrac-tion,the metal contents and glycine contents of calcium glycinate,magnesium glycinate and zinc glycinate.展开更多
Ten previously undescribed dammarane-type triterpenoid glycosides,cyclocarysaponins A–J(1–10),were isolated from the leaves of Cyclocarya paliurus(Batal.)Iljinskaja.The structures of these compounds were characteriz...Ten previously undescribed dammarane-type triterpenoid glycosides,cyclocarysaponins A–J(1–10),were isolated from the leaves of Cyclocarya paliurus(Batal.)Iljinskaja.The structures of these compounds were characterized through detailed spectroscopic analysis,including 1D and 2D nuclear magnetic resonance(NMR)and high-resolution electrospray ionization mass spectrometry(HR-ESI-MS).The cytotoxic activities of all isolates were assessed against five human cancer cell lines(Bel-7402,Caski,BGC-823,A2780,and HCT-116).Of the tested compounds,compounds 1,7,and 9 exhibited selective cytotoxicity against one or more human cancer cell lines.展开更多
文摘Metal glycinate chelates are formed by glycine and metal compounds through chemical reactions.Calcium glycinate,magnesium glycinate and zinc glycinate are kinds of new-type and ideal nutrient supplements,which have satisfactory physico-chemical properties and bioactivities.They are important for prophylaxis and treat metal deficiency.The structural characterization shows that the metal ion is bonded to the amino and carboxyl group to form two five-membered rings.This paper mainly studies the structure characterization of the metal chelated glycinates by their solubility,infrared spectrum,thermal analysis,mass spectrometry,polycrystal difrac-tion,the metal contents and glycine contents of calcium glycinate,magnesium glycinate and zinc glycinate.
基金supported by the National Natural Science Foundation of China(Nos.31960090 and 32160562)the State Key Laboratory of Food Science and Resources,Nanchang University(No.SKLF-ZZB-202129)。
文摘Ten previously undescribed dammarane-type triterpenoid glycosides,cyclocarysaponins A–J(1–10),were isolated from the leaves of Cyclocarya paliurus(Batal.)Iljinskaja.The structures of these compounds were characterized through detailed spectroscopic analysis,including 1D and 2D nuclear magnetic resonance(NMR)and high-resolution electrospray ionization mass spectrometry(HR-ESI-MS).The cytotoxic activities of all isolates were assessed against five human cancer cell lines(Bel-7402,Caski,BGC-823,A2780,and HCT-116).Of the tested compounds,compounds 1,7,and 9 exhibited selective cytotoxicity against one or more human cancer cell lines.
