ZnO nanostructures were prepared on corning glass substrate by flow coating process with different annealing temperature from 100?C to 600?C. Fresh and two days aged solutions were used to investigate the growth behav...ZnO nanostructures were prepared on corning glass substrate by flow coating process with different annealing temperature from 100?C to 600?C. Fresh and two days aged solutions were used to investigate the growth behavior and to evaluate the nanostructure of ZnO. The effect of preparation conditions on the deposition of ZnO nanostructure was investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), Raman, and photoluminescence spectroscopy (PL). The results indicated that the solution aging condition and annealing temperature have a strong influence on the morphology and structural properties of the ZnO nanostructure. The solution aged after two days shows the different morphologies compared with the freshly prepared solution.展开更多
The comparison of the low temperature sintering and the microwave dielectric properties of Li_(2)MgSiO_(4)(LMS)ceramics prepared by citrate gel(CG)route and solid state(SS)ceramic route are discussed in this paper.The...The comparison of the low temperature sintering and the microwave dielectric properties of Li_(2)MgSiO_(4)(LMS)ceramics prepared by citrate gel(CG)route and solid state(SS)ceramic route are discussed in this paper.The LMS prepared using CG route sintered at 1175℃/2h hasε_(r)=5.3 and tanδ=1×10^(-3)at 9 GHz.The si ntering temperature of LMS is lowered to 950℃with the addition of 5 wt%lithium magnesium zinc borosilicate glass and hasε_(r)=5.6 and tanδ=2×10^(-3)at 9GHz.The amount of glass required to lower the sintering temperature of ceramics prepared using CG are slightly higher than that of Ss ceramic route.The LMS ceramics prepared using SS ceramic route shows excellent microwave dielectric properties with low sintering tem-perature compared to CG route.展开更多
文摘ZnO nanostructures were prepared on corning glass substrate by flow coating process with different annealing temperature from 100?C to 600?C. Fresh and two days aged solutions were used to investigate the growth behavior and to evaluate the nanostructure of ZnO. The effect of preparation conditions on the deposition of ZnO nanostructure was investigated by scanning electron microscopy (SEM), X-ray diffraction (XRD), Raman, and photoluminescence spectroscopy (PL). The results indicated that the solution aging condition and annealing temperature have a strong influence on the morphology and structural properties of the ZnO nanostructure. The solution aged after two days shows the different morphologies compared with the freshly prepared solution.
文摘The comparison of the low temperature sintering and the microwave dielectric properties of Li_(2)MgSiO_(4)(LMS)ceramics prepared by citrate gel(CG)route and solid state(SS)ceramic route are discussed in this paper.The LMS prepared using CG route sintered at 1175℃/2h hasε_(r)=5.3 and tanδ=1×10^(-3)at 9 GHz.The si ntering temperature of LMS is lowered to 950℃with the addition of 5 wt%lithium magnesium zinc borosilicate glass and hasε_(r)=5.6 and tanδ=2×10^(-3)at 9GHz.The amount of glass required to lower the sintering temperature of ceramics prepared using CG are slightly higher than that of Ss ceramic route.The LMS ceramics prepared using SS ceramic route shows excellent microwave dielectric properties with low sintering tem-perature compared to CG route.
