This paper presents the estimation of three-dimensional volumetric errors of a machining center by using a tracking interferometer. A tracking interferometer is a laser interferometer with the mechanism to steer the l...This paper presents the estimation of three-dimensional volumetric errors of a machining center by using a tracking interferometer. A tracking interferometer is a laser interferometer with the mechanism to steer the laser direction to follow a target retroreflector. Based on the triangulation principle, the three-dimensional position of the target can be estimated from measured laser displacements. Its capability to measure three-dimensional positioning errors for arbitrary trajectories is important for the indirect measurement of the machine's kinematic model. This paper presents experimental investigation of the estimation accuracy of the multilateration-based measurement by a tracking interferometer. A tracking interferometer developed by a part of the authors is used in experiments. In the present experiment, the measured volume of target positions was 100 mm × 100 mm × 100 mm. The estimation accuracy of targets within this volume was not sufficiently high compared to the positioning error of the measured machine tool. The results of the experiment and simulation show that the estimation uncertainty is dependent on tracking interferometer locations relative to target locations. Error sensitivity analysis shows that wider distribution of tracker positions in XY improves the estimation accuracy.展开更多
The sampling Moiré(SM) method is one of the vision-based non-contact deformation measurement methods, which is a powerful tool for structural health monitoring and elucidation of damage mechanisms of materials. I...The sampling Moiré(SM) method is one of the vision-based non-contact deformation measurement methods, which is a powerful tool for structural health monitoring and elucidation of damage mechanisms of materials. In this review, the basic principle of the SM method for measuring the twodimensional displacement and strain distributions is introduced. When the grid is not a standard orthogonal grating and cracks exist on the specimen surface, the measurement methods are also stated. Two of the most typical application examples are described in detail. One is the dynamic deflection measurement of a large-scale concrete bridge, and the other is the residual thermal strain measurement of small-scale flip chip packages. Several further development points of this method are pointed out. The SM method is expected to be used for deformation measurement of various structures and materials for residual stress evaluation, crack location prediction, and crack growth evaluation on broad scales.展开更多
The frequency of digitally controlled iodine stabilized He-Ne laser locked to a hyperfine component in ^127I2 was measured using the National Metrology Institute of Japan's reference iodine stabilized He-Ne laser. Th...The frequency of digitally controlled iodine stabilized He-Ne laser locked to a hyperfine component in ^127I2 was measured using the National Metrology Institute of Japan's reference iodine stabilized He-Ne laser. This laser is operated under the conditions of the practical implementation and its frequency with respect to the International Committee for Weights and Measure recommended value is known from international comparisons. Adopting a sampling rate of 120 kHz for the control system of an iodine stabilized He-Ne laser enables frequency deviation of the test laser from the reference laser by + 5 kHz (relative accuracy of 1 ×10^11) thus limited only by the reproducibility of the iodine stabilized He-Ne laser itself.展开更多
Since first establishing thermal measurement techniques for micrometer-scale wires,various methods have been devised and improved upon.However,the uncertainty of different measurements on the same sample has not yet b...Since first establishing thermal measurement techniques for micrometer-scale wires,various methods have been devised and improved upon.However,the uncertainty of different measurements on the same sample has not yet been discussed.In this work,a round robin test was performed to compare the thermal conductivity and thermal diffusivity measurement methods for a fine metal wire.The tested material was a pure gold wire,with a diameter of 30μm.The wire was cut into certain lengths and distributed to four institutions using five different measurement methods:the direct current(DC)self-heating method,the DC heating T-type method,the 3ωmethod for thermal conductivity,the scanning laser heating alternating current(AC)method,and the spot periodic heating radiation thermometry method for thermal diffusivity.After completing the measurements,the reported thermal conductivity and thermal diffusivity at room temperature,i.e.,317 W·m^(-1)·K^(-1)and 128×10^(-6)m^(2)·s^(-1),respectively,were adopted as references for comparison with the measurement results.The advantages and disadvantages of each method are described in terms of the effect of electrical and thermal junctions fabricated on a wire,such as an electrode,a thermocouple,and a heat bath.The knowledge obtained from the tested methods will be useful for selecting and designing a measurement technique for various wire-like materials.展开更多
Carbazole-triazine dendrimers with a bulky terminal substituent were synthesized,and the thermally activated delayed fluorescence(TADF)property was investigated.Compared to unsubstituted carbazole dendrimers,dendrimer...Carbazole-triazine dendrimers with a bulky terminal substituent were synthesized,and the thermally activated delayed fluorescence(TADF)property was investigated.Compared to unsubstituted carbazole dendrimers,dendrimers with bulky terminal substituents showed comparable to better photoluminescence quantum yields(PLQY)in neat films.Phenylfluorene(PF)-substituted dendrimers showed the highest PLQY of 81%,a smallΔEst of 0.06 eV,and the fastest reverse intersystem crossing(RISC)rate of∼1×10^(5 )s^(−1) compared to other dendrimers.Phosphorescence measurements of dendrimers and dendrons(fragments)indicate that the close proximity of the triplet energy of phenylfluorene-substituted carbazole dendrons(^(3)LE)to that of phenylfluorene-substituted dendrimers(^(1)CT,^(3)CT)contributes to RISC promotion and improves TADF efficiency.Terminal modification fine-tunes the energy level and suppresses intermolecular interactions,and this study provides a guideline for designing efficient solution-processable and non-doped TADF materials.展开更多
Sodium-ion batteries are promising for large-scale energy storage due to sodium's low cost and infinite abundance. The most popular cathodes for sodium-ion batteries, i.e., the layered sodium-containing oxides, us...Sodium-ion batteries are promising for large-scale energy storage due to sodium's low cost and infinite abundance. The most popular cathodes for sodium-ion batteries, i.e., the layered sodium-containing oxides, usually exhibit reversible host rearrangement between P-type and O-type stacking upon charge/discharge. Herein we demonstrate that such host rearrangement is unfavorable and can be suppressed by introducing transition-metal ions into sodium layers. The electrode with stabilized P3-type stacking delivers superior rate capability, high energy efficiency, and excellent cycling performance. Owing to the cation-mixing nature, it performs the lowest lattice strain among all reported cathodes for sodium-ion batteries. Our findings highlight the significance of a stable host for sodium-ion storage and moreover underline the fundamental distinction in material design strategy between lithium-and sodium-ion batteries.展开更多
文摘This paper presents the estimation of three-dimensional volumetric errors of a machining center by using a tracking interferometer. A tracking interferometer is a laser interferometer with the mechanism to steer the laser direction to follow a target retroreflector. Based on the triangulation principle, the three-dimensional position of the target can be estimated from measured laser displacements. Its capability to measure three-dimensional positioning errors for arbitrary trajectories is important for the indirect measurement of the machine's kinematic model. This paper presents experimental investigation of the estimation accuracy of the multilateration-based measurement by a tracking interferometer. A tracking interferometer developed by a part of the authors is used in experiments. In the present experiment, the measured volume of target positions was 100 mm × 100 mm × 100 mm. The estimation accuracy of targets within this volume was not sufficiently high compared to the positioning error of the measured machine tool. The results of the experiment and simulation show that the estimation uncertainty is dependent on tracking interferometer locations relative to target locations. Error sensitivity analysis shows that wider distribution of tracker positions in XY improves the estimation accuracy.
基金supported by Japan Society for the Promotion of Science (JSPS) KAKENHI (Grant Nos. JP20K04171 and JP20H02038)。
文摘The sampling Moiré(SM) method is one of the vision-based non-contact deformation measurement methods, which is a powerful tool for structural health monitoring and elucidation of damage mechanisms of materials. In this review, the basic principle of the SM method for measuring the twodimensional displacement and strain distributions is introduced. When the grid is not a standard orthogonal grating and cracks exist on the specimen surface, the measurement methods are also stated. Two of the most typical application examples are described in detail. One is the dynamic deflection measurement of a large-scale concrete bridge, and the other is the residual thermal strain measurement of small-scale flip chip packages. Several further development points of this method are pointed out. The SM method is expected to be used for deformation measurement of various structures and materials for residual stress evaluation, crack location prediction, and crack growth evaluation on broad scales.
文摘The frequency of digitally controlled iodine stabilized He-Ne laser locked to a hyperfine component in ^127I2 was measured using the National Metrology Institute of Japan's reference iodine stabilized He-Ne laser. This laser is operated under the conditions of the practical implementation and its frequency with respect to the International Committee for Weights and Measure recommended value is known from international comparisons. Adopting a sampling rate of 120 kHz for the control system of an iodine stabilized He-Ne laser enables frequency deviation of the test laser from the reference laser by + 5 kHz (relative accuracy of 1 ×10^11) thus limited only by the reproducibility of the iodine stabilized He-Ne laser itself.
文摘Since first establishing thermal measurement techniques for micrometer-scale wires,various methods have been devised and improved upon.However,the uncertainty of different measurements on the same sample has not yet been discussed.In this work,a round robin test was performed to compare the thermal conductivity and thermal diffusivity measurement methods for a fine metal wire.The tested material was a pure gold wire,with a diameter of 30μm.The wire was cut into certain lengths and distributed to four institutions using five different measurement methods:the direct current(DC)self-heating method,the DC heating T-type method,the 3ωmethod for thermal conductivity,the scanning laser heating alternating current(AC)method,and the spot periodic heating radiation thermometry method for thermal diffusivity.After completing the measurements,the reported thermal conductivity and thermal diffusivity at room temperature,i.e.,317 W·m^(-1)·K^(-1)and 128×10^(-6)m^(2)·s^(-1),respectively,were adopted as references for comparison with the measurement results.The advantages and disadvantages of each method are described in terms of the effect of electrical and thermal junctions fabricated on a wire,such as an electrode,a thermocouple,and a heat bath.The knowledge obtained from the tested methods will be useful for selecting and designing a measurement technique for various wire-like materials.
基金Ministry of Education,Culture,Sports,Science and Technology,Grant/Award Number:ARIM/JPMXP1222JI0040Japan Society for the Promotion of Science,Grant/Award Numbers:KAKENHI/JP20KK0316,KAKENHI/JP21H05405,KAKENHI/JP22H02055,KAKENHI/JP23H02026,KAKENHI/JP23H03966,KAKENHI/JP20H02801。
文摘Carbazole-triazine dendrimers with a bulky terminal substituent were synthesized,and the thermally activated delayed fluorescence(TADF)property was investigated.Compared to unsubstituted carbazole dendrimers,dendrimers with bulky terminal substituents showed comparable to better photoluminescence quantum yields(PLQY)in neat films.Phenylfluorene(PF)-substituted dendrimers showed the highest PLQY of 81%,a smallΔEst of 0.06 eV,and the fastest reverse intersystem crossing(RISC)rate of∼1×10^(5 )s^(−1) compared to other dendrimers.Phosphorescence measurements of dendrimers and dendrons(fragments)indicate that the close proximity of the triplet energy of phenylfluorene-substituted carbazole dendrons(^(3)LE)to that of phenylfluorene-substituted dendrimers(^(1)CT,^(3)CT)contributes to RISC promotion and improves TADF efficiency.Terminal modification fine-tunes the energy level and suppresses intermolecular interactions,and this study provides a guideline for designing efficient solution-processable and non-doped TADF materials.
基金The financial support from the National Basic Research Program of China(2014CB932300)Natural Science Foundation of Jiangsu Province of China(BK20170630)+1 种基金NSF of China(21633003 and 51602144)sponsored by the JST-CREST ‘‘Phase Interface Science for Highly Efficient Energy Utilization",JST(Japan)
文摘Sodium-ion batteries are promising for large-scale energy storage due to sodium's low cost and infinite abundance. The most popular cathodes for sodium-ion batteries, i.e., the layered sodium-containing oxides, usually exhibit reversible host rearrangement between P-type and O-type stacking upon charge/discharge. Herein we demonstrate that such host rearrangement is unfavorable and can be suppressed by introducing transition-metal ions into sodium layers. The electrode with stabilized P3-type stacking delivers superior rate capability, high energy efficiency, and excellent cycling performance. Owing to the cation-mixing nature, it performs the lowest lattice strain among all reported cathodes for sodium-ion batteries. Our findings highlight the significance of a stable host for sodium-ion storage and moreover underline the fundamental distinction in material design strategy between lithium-and sodium-ion batteries.